• Journal of Magnetics
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• 제9권4호
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• pp.105-108
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• 2004

The attempt for the addition of double-phase nanocomposite $Nd_2Fe_{14}BFe_3B$ powders, respectively, into several $RE_2Fe_{14}B$(RE=Pr, Nd) powders with high magnetic properties was carried out. The powders were compounded and compressed to take shape bonded magnets. By means of investigating the variation of compound magnet $B_r$, the interaction between magnetic powders was revealed. The result shows that not chemical just but physical interaction exists between elements. The compound effect of $Nd_2Fe_{14}BFe_3B$-ferrite bonded magnets was detailed studied. The functional relation was revealed between magnetic properties and ferrite content. That is $Y = 5.42 x^2 -11.34x + 6.62$. The variation of $_iH_c$ temperature coefficient ${\beta}_{iHc}$ with ferrite content was investigated. Following the ferrite content increased, ${\beta}_{iHc}$ and $h_{irr}$ were obviously decreased, compression-resistant strength was enhanced.

• 폴리머
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• 제26권1호
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• pp.98-104
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• 2002

본 연구는 압축성형으로 제조되는 고특성 등방성 $Nd_2Fe_{14}B$/에폭시 본드자석을 개발하기 위하여 수행되었다. 본드자석의 자기특성은 본드자석의 밀도에 직접적으로 비례하였으며, 평균입도가 $200mu{m}$인 $Nd_2Fe_{14}B$ 자성분말을 분쇄공정 없이 그대로 사용할 때 고특성을 나타내었다. 본드자석은 자성분말 기준으로 2.0 wt%의 에폭시 수지, 0.8 wt%의 실란 커플링제, 0.7 wt%의 고온 경화제를 첨가하고, $150 ^{\circ}C$/3시간의 경화조건에서 높은 특성을 나타내었다. 적정조건에서 제조된 고특성 본드자석은 $6.1 g/cm^3$의 밀도, 7.1 kG의 잔류자속밀도, 9.7 MGOe의 최대자기에너지적, 그리고 17 kg/$mm^2$의 압축강도를 나타내었다.

• 한국전기전자재료학회논문지
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• 제23권12호
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• pp.988-995
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• 2010

In this study the (Alnico, Sm-Co) bonded magnets were fabricated by mixing the Sm-Co added alnico alloy powders with epoxy resin and binder, appropriately. Also, the hybrid ring magnets of (Alnico, Sm-Co)/Sr-ferrite were fabricated by coupling the Sr-ferrite composite layer with an (Alnico, Sm-Co) magnet. The magnetic properties of (Alnico, Sm-Co) ring magnets were varied with the amount of Sm-Co powders. The addition of Sm-Co powders increased a remanent induction($B_r$) and coercive force($_BH_C$), while decreasing a surface flux density and repulsive distance. The surface flux density and repulsive distance for the (Alnico, Sm-Co) ring magnet increased with a magnetizing voltage up to about 160 V and reached an apparent saturation point. Also, the measurements of temperature and moisture characteristics showed that the surface flux densities of N-S poles and repulsive distance decreased a little within 4% after 10 days passed.

• 한국정밀공학회지
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• 제17권2호
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• pp.89-96
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• 2000

This paper describes the characteristic of die finishing to obtain smooth surface using electro-chemical grinding after cutting process. Electro-chemical grinding is possible under lower load and tool wear comparing with those in the mechanical grinding. Conventionally, if the metal bonding material of the grinding wheel is directly t contacted with workpiece, the current is circulated without electrolytic phenomena. Sometimes, electrical discharge is occurred between tool and workpiece. To cope with this problem, the metal-resin bonded pellet was used in this study. This pellet is composed of optimal volume of metal and resin powders and its characteristics are changable with the each volume of powders. Finally, high efficient die finishing is realized using metal resin bonded pellet in electro-chemical grinding.

• 한국세라믹학회지
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• 제28권4호
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• pp.289-296
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• 1991

Hydroxyapatite (HAp)-zirconia bioceramics, which have excellent biocompatibility with tissue of bone and tooth and good mechanical properties, were synthesized, and their properties and biocompatibility were investigated. HAp powders were synthesized with Ca/P=1.67 and pH 11 by precipitation method. A fine spherical monodispersed ZrO2 powders were prepared by metal alkoxide method, and then they were partially stabilized with 10 mol% CaO by solid state reaction at 1300℃. HAp-zirconia composites were prepared by sintering of these HAp mixed with various amount CaO-partially stabillized zirconia (PSZ). When HAp containing 15 wt% PSZ with 10 mol% CaO (PSZ(10C)) were sintered at 1250℃, it was prevented to decompose into TCP and ZrO2 was uniformly dispersed at HAp matrix. Mechanical strength of these sintered bodies were increased by addition of 15 wt% PSZ(10C), the bending strength of compacts fired at 1250℃ was 165 MPa. HAp-PSZ composites chemically bonded each other in Ringer's solution and the component of bonded layer was HAp. These composites did not prevent cell-growing and exhibit any cytotoxic effects.

