• Title/Summary/Keyword: Bonding test

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Effect of surface treatment on shear bond strength of relining material and 3D-printed denture base

  • Park, Se-Jick;Lee, Joon-Seok
    • The Journal of Advanced Prosthodontics
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    • v.14 no.4
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    • pp.262-272
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    • 2022
  • PURPOSE. This study aimed to analyze the shear bond strength between the 3D-printed denture base and the chairside relining material, according to the surface treatment. MATERIALS AND METHODS. Cylindrical specimens were prepared using DENTCA Denture Base II. The experimental groups were divided into 6 (n = 10): no surface treatment (C), Tokuyama Rebase II Normal adhesive (A), sandblasting (P), sandblasting and adhesive (PA), sandblasting and silane (PS), and the Rocatec system (PPS). After bonding the chairside relining material to the center of the specimens in a cylindrical shape, they were stored in distilled water for 24 hours. Shear bond strength was measured using a universal testing machine, and failure mode was analyzed with a scanning electron microscope. Shear bond strength values were analyzed using one-way analysis of variance, and Tukey's honest significant difference test was used for post-hoc analysis (P < .05). RESULTS. Group PPS exhibited significantly higher shear bond strength than all other groups. Groups P and PA displayed significantly higher bond strengths than the control group. There were no significant differences between groups PS and A compared to the control group. Regarding the failure mode, adhesive failure occurred primarily in groups C and A, and mixed failure mainly in groups P, PA, PS, and PPS. CONCLUSION. The shear bond strength between the 3D-printed denture base and the chairside relining material exhibited significant differences according to the surface treatment methods. It is believed that excellent adhesive strength will be obtained when the Rocatec system is applied to 3D-printed dentures in clinical practice.

Banana agriculture waste as eco-friendly material in fibre-reinforced concrete: An experimental study

  • Mohammed M., Attia;Abd Al-Kader A., Al Sayed;Bassam A., Tayeh;Shymaa M.M., Shawky
    • Advances in concrete construction
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    • v.14 no.5
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    • pp.355-368
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    • 2022
  • This paper investigates the impact of length and volume fractions (VFs) of banana fibres (BFs) on the mechanical and physical properties of concrete. The mechanical properties were compressive strength, splitting tensile, flexural strength, and bond stress, while the physical properties were unit weight and absorption. The slump test was used to determine workability. The concrete's behaviour with BFs was studied using scanning electron microscopy. Experimental work of concrete mixtures with BFs of various lengths (12 mm, 25 mm, and 35 mm) and VFs (0%, 0.5%, 1.0%, and 1.5%) were carried out. The samples did not indicate any agglomeration of fibres or heterogeneity during mixing. The addition of BFs to concrete with VFs of up to 1.50% for all fibre lengths have a significant impact on mechanical properties, also the longer fibres performed better than shorter ones at all volume fractions of BFs. The mix10, which contain BFs with VFs 1.5% and length 35 mm, demonstrated the highest mechanical properties. The compressive strength, splitting tensile, flexural strength, and bond stress of the mix10 were 37.71 MPa, 4.27 Mpa, 6.12 MPa, and 6.75 MPa, an increase of 7.37%, 20.96%, 24.13%, and 11.2% over the reference concrete, which was 35.12 MPa, 3.53 MPa, 4.93 MPa, and 6.07 MP, respectively. The absorption is increased for all lengths by increasing the VFs up to 1.5%. Longer fibres have lower absorption, while shorter fibres have higher absorption. The mix8 had the highest absorption of 4.52%, compared to 3.12% for the control mix. Furthermore, the microstructure of concrete was improved through improved bonding between the fibres and the matrix, which resulted in improved mechanical properties of the composite.

Ag Sintering Die Attach Technology for Wide-bandgap Power Semiconductor Packaging (Wide-bandgap 전력반도체 패키징을 위한 Ag 소결 다이접합 기술)

  • Min-Su Kim;Dongjin Kim
    • Journal of the Microelectronics and Packaging Society
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    • v.30 no.1
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    • pp.1-16
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    • 2023
  • Recently, the shift to next-generation wide-bandgap (WBG) power semiconductor for electric vehicle is accelerated due to the need to improve power conversion efficiency and to overcome the limitation of conventional Si power semiconductor. With the adoption of WBG semiconductor, it is also required that the packaging materials for power modules have high temperature durability. As an alternative to conventional high-temperature Pb-based solder, Ag sintering die attach, which is one of the power module packaging process, is receiving attention. In this study, we will introduce the recent research trends on the Ag sintering die attach process. The effects of sintering parameters on the bonding properties and methodology on the exact physical properties of Ag sintered layer by the realization 3D image are discussed. In addition, trends in thermal shock and power cycle reliability test results for power module are discussed.

