• Title/Summary/Keyword: Bath Dipping time

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A Study on the Erosion Behavior of the Ceramic Sprayed Coating Layer in the Molten 55% Al-Zn (용융 55%Al-Zn 중에서 세라믹 용사 피막의 침식 거동에 관한 연구)

  • 강태영;임병문;최장현;김영식
    • Journal of Welding and Joining
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    • v.18 no.3
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    • pp.51-59
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    • 2000
  • Sink roll has been used in molten 55%Al-Zn alloy bath of continuous galvanizing line for sinking and stabilizing working steel strip in molten metal bath. In the process, the sink roll body inevitably build up dross compounds and pitting on the sink roll surface during 55%Al-Zn alloy coated strip production, and the life time of the sink roll is shorten by build up dross compounds and pitting. The present study examined the application of thermally sprayed ceramic coatings method on sink roll body for improving erosion resistance at molten 55% Al-Zn pool. In this experiment, the stainless steels such as STS 316L and STS 430F were used as the substrate materials. The CoNiCr and WE-Co powder were selected as bond coating materials. Moreover $Al_2O_3-ZrO_2-SiO_2 and ZrO_2-SiO_2$ powders selected as the top coating materials. Appearances of the specimens before and after dipping to molten 55%Al-Zn pool were compared and analyzed. As a result of this study, STS430F of substrate, WC-Co of bond spray coatings, $ZrO_2-SiO_2$ power of top spray coatings is the best quality in erosion resistance test at molten 55%Al-Zn pool

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A Study on the Preparation of Poly(vinyl alcohol) Polarizing Film (폴리비닐알코올 편광필름 제조에 관한 연구)

  • 김삼수;우화령;류원석
    • Textile Coloration and Finishing
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    • v.16 no.4
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    • pp.19-25
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    • 2004
  • Both poly(vinyl alcohol)$(PVA)-I_2$ and PVA-dye polarizing film were prepared using PVA with number-average degree of polymerization of 1,700, 2,300, 2,600. The optical property of used dye in this study closed to the that of iodine. The PVA-dye polarizing film was prepared through the dyeing process. In comparison of the result of the measurement of the heat and humidity resistance of two types polarizing films, it of PVA-dye polarizing film was higher than that of a conventional $PVA-I_2$polarizing film. The transmittance and the polarization efficiency of PVA-dye polarizing film was significantly influenced by dye concentration, dipping time, salt concentration, and temperature of dye bath. The PVA-dye polarizing film exhibited a high polarization efficiency of 99.3% and a good transmittance of 42.4%.

Charactristice of a colored Galvanized Coating using Ti-Zn Alloy System (Zn-Ti계용융아연 도금강판의 착색화 특성)

  • 전선호
    • Journal of the Korean institute of surface engineering
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    • v.30 no.5
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    • pp.320-332
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    • 1997
  • The development of colored surface on zinc coating by the oxidation of a melten alloy of zinc with a minor amount of oxygen-avid additive such as tianium has been studied. Using a galvanizing Zinc alloy containing 0.1 to 0.3wt%Ti, gold, purple or blue color was developed clearly and stably, depending upon the extent of oxidation, by air cooling after hot dipping in a bath at temperature of $550^{\circ}C$ to $600^{\circ}C$. The source of the color is light interference with surface oxide layer. THe final color depends on the thickness of the color depends on the thickness of $TiO_2$, played So compositing, temperature and time at elevated temperature after are all controlling variables. Since oxidation film such as $TiO_2$ played role of passivation film, the corrosion resistance in a colored galvanized steel sheet. It is also thought that surface oxide layer of $TiO_2$ inhibited dissolution of the coating layer.

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Establishment of Washing Conditions for Salad to Reduce the Microbial Hazard (샐러드의 미생물학적 위해 감소를 위한 세척 조건 확립)

  • Kim, Jeong-Weon;Kim, Soo-Hee
    • Korean journal of food and cookery science
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    • v.21 no.5
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    • pp.703-708
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    • 2005
  • The purposes of this study were to establish washing conditions for vegetable salad to reduce the microbial hazard by using sodium hypochlorite solution and eventually to implement HACCP for salad processing. By using the salad production line of Shinkeum Co. located in Gwacheon, Gyunggi-do, salad samples were washed under several washing conditions (chlorine dip period, chlorine concentration, rinse time, etc.) to determine the most effective conditions. The original washing line consisted of 3 baths (100 ppm chlorine water dip, water rinse, and water rinse), each with a capacity of 100 L of tap water and 5 kg of salad. First, the salad samples were washed with 100 ppm of sodium hypochlorite solution for various dip times (3, 6, 9, 12 min); however, only a 1 log- or less-reduction in total microbial counts was achieved in all groups and the time of chlorine water dip was not a significant factor in reducing the microbial hazard. When another water bath was added before the chlorine water dip (4-bath washing), a 2 log-reduction in total microbial counts was achieved. This result suggested the importance of pre-dipping salad materials in water before chlorine treatment to reduce the organic load on the surface of the vegetables. Coliforms were not detected at all after washing. As the concentration of chlorine $(50{\sim}150\;ppm)$ and rinse time $(0.5{\sim}2\;min)$ increased, greater microbial reduction was achieved; however, physical damage of the salad was observed. Finally, the optimum washing conditions for salad were determined as 3 min-water dip, 3 min-chlorine (100 ppm) dip, 2 min-rinse, and 2 min-rinse.

