• Journal of the Korean Wood Science and Technology
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• 제44권3호
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• pp.315-322
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• 2016

2개 이상의 보부재 집성재 요소들의 측면접착으로 제작된 "블록접착집성재"는 대단면 목조건축물의 건축부재로 활용 가능한 구조용재다. 블록접착집성재의 측면은 접착제의 종류와 도포량 및 압체압력을 각기 다른 조합으로 접착하여 박리시험과 전단블록시험으로 접착성능을 검토하였다. 실험결과 레조시놀접착제 $500g/m^2$을 도포하고 압체압력 1.5 MPa의 조건으로 제작된 블록접착집성재의 측면접착성능이 가장 양호하였다. 양호한 측면접착조건으로 제작된 블록접착집성재는 동일단면계수의 대조군 집성재와 휨 강도 성능을 비교 검토하였다. 블록접착집성재의 휨 탄성계수는 대조군 집성재와 유사하였으며, 파괴계수는 대조군집성재 보다 27% 향상되었다. 할렬은 대조군집성재 보다 블록접착집성재에서 다량 발생하였으며, 블록접착집성재의 측면접착층에서 계면파괴나 응집파괴는 관찰되지 않았다.

• Restorative Dentistry and Endodontics
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• 제22권1호
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• pp.144-155
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• 1997

This study evaluated shear bond strength between porcelain and resin cement according to various surface treatments of porcelain, and surface condition of debonded porcelain. 50 porcelain specimens(Celay block A2M7) and composite resin specimens(Clearfil Photo-Bright) were prepared, and divided into 5 experimental groups according to the treatment method of porcelain surface. 5 experimental groups by surface treatments were as follows; CONTROL Group : No surface treatment was done on the surface of porcelains. SAND Group : The surface of porcelains were sandblasted with $50{\mu}m$ aluminum oxide for 5 seconds. HF Group: The surface of porcelains were etched with 8% Hydrofluoric acid for 4 minutes. SIL Group: The surface of porcelains were coated with silane coupling agent and heated at $100^{\circ}C$ for 5 minutes. SAND+HF+SIL Group : The surface of porcelains were sandblasted with $50{\mu}m$ aluminum oxide for 5 seconds and etched with 8% Hydrofluoric acid for 4 minutes, and coated with silane coupling agent and heated at $100^{\circ}C$ for 5 minutes. After surface treatments on the prepared porcelain surface two pastes of Panavia 21$^{(R)}$ were mixed, they were applied between composite resin block and porcelain surface, and then excessive resin cements were removed, and its margin was surrounded with Oxyguard II. All specimens were stored for 24 hours in water at $37^{\circ}C$ and tested with Instron testing machine between porcelains and resin cements, and debonded porcelain surfaces were observed under Scanning Electon Microscope(Hitachi S-2300) at 20kvp. The values from each group were compared statistically by Student's t-test. The obtained results were as follows; 1. The shear bond strength without surface treatment of porcelain was the lowest among all experimental groups(p<0.05). 2. The detached porcelain surface with sandblasting alone had more remarkable cracks than with only Hydrofluoric Acid or Silane coupling 2gent, but showed the lowest value of shear bond strength among surface treated groups(p<0.05), 3. When porcelain surface was treated by hydrofluoric acid, it affected shear bond strength more than silane coupling agent, but there were no significant statistical differences(p>0.05). 4. When three methods were combined to increase shear bond strength between porcelains and resin cements, its value was the highest than the others(p<0.05). 5. In Scannig Electron Micrograph of detached porcelain surface with no treatment, the sample revealed adhesive failure between the porcelain and resin cement whereas detached porcelain surface with combination of three method cohesive failure on the porcelain.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 1991년도 가을 학술발표회 논문집
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• pp.107-112
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• 1991

The object of this study is to investigate material characteristics and flexural behavior of high strength concrete. Principal causes of variations of high compressive strength include the strength-producing capabilities of cement and silica hume. Compressive strength of 1200 kgf/$\textrm{cm}^2$ is introduced for identifying the effect of the variation of the size of porocity and alternative method of measurement, Acoustic Emition method, is applied to examine the phenominon of concrete failure. The main test variables in the beam element are tensile steel ratios, presence of shear reinforcement, and change of steel shape. The estimation of stress block in the flexural test of this element tends to support the present theory and may suggest a desirable shape of the stress block.

