• Proceedings of the PSK Conference
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• 2002.04a
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• pp.200.1-200.1
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• 2002

• Analytical Science and Technology
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• v.15 no.4
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• pp.1039-1050
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• 2002

• Analytical Science and Technology
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• v.17 no.6
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• pp.1043-1058
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• 2004

• Analytical Science and Technology
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• v.13 no.5
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• pp.666-674
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• 2000

The present study describes an analytical method for the determination of polybrominated biphenyls (PBBs) in biota samples by gas chromatography-mass spectrometry (GC/MS). PBBs are extracted twice from 20 g samples with mixture solvent 40mL acetone and 80mL hexane using ultrasonic agitation for 20 min. Lipids in extracts are degraded by concentrated sulfuric acid and then PBBs are purified with Florisil column. The purified extracts are analyzed by GC/MS-selected ion monitoring mode for the quantitation of PBBs in biota sample. The overