• Proceedings of the KSME Conference
• /
• 2001.06d
• /
• pp.60-65
• /
• 2001

Bomb calorimeter was developed for measuring the calorific value of combustible matter such as wastes. The calorimeter consist of bomb, stirred-water type bucket, thermometer and ignition circuit. Operation and performance of the calorimeter have been tested experimentally. In the present study, calorific values of light oil, lamp oil and bunker C oil is measured using the bomb calorimeter. Mass of the sample is fixed at lg, and oxygen pressure in the bomb is used as an experimental parameter. Sample in the oxygen bomb is burned with electrically heated Ni-Cr wire of 100mm in length, and temperature of water in the bucket become increased by $5^{\circ}C$ during about 30min. Calorific value of the sample is calculated with the temperature difference of water. Combustion tests, such as the record of temperature history and the inspection of remnants, are performed at 4, 6, 8 and 10 atm of the oxygen pressure. From the test results, oxygen pressure in the bomb must be over 10atm for complete combustion.

• 한국연소학회:학술대회논문집
• /
• 2001.06a
• /
• pp.23-30
• /
• 2001

Bomb calorimeter was developed for measuring the calorific value of combustible matter such as wastes. The calorimeter consist of bomb, stirred-water type bucket, thermometer and ignition circuit. Operation and performance of the calorimeter have been tested experimentally. In the present study, calorific values of light oil, lamp oil, benzoic acid, ethyl alcohol and methyl alcohol is measured using the bomb calorimeter. Mass of the sample is fixed at 19, and oxygen pressure in the bomb is used as an experimental parameter. Sample in the oxygen bomb is burned with electrically heated Ni-Cr wire of 100mm in length, and temperature of water in the bucket become increased by $2{\sim}5^{\circ}C$ during about 30min. Calorific value of the sample is calculated with the temperature difference of water. Combustion tests, such as the record of temperature history and the inspection of remnants, are performed at 6, 8 and 10 atm of the oxygen pressure. From the test results, oxygen pressure in the bomb must be over 10atm for complete combustion.

• Journal of the Korean Wood Science and Technology
• /
• v.44 no.6
• /
• pp.864-871
• /
• 2016

This study was conducted to compare and analyze gross calorific values from measurement methods of lignocellulosic biomass and calculation data from calorific value prediction models based on the elemental content. The deviation of Liriodendron tulipifera (LT) and Populus euramericana (PE) was shown 7.7 cal/g and 7.4 cal/g respectively in palletization method, which are within repeatability limit 28.8 cal/g of ISO FDIS 18125. In the case of Thailand charcoal (TC), nontreatment method and palletization method was satisfied with repeatability limit as 22.8 cal/g and 8.8 cal/g respectively. Seowon charcoal (SC) was shown deviation of 11.4 cal/g in nontreatment method, because the density and chemical affinity of sample increases as the carbon content increases from heat treatment at high temperature in the case of TC and SC. In addition, after applying the elemental content of each of these samples to the calorific value prediction models, the study found that Model Equation (3) was relatively consistent with measured calorific values of all these lignocellulosic biomass. Thus, study about the correlation between the density and size of particle should be conducted in order to select the measurement method for a wide range of solid biofuels in the future.

• Proceedings of the Korean Society of Agricultural Engineers Conference
• /
• 2000.10a
• /
• pp.563-568
• /
• 2000

Animal waste is a major agricultural waste or wastewater that requires appropriate treatment to prevent environmental pollution. In this presentation, it is examined if incineration of manure compost is an alternative to treatment of animal waste. Heating values of selected biomass including manure compost were obtained using a bomb calorimeter. Based on heating values of manure and manure compost, ranging from 1200 - 1500 kcal/kg on wet base, incineration could be an alternative for animal waste treatment if available land is limited for land application and sufficient reduction of water content in manure compost.

• Fire Science and Engineering
• /
• v.22 no.5
• /
• pp.72-78
• /
• 2008

The mass loss rate and heat release rate of EPS sandwich panel cores were analysed using variable external irradiation level. The experimental materials were exposed to incident heat fluxes form 20 to 50 kW/$m^2$. For the measurement of mass loss rate and heat release rate, the size of specimen was $100mm{\times}100mm{\times}50mm$ and the samples were 3 different kinds. The combustion heat were carried out from the Oxygen bomb calorimeter and the mass loss rate and heat release rate were carried out from the Mass loss calorimeter according to ISO 5660-1. As the results of this study, the mass loss rate of Type A, B, and C were 2.7 g/$m^2s$, 2.8 g/$m^2s$, and 2.3 g/$m^2s$ and the heat release rate of Type A, B, and C were 58.23 kW/$m^2$, 47.19 kW/$m^2$, and 50.06 kW/$m^2$ respectively at the heat flux of 50 kW/$m^2$. In conclusion, when the heat release characteristics applied to a classification system of Canada, Type A and C can be classified grade C-3, and Type C can be classified grade C-2 from all data of this study.