• The Journal of Advanced Prosthodontics
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• 제12권5호
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• pp.251-258
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• 2020

PURPOSE. The bond strengths between resin denture teeth with various compositions and denture base resins including conventional and CAD/CAM purposed materials were evaluated to find influence of each material. MATERIALS AND METHODS. Cylindrical rods (6.0 mm diameter × 8.0 mm length) prepared from pre-polymerized CAD/CAM denture base resin blocks (PMMA Block-pink; Huge Dental Material, Vipi Block-Pink; Vipi Industria) were bonded to the basal surface of resin teeth from three different companies (VITA MFT^®; VITA Zahnfabrik, Endura Posterio^®; SHOFU Dental, Duracross Physio^®; Nissin Dental Products Inc.) using resin cement (Super-Bond C&B; SUN MEDICAL). As a control group, rods from a conventional heat-polymerizing denture base resin (Vertex™ Rapid Simplified; Vertex-Dental B.V. Co.) were attached to the resin teeth using the conventional flasking and curing method. Furthermore, the effect of air abrasion was studied with the highly cross-linked resin teeth (VITA MFT^®) groups. The shear bond strengths were measured, and then the fractured surfaces were examined to analyze the mode of failure. RESULTS. The shear bond strengths of the conventional heat-polymerizing PMMA denture resin group and the CAD/CAM denture base resin groups were similar. Air abrasion to VITA MFT^® did not improve shear bond strengths. Interfacial failure was the dominant cause of failure for all specimens. CONCLUSION. Shear bond strengths of CAD/CAM denture base materials and resin denture teeth using resin cement are comparable to those of conventional methods.

• 대한치과보철학회지
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• 제45권6호
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• pp.743-752
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• 2007

Statement of problem. The aims of the study were to evaluate the effect of current surface conditioning methods on the bond strength of a resin composite luting cement bonded to ceramic surfaces and to identify the optimum cement type. Material and methods. The sixty zirconia ceramic specimens(10 per group) with EVEREST milling machine and 60 tooth block were made. The zirconia ceramic surface was divided into two groups according to surface treatment: (1) airborne abrasion with $110{\mu}m$ aluminum oxide particles; (2) Rocatec system, tribochemical silica coating. The zirconia ceramic specimens were cemented to tooth block using resin cements. The tested resin cements were Rely X ARC, Panavia F and Superbond C&B. Each specimen was mount in a jig of the universal testing machine for shear strength. The results were subjected to 2-way ANOVA and Post hoc tests was performed using Tukey, Scheffe, and Bonferroni test. Results. The mean value of shear bond strength(MPa) were as follows: $$RelyXARC(+Al_2O_3),5.35{\pm}1.69$$; $$RelyXARC(+Rocatec),8.50{\pm}2.13$$; $$PanaviaF(+Al_2O_3),9.58{\pm}1.13$$; $$PanaviaF(+Rocatec),12.98{\pm}1.71$$; $$SuperbondC&B(+Al_2O_3)8.27{\pm}2.04$$; $$SuperbondC&B(+Rocatec),14.46{\pm}2.39$$. There was a significant increase in the shear bond strength when the ceramic surface was subjected to the tribochemical treatment(Rocatec 3M) in all cement groups(P<0.05). Bonding strengths of cements applied to samples treated with $Al_2O_3$ were compared; Rely X ARC showed the lowest values, whereas Panavia F cement showed higher value than that of Superbond C&B group with no statistical significance. When the bond strength of cements with of Rocatec treatment was compared, Rely X ARC showed lowest values. Overall, it was apparent that tribochemical treated Super-Bond possessed higher mean bond strength (14.46MPa; P<0.05) than that of Panavia F cement group with no significance. Conclusions. Silica coating followed silanization(Rocatec treatment) increase the bond strength between resin cement and zirconia ceramic. Panavia F containing phosphate monomer and Superbond C&B comprised of 4-META tend to bond chemically with zirconia ceramic, thus demonstrating higher bond strength compared to BisGMA resin cement. Superbond C&B has shown to have highest value of bonding strength to zirconia ceramic after Rocatec treatment compared to other cement.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 2004년도 추계 학술발표회 제16권2호
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• pp.409-412
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• 2004

Over last decade extensive researches have been undertaken on the strength behaviour of Fiber Reinforced Concrete(FRC) structures. But the use of Ultra-High Strength Steel Fiber Cementitious Concrete Composites is in its infancy and there is a few experiments, analysis method and design criteria on the structural elements constructed with this new generation material which compressive strength is over 150 MPa and characteristic behaviour on the failure status is ductile. The objective of this paper is to investigate and analyze the behaviour of reinforced rectangular structural members constructed with ultra high performance cementitious composites (UHPCC). This material is known as reactive powder concrete (RPC) mixed with domestic materials and its compressive strength is over 150MP. The variables of test specimens were shear span ratio, reinforcement ratio and fiber quantity. Even if there were no shear stirrups in test specimens, most influential variable to determine the failure mode between shear and flexural action was proved to be shear span ratio. The characteristics of ultra high-strength concrete is basically brittle, but due to the steel fiber reinforcement behaviour of this structure member became ductile after the peak load. As a result of the test, the stress block of compressive zone could be defined. The proposed analytical calculation of internal force capacity based by plastic analysis gave a good prediction for the shear and flexural strength of specimens. The numerical verification of the finite element model which constitutive law developed for Mode I fracture of fiber reinforced concrete correctly captured the overall behaviour of the specimens tested.