Effects of Processing Conditions and Natural Antimicrobial Materials on Quality of Freeze-dried, Seasoned and Roasted Alaska Pollack (Theragra chalcogramma) (가공조건과 천연항균제의 처리가 황태양념구이의 품질에 미치는 영향)

  • CHO Soon-Yeong;SHIM Jae-Man;CHOI Yong-Seok;KIM Ok-Sun
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.36 no.5
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    • pp.437-441
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    • 2003
  • This research investigated the effects of processing conditions and natural antimicrobial materials on quality of freeze-dried, seasoned and roasted Alaska pollack (Theragra chalcogramma). The optimum dipping time and moisture contents of freeze-dried Alaska pollack were 1 sec in $1\%$ salt solution, $48.6\%$ respectively. The freeze-dried, seasoned and roasted Alaska pollack product showed high sensory value. As sterilization time increased over 30 mins in water bath at $100^{\circ}C$ the browning degree of the freeze-dried, seasoned and roasted Alaska pollack product increased. Among various antibrowning agents, $3\%$ corn starch was better in preventing browning than sporix treatment. The freeze-dried, seasoned and roasted Alaska pollack product added with lactate Ca and catechin had the antimicrobial, and the VBN contents of the product showed low level.

Dyeability of Silk Fabrics Using Extracts of Ligustrum Japonicum Thunb Fruit (광나무 열매 추출물을 이용한 견직물의 염색성)

  • Lee, Hye-Sun;Ko, Sung-Mi
    • Textile Coloration and Finishing
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    • v.22 no.1
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    • pp.71-76
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    • 2010
  • In this study the optimum dyeing conditions and blocking effect of UV deodorization efficiency of Ligustrum japonicum Thunb were investigated. Colorants were water-extracted from Ligustrum japonicum Thunb fruit and freeze-drided to obtain colorants powder. The effects of dye concentration, dyeing temperature, dyeing time, and the number of dipping count were studied. Fastness to dry cleaning, rubbing, perspiration, and light were measured according to KS K 0644, KS K 0650, KS K 0715 and KS K 0700, respectively. In order to examine the dyeability according to dyeing conditions, reflectance of fabrics were measured by using UV/VIS spectrophotometer. The bath ratio was 1:20. Dyeing concentration was 100, 200, 300, 400 and 500% on the weight of fiber. Dyeing time was 20, 40, 60, and 80 minutes. Dyeing temperature was 20, 40, 60, 80, and $100^{\circ}C$. The infrared high pressure dying machine was used. As dyeing concentration increased, dye adsorption increased up to 400% and it slowed down. Dye uptake was increased with raising themperature up to $80^{\circ}C$ and it slowed down. Dye adsorption occurred rapidly at first 20 minutes and then it slowed down and reached almost maximum dye uptake at 60 min. Dye uptake increased by repeated dyeing. Therefore, it is considered that optimum dyeing condition is 400%(o.w.f.), $80^{\circ}C$, 60 min. And repeated dyeing improves dye uptake. Color fastness to dry cleaning and rubbing was good, but light fastness and perspiration fastness was not good. Blocking effect of ultraviolet radiation and deodorization efficiency was good.

An Electrochemical Study on the Corrosion Resistance Improvement of Galvanizing Steel by Dipping to Solution with Inhibitor (인히비터 첨가용액의 침지에 의한 용융아연도금 강판의 내식성 개선에 관한 전기화학적 연구)