Development of Bamboo Zephyr Composite and the Physical and Mechanical Properties

  • SUMARDI, Ihak;ALAMSYAH, Eka Mulya;SUHAYA, Yoyo;DUNGANI, Rudi;SULASTININGSIH, Ignasia Maria;PRAMESTIE, Syahdilla Risandra
    • Journal of the Korean Wood Science and Technology
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    • v.50 no.2
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    • pp.134-147
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    • 2022
  • The objective of this study is to determine the effect of fiber direction arrangement and layer composition of hybrid bamboo laminate boards on the physical and mechanical properties. The raw material used was tali bamboo (Gigantochloa apus (J.A. & J.H. Schultes) Kurs) rope in the form of flat sheets (zephyr) and falcata veneer (Paraserianthes falcataria (L) Nielsen). Zephyr bamboo was arranged in three layers using water-based isocyanate polymer (WBPI) with a glue spread rate of 300 g/m2. There were variations in the substitution of the core layer with falcata veneers (hybrid) as much as two layers and using a glue spread rate of 170 g/m2. The laminated bamboo board was cold-pressed at a pressure of 22.2 kgf/cm2 for 1 h, and the physical and mechanical properties were evaluated. The results showed that the arrangement of the fiber direction significantly affected the dimensional stability, modulus of rupture, modulus of elasticity, shear strength, and screw withdrawal strength. However, the composition of the layers had no significant effect on the physical and mechanical properties. The bonding quality of bamboo laminate boards with WBPI was considered to be quite good, as shown by the absence of delamination in all test samples. The bamboo hybrid laminate board can be an alternative based on the physical and mechanical properties that can meet laminated board standards.

A Study on Paving Technique using Polymer Epoxy Resin Materials (고분자 에폭시 수지혼합물을 이용한 포장기술 연구)

  • Oh, Seung Hwoon;Kim, Nak Seok;Kim, Wan Sang
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.29 no.2D
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    • pp.209-216
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    • 2009
  • This study was conducted to develop a thin paving technique using polymer epoxy resin materials which is considered as a durable pavement materials. The mechanical performance characteristics of the polymer epoxy resin materials were also evaluated to confirm the validity as a pavement materials. To estimate the performance properties of the materials, bending tests and bonding tests were performed using freeze-thaw and ultra-violet rays to accelerate the aging of materials. In addition, HYUNStay, a commercial structural analysis program for cable-stayed bridges, was used to compare the effect of paving materials between the polymer epoxy resin materials and the conventional ones on the reduction of cable tension and on the stability of the main tower. According to the test results, it is noted that the thin paving technique using polymer epoxy resin materials can improve the performance and durability of pavement compared to the conventional one.

A Study on the Strength Enhancement of Wale in Temporary Retaining Structures (흙막이 지하 가시설 구조체의 띠장 휨 강성 증대를 위한 연구)

  • Lim, Dong Hwan;Lee, Yong Jun;Ahn, Sang Ro
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.29 no.3C
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    • pp.91-96
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    • 2009
  • The purpose of this study was to investigate a method for the strength enhancement of wale in temporary retaining structures. Tests on the wale structures strengthened with carbon fibre reinforced plastic (CFRP) strips and prestressed with seven wire strands were conducted. From this test, it is found that the flexural stiffness and strength of the wales strengthened with CFRP strips and seven wire strands were significantly improved compared to the unstrengthened one. The ultimate tensile strains of attached CFRP strips on the steel beam were in the range of 8,000 and $11,000{\mu}{\epsilon}$, and it is noticed that the bonding ability with steel and CFRP strips is good. In this paper, a new method for enhancing the strength of wale in retaining structures is suggested.

Synthesis of Carbon Nano Silicon Composites for Secondary Battery Anode Materials Using RF Thermal Plasma (RF 열플라즈마를 이용한 이차전지 음극재용 탄소나노실리콘복합소재 합성)

  • Soon-Jik Lee;Dae-Shin Kim;Jeong-Mi Yeon;Won-Gyu Park;Myeong-Seon Shin;Seon-Yong Choi;Sung-Hoo Ju
    • Korean Journal of Materials Research
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    • v.33 no.6
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    • pp.257-264
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    • 2023
  • To develop a high capacity lithium secondary battery, a new approach to anode material synthesis is required, capable of producing an anode that exceeds the energy density limit of a carbon-based anode. This research synthesized carbon nano silicon composites as an anode material for a secondary battery using the RF thermal plasma method, which is an ecofriendly dry synthesis method. Prior to material synthesis, a silicon raw material was mixed at 10, 20, 30, 40, and 50 wt% based on the carbon raw material in a powder form, and the temperature change inside the reaction field depending on the applied plasma power was calculated. Information about the materials in the synthesized carbon nano silicon composites were confirmed through XRD analysis, showing carbon (86.7~52.6 %), silicon (7.2~36.2 %), and silicon carbide (6.1~11.2 %). Through FE-SEM analysis, it was confirmed that the silicon bonded to carbon was distributed at sizes of 100 nm or less. The bonding shape of the silicon nano particles bonded to carbon was observed through TEM analysis. The initial electrochemical charging/discharging test for the 40 wt% silicon mixture showed excellent electrical characteristics of 1,517 mAh/g (91.9 %) and an irreversible capacity of 133 mAh/g (8.1 %).