• 한국세라믹학회지
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• 제27권3호
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• pp.311-320
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• 1990

Hydroxyapatite powders were synthesized with Ca/P=1.67, 1.70 and pH=7, 11 by precipitation method and fluorine substituted hydroxyapatite ceramics were prepared using these powders. After characterization of these hydorxyapatite bioceramics, chemical bonding between these sepcimens in simulated body fluid was investigated. Bysubstitution of 7.5% of fluorine, hydroxyapatite was prevented to decompose into β-tricalcium phosphate and its sintered density and mechanical strength were increased. The bending strength of these hydroxyapatite ceramics was 137MPa. The hydroxyapatite ceramics chemically bonded each other in Ringer's solution and the component of bonded layer was also hydroxyapatite.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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• pp.742-743
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• 2006

Filling of the tool die directly influences dimensional tolerances and density variation. To minimize the variations in filling, both within different sections of the cavity and from part to part, are of great importance for produce high quality P/M parts. Filling of the tool die is also one of the limiting factors in the productivity in powder pressing. By using aeration filling in combination with bonded powder mixes, both weight scatter and productivity can be improved. In this presentation results are presented showing the benefit of using aeration filling for different types of powders

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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• pp.1286-1287
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• 2006

[ $Nd_2Fe_{14}B/{\alpha}-Fe$ ] nanocomposite powders with a nominal composition of $Nd_{12}Fe_{82}B_6$ were prepared by HDDR combined with mechanical milling. The microstructure was studied by Mossbauer spectrometry and TEM. The magnetic properties were investigated by VSM using bonded magnet samples. The results showed that the annealing temperature had significant influence on both the recombination kinetics and the grain size of the $Nd_2Fe_{14}B$ and ${\alpha}-Fe$ phases, and the bonded magnets presented the best magnetic properties when the nanocomposite powders were prepared by annealing at $760^{\circ}C$ for 30 min.

• 한국자기학회지
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• 제5권5호
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• pp.824-827
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• 1995

Dielectromagnets are permanent magnets made from resin-bonded hard magnetic powders. Magnetic properties of dielectromagnets depend on kind of used hard magnetic materials as chemical compound, shape, size of grain and applied technology. Comparison of advantages and disadvantages of dielectromagnets made from different kind of magnetic powders induced us to try to prepare dielectromagnets from mixture of hard magnetic powders, not only one of them. The purpose of investigation on this kind of dielectromagnets is to find formula to prepare permanent magnets with properties adequate to different kind of electrical motors requirements. As hard magnetic materials we used powders of ferrite, melt-spun ribbon Nd-Fe-B and Alnico. Papers present results of investigation on technology of this kind of dielectromagnets. It shows also influence of kind of mixture and used technology on magnetic properties of dielectromagnets.

• 한국세라믹학회지
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• 제39권1호
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• pp.45-50
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• 2002

평균입경 25$\mu m$의 Si조대분말에 소결조제의 조성과 양을 변화시켜 질화반응 질화규소 (RBSN)세라믹스를 제조할 때 나타나는 치밀화 거동, 미세구조의 발달 및 기계적 특성에 대하여 고찰하였다. 6wt% $Y_2O_3$ + 1wt% $Al_2O_3$(6YlA)의 소결조제를 첨가한 경우에는 치밀화를 이루지 못하였으나, 6wt% $Y_2O_3+3\;wt%\;Al_2O_3+2\;wt%\;SiO_2(6Y3A2S)$와 9wt% $Y_2O_3$+1.5wt% $A1_2O_3$+ 3w% $SiO_2$(9Yl.5A3S)의 소결조제를 첨가하여 이론밀도에 가까운 치밀화를 이루었다. $1900^{\circ}C$에서 소결한 6Y3A2S시편의 경우, 960MPa의 높은 파괴강도값과 $6.5MPa.m^{1/2}$의 파괴인성값을 얻었다.