  • Moon, Kyung-Man;Cho, Hwang-Rae;Kang, Tae-Young;Lee, Myung-Hoon;Kim, Yun-Hae
    • Journal of Advanced Marine Engineering and Technology
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    • v.31 no.2
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    • pp.173-181
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    • 2007
  • Recently, galvanizing method is predominantly being used not only a economical point of view but also due to it s stability and long life. For example, guard rail of high way, all kinds of structures for ship etc. were protected with galvanizing and demand of galvanized structural materials was being increased with more and more. However, galvanized structures were inevitably being deteriorated with time eventually because they were corroded with solution of galvanizing film and exfoliation of it s film in the present severe corrosive environment. Therefore, it is necessary to improve the corrosion resistance of the galvanizing film through various methods such as variation of chemical composition of galvanizing bath, chromate treatment and coating treatment. In this study, three test specimens such as pure galvanizing, galvarium, and chromate treatment were submerged at tap water with inhibitor addition. And the effect of their corrosion resistance improvement was comparatively investigated with electrochemical method. Corrosion current density of the galvanized steel was the largest among three specimens, however, the galvarium steel showed the lowest corrosion current density. Futhermore, these three kinds of test specimens indicated considerably excellent corrosion resistance by dipped at tap water with inhibitor addition. Especially, the galvanized steel showed the best effect of corrosion resistance improvement than other test specimens.

Dye Adsorption Ability of Chitin in Reactive Dyebath (반응염료염액에서의 키틴의 염료흡착성능)

  • 유혜자;김정희;이혜자;이전숙
    • Journal of the Korean Society of Clothing and Textiles
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    • v.26 no.2
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    • pp.349-354
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    • 2002
  • In order to decolorize the reactive dye wastewater, we investigated the dye-adsorption ability of chitin, which was natural polymer obtained from shrimp shell. Chitin particle(less than 250 ${\mu}{\textrm}{m}$n) was prepared from shrimp shells in the processes of decalcification in aqueous hydrochloric acid solution and deproteination in aqueous sodium hydroxide solution. The particle size of chitin was controlled to less than 250 ${\mu}{\textrm}{m}$. Three tripes of the reactive dyes-C.I. Reactive Red 120, C.I. Reactive red 241 and C.I. Reactive Black 5-were used. Dye adsorption ability of chitin was investigated by dipping the particle in the dyebaths of concentration of 0.0l%, 0.03% and 0.05% for various periods of time(1,3,5, 10,20,40,80,160minutes). The influence of addition of salt(Na$_2$SO$_4$) and alkali to the dyebaths on dye-absorption was also investigated. We obtained the following results fur the dye-absolution ability of chitin in the dyebaths of three types of reactive dyes. 1) The amount of dye uptake by chitin was increased by addition of salt to the dyebaths. 2) As the concentration of alkali became higher than 3g/I, the amount of dye uptake by chitin was increased. Chitin showed good dye-adsorption ability, when the alkali concentration was high. 3) Chitin showed equal dye uptake in the three types of dyebaths when the dye concentration was 0.0l%. Over 90% of dyestuffs was adsorbed from the dyebaths in ten minutes. When the dye concentration was higher, better adsorption ability was showed in a dye bath of Reactive black 5 than in the others. When the dye concentration was 0.03%, 90% of Reactive red 120 and Reactive red 241 was adsorbed in 40 minutes and the same of Reactive black 5 in 10 minutes. When the dye concentration was 0.05%, 9()% of Reactive red 120 was adsorbed in 80 minutes, and Reactive black 5 in to minutes.

Residue level and pharmacokinetics of trichlorfon in the Japanese eel (Anguilla japonica) after bath treatment (Trichlorfon (TCF)의 약욕 투여에 따른 뱀장어 체내 약물 잔류량 및 약물동태학 연구)

  • Jo, Hyun Ho;Chung, Joon Ki
    • Journal of fish pathology
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    • v.35 no.1
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    • pp.93-102
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    • 2022
  • This study performed a trichlorfon (TCF) residue and pharmacokinetic analysis with Japanese eels, Anguilla japonica, to obtain baseline data to establish the maximum residue level (MRL) of TCF in A. japonica. After dipping A. japonica in 30 ppm and 150 ppm of TCF at 28℃ and 18℃, drug residue in the body was analyzed with LC-MS/MS, and these results were further analyzed with the PK solver program to obtain the pharmacokinetic parameters of TCF in the serum, muscles, and liver. The maximum concentrations (Cmax) in the serum, muscles, and liver were 25.87-357.42, 129.91-1043.73, and 40.47-375.20, respectively, and the time to maximum concentration (Tmax) was 0.13-1.32h, 1.17-3.34h, and 0.14-5.40h, respectively. The terminal elimination half-life (T1/2) was 2.13-3.92h, 5.30-10.35h, and 0.65-13.81h, respectively. In the 30 mg/L concentration group, TCF was not detected in the serum of eels 96 hours after bathing, and was below the detection limit after 336 hours in muscle and liver. On the other hand, in the 150 mg/L concentration group, TCF was not detected in the serum of eels 336 hours after bathing, but was detected in muscle and liver at 336 hours. In conclusion, the results of this study would be useful in establishing the MRL of TCF in farmed A. japonica.