• Fire Science and Engineering
• /
• v.22 no.3
• /
• pp.258-264
• /
• 2008

This study proposes the experimental methods which shows various guidelines for systematic study of surface forest fuels. The thermal characteristics of surface fire fuels such as Quercus Variabilis and Pinus Densiflora fallen leaves are measured using TGA and Oxygen Bomb Calorimeter. Both of them are common species of Korean forest. Also the combustion characteristics of surface fire fuels are analysed according to the methods which are commonly used in Pool Fire analysis. The measured parameters are gas velocity, temperature, flame height, heat release rate and mass loss rate. A system is designed to simulate the surface fire. Methods and results are shown for the application of forest fire study.

• Journal of the Korean Society of Safety
• /
• v.23 no.6
• /
• pp.84-90
• /
• 2008

The mass loss rate and heat release rate of puzzle mats were analysed using variable external irradiation level. Five samples of puzzle mat were tested in this study : Type A, B, C, D and E. Type A, B and C are all general grades whereas Type D and E are both Flame retardant grades. Incident heat fluxs of $25kW/m^2$, $35kW/m^2$, $50kW/m^2$ and $70kW/m^2$ were selected for these experiments. All samples were tested in the horizontal orientation and were wrapped in a single layer of aluminum foil. Each sample was nominally 20mm thick and 100mm square. The combustion heat and mass loss rate were carried out from Oxygen bomb calorimeter and mass loss calorimeter according to ISO 5660-1 respectively. Heat release rates were calculated using the equation ${\dot{Q}}=A_f{\dot{m}}"_X{\Delta}H_c=0.75A_f{\dot{m}}"{\Delta}H_c$. where $A_f$ is the horizontal burning area of the sample, $\dot{m}"$ is mass loss rate per unit area, ${\Delta}H_c$ is complete heat of combustion and 0.75 is combustion efficiency.

• YAKHAK HOEJI
• /
• v.29 no.3
• /
• pp.144-151
• /
• 1985

Cathodic stripping voltammetric determination of traces of selenium in plant samples was studied. Stripping peak of selenium (IV) from Cu-Se intermettalic deposit in acidic media containing copper (II) ion is specific, highly sensitive and well defined, is successfully used for the quantitative determination of selenuin down to the level of 1ng/ml. Sample is burnt in a calorimeter bomb under the oxygen pressure of 40atm. and the selenium is absorbed in 0.1M NaOH. After the solution is filtrated, concentrated and acidified with HCl, then passed through a column of cation exchange resin in the $H^{+}$ form(Dowex 50X-8). The column eluate is analyzed for selenium by differential pulse cathodic stripping voltammetric method. Analytical results of selenium for NBS SMR is well agreement with the certified values. Results are given for a series of plant materials.

• Journal of Nutrition and Health
• /
• v.43 no.1
• /
• pp.5-11
• /
• 2010

We conducted comparative study on metabolizable energy content of extracts of angelica keiskei and its byproduct. Total six different groups consisting of five test groups treated with angelica keiskei and one control group were compared. Each of the five test groups were given 30% of one of whole plant, extracts, fermented of extracts, byproduct and extracts plus byproduct, respectively, mixed with AIN93M. After 3 days of adjustment period, all groups were subjected to 4 days of test period during which the amounts of feed intake and excretion were measured everyday. All feces were treated for the prevention of decomposition and changes before its energy content were measured using a bomb calorimeter. The amount of excretion was $4.8\;{\pm}\;0.3\;g$/rat/3 days in control group and 9.9-15.0 g/rat/3 days in the groups were added with extracts of angelica keiskei indicating that the angelica keiskei-treated groups produce 2-3 times more excretion. Metabolic energy of control diet was 4,133.3 kcal. This was found to be 15 to 20% higher compared with the metabolic energy content ranging from 3,117.0 kcal/kg (extracts of angelica keiskei) to 3,259.8 kcal/kg (extracts plus byproducts) angelica keiskei-treated groups. This is interpreted as the result of the decreased metabolic energy in the test diets were substituted with 30% of ngelica keiskei-treated ingredient which has low metabolic content itself. One notable finding is that the metabolic content of the group mixed with byproducts and extracts (1,763.0 kcal/kg) is 27% higher than that of extracts of angelica keiskei (1,286.8 kcal/kg) indicating that mechanical grinding increases the rate of digestion and absorption increasing, in turn, the energy content used in the body. The results of analysis of overall caloric absorption showed absorption rate in order of Whole plant < extracts < byproduct < extract plus byproduct < fermented of extract.

• Fire Science and Engineering
• /
• v.21 no.4
• /
• pp.25-31
• /
• 2007

The combustion characteristics and combustion heat of sandwich panel cores were analysed using variable external irradiation level. The characteristics such as ignition time, critical heat flux, ignition temperature and surface temperature profile were measured. Fuel samples were exposed to incident heat fluxes from 15 to $50\;kW/m^2$. For the measurement of various combustion characteristics, the size of specimen was $100\;mm\;{\times}\;100\;mm\;{\times}\;50\;mm$ and the samples were 3 different kinds. As results, Type B showed the best characteristics in measurement of combustion heat and ignition temperature and Type C showd the best characteristics in critical heat flux and surface temperature profile than that of the other two. In conclusion, we knew that Type C had the best performance in fire safety from all data of this study.