• 대한치과보철학회지
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• 제29권1호
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• pp.255-264
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• 1991

The purpose of this study was to evaluate the effect of the shear bond strength between porcelain laminate veneer and enamel according to the surface treatment and thermocycling. Group I, as a control group, was sandblasted only; group II was sandblasted and etched; group III was sandblasted and silane treated; and group IV was sandblasted, etched and silane treated. A porcelain block was placed onto the etched enamel under a 150g static load and the bonded site was light-cured from 4 directions for 1 minute each. The 72 bonded specimens were stored in water at $37^{\circ}C$ for 1 day. Half of each group were thermocycled at $4^{\circ}C$ and $60^{\circ}C$ for 100 cycles with a dwelling time in each bath of 1 min. Following thermocycling, the specimens were installed in an Instron universal testing machine and the shear bond strength was measured. After the specimens were fractured, the fractured surfaces were examined with SEM. The obtained results were as follows : 1. The shear bond strength of the sandblasted and etched and silane treated group(Group IV) was the strongest of all, and the shear bond strengths between the sandblasted group(Group I) and the sandblasted and silane treated group(Group III) were not statistically different(p>0.05). 2. When the shear bond strength was measured after thermocycling, only the sandblasted, etched and silane treated group(Group IV) was statistically different(p<0.05). 3. The scanning electron microscopic views of the fractured surfaces show more irregularities and more resin fragments in the etched group than in the unetched group. 4. The scanning electron microscopic views of the fractured surfaces show a more delicate surface after thermocycling and after silane treatment than before thermocycling and before silane treatment.

• Journal of the Korean Wood Science and Technology
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• 제41권2호
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• pp.158-163
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• 2013

Cross laminated timber (CLT) has been an rising issue as a promising building material replacing steel-concrete in mid story rise construction. But, there was no specific standard for CLT because it had been developed in industrial section. Recently, new draft for requirements of CLT was proposed by EN which suggested to evaluate the performance of adhesive in CLT by the same method as glulam. But, it has been reported that shear performance of cross laminated timber is governed by rolling shear. Therefore, block shear tests were carried out to compare parallel to grain laminating and cross laminating using commercial one component PUR (Poly urethane resin). The result showed that the current glulam standard for evaluating bonding performance is not appropriate for CLT. Beacause shear strength of cross laminating decreased to 1/3 of parallel to grain laminating and this strength was representing shear performance of wood itself not the bond. However, cross laminating showed no significant effect on wood failure. Thus, wood failure can be used as a requirement of CLT bonding. Based on the results, cross laminating effect should be included when evaluating adhesive performance of CLT correctly and should be considered as an important factor.

• Steel and Composite Structures
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• 제27권5호
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• pp.537-543
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• 2018

Mechanical shear connectors are commonly used to transfer longitudinal shear forces across the steel-concrete interface in composite beams. Steel pipe as a new shear connector is proposed in this research and its performance to achieve composite strength is investigated. Experimental monotonic push-out tests were carried out for this connector. Then, a nonlinear finite element model of the push-out specimens is developed and verified against test results. Further, the finite element model is used to investigate the effects of pipe thickness, length and diameter on the shear strength of the connectors. The ultimate strengths of these connectors are reported and their respective failure modes are discussed. This paper comprises of the push-out tests of ten specimens on this shear connector in both the vertical and horizontal positions in different reinforced concretes. The results of experimental tests are given as load-deformation plots. It is concluded that the use of these connectors is very effective and economical in the medium shear demand range of 150-350 KN. The dominant failure modes observed were either failure of concrete block (crushing and splitting) or shear failure of pipe connector. It is shown that the horizontal pipe is not as effective as vertical pipe shear connector and is not recommended for practical use. It is shown that pipe connectors are more effective in transferring shear forces than channel and stud connectors. Moreover, based on the parametric study, a formula is presented to predict the pipe shear connectors' capacity.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 2005년도 추계 학술발표회 제17권2호
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• pp.57-60
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• 2005

The objective of this paper is to investigate and analyze the behaviour of prestressed I section structural members constructed with ultra high perfomance steel fiber reinforced cementitious concrete (SFR-UHPC). This material is known as reactive powder concrete (RPC) mixed with domestic materials and its compressive strength is over 150MP. The parameters of test specimens were span to depth ratio, prestressing force, prestressing wire placement and web width. Most influential parameter to determine the failure mode between shear and flexural action was proved to be shear span ratio. The characteristics of ultra high-strength concrete is basically brittle, but due to the steel fiber reinforcement behaviour of this structure member became ductile after the peak load. As a result of the test, the stress block of compressive zone should be redefined. The proposed analytical calculation of internal force capacity based by plastic analysis gave a good prediction for the shear and flexural strength of specimens. The numerical verification of the finite element model which constitutive law developed for Mode I fracture of fiber reinforced concrete correctly captured the overall behaviour of the specimens tested.