Influence of Composition of Layer Layout on Bending and Compression Strength Performance of Larix Cross-Laminated Timber (CLT)

  • Da-Bin SONG;Keon-Ho KIM
    • Journal of the Korean Wood Science and Technology
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    • v.51 no.4
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    • pp.239-252
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    • 2023
  • In this study, bending and compression strength tests were performed to investigate effect of composition of layer layout of Larix cross-laminated timber (CLT) on mechanical properties. The Larix CLT consists of five laminae, and specimens were classified into four types according to grade and composition of layer. The layer's layout were composited as follows 1) cross-laminating layers in major and minor direction (Type A), and 2) cross-laminating external layer in major direction and internal layer applied grade of layer in minor direction (Type B). E12 and E16 were used as grades of lamina for major direction layer of Type A and external layer of Type B according to KS F 3020. In results of the bending test of CLT using same grade layer according to layer composition, the modulus of elasticity (MOE) of Type B was higher than Type A. In case of prediction of bending MOE of Larix CLT, the experimental MOE was higher than 1.00 to 1.09 times for Shear analogy method and 1.14 to 1.25 times for Gamma method. Therefore, it is recommended to predict the bending MOE for Larix CLT by shear analogy method. Compression strength of CLT in accordance with layer composition was measured to be 2% and 9% higher for Type A using E12 and E16 layers than Type B, respectively. In failure mode of Type A, progress direction of failure generated under compression load was confirmed to transfer from major layer to minor layer by rolling shear or bonding line failure due to the middle lamina in major direction.

Effect of dentin roughening and type of composite material on the restoration of non-carious cervical lesions: an in vivo study with 18 months of follow-up

  • Sanjana Verma;Rakesh Singla;Gurdeep Singh Gill;Namita Jain
    • Restorative Dentistry and Endodontics
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    • v.48 no.4
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    • pp.35.1-35.14
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    • 2023
  • Objectives: The purpose of this study was to evaluate the impact of dentin roughening and the type of composite resin used (either bulk-fill flowable or nanohybrid) on the restoration of non-carious cervical lesions (NCCLs) with an 18-month follow-up period. Materials and Methods: This prospective split-mouth study included 36 patients, each with a minimum of 4 NCCLs. For each patient, 4 types of restorations were performed: unroughened dentin with nanohybrid composite, unroughened dentin with bulk-fill flowable composite, roughened dentin with nanohybrid composite, and roughened dentin with bulk-fill flowable composite. A universal bonding agent (Tetric N Bond Universal) was applied in self-etch mode for all groups. The restorations were subsequently evaluated at 6, 12, and 18 months in accordance with the criteria set by the FDI World Dental Federation. Inferential statistics were computed using the Friedman test, with the level of statistical significance established at 0.05. Results: The 4 groups exhibited no significant differences in relation to fracture and retention, marginal staining, marginal adaptation, postoperative hypersensitivity, or the recurrence of caries at any follow-up point. Conclusions: Within the limitations of the present study, over an 18-month follow-up period, no significant difference was present in the clinical performance of bulk-fill flowable and nanohybrid composite restorations of non-carious cervical lesions. This held true regardless of whether dentin roughening was performed.

Effect of Adding Graphene/Carbon Nanotubes (FCN) on the Mechanical Properties of Polyamide-Nylon 6 (그래핀/탄소나노튜브(FCN) 첨가에 따른 Polyamide-Nylon 6의 기계적 특성에 미치는 영향)

  • Seung-Jun Yeo;Hae-Reum Shin;Woo-Seung Noh;Man-Tae Kim
    • Journal of the Korean Society of Industry Convergence
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    • v.26 no.6_3
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    • pp.1297-1303
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    • 2023
  • Research on enhancing the mechanical strength, lightweight properties, electrical conductivity, and thermal conductivity of composite materials by incorporating nano-materials is actively underway. Thermoplastic resins can change their form under heat, making them highly processable and recyclable. In this study, Polyamide-Nylon 6 (PA6), a thermoplastic resin, was utilized, and as reinforcing agents, fused carbon nano-materials (FCN) formed by structurally combining Carbon Nanotube(CNT) and Graphene were employed. Nano-materials often face challenges related to cohesion and dispersion. To address this issue, Silane functional groups were introduced to enhance the dispersion of FCN in PA6. The manufacturing conditions for the composite materials involved determining the use of a dispersant and varying FCN content at 0.05 wt%, 0.1 wt%, and 0.2 wt%. Tensile strength measurements were conducted, and FE-SEM analysis was performed on fracture surfaces. As a result of the tensile strength test, it was confirmed that compared to pure PA6, the strength of the polymer composite with a content of 0.05 wt% was improved by about 60%, for 0.1 wt%, about 65%, and for 0.2 wt%, the strength was improved by 50%. Also, when compared according to the content of FCN, the best strength value was shown when 0.1 wt% was added. The elastic modulus also showed an improvement of about 15% in the case of surface treatment compared to the case without surface treatment, and an improvement of about 70% compared to pure PA6. Through FE-SEM, it was confirmed that the matrix material and silane-modified nanomaterial improved the dispersibility and bonding strength of the interface, helping to support the load evenly and enabling effective stress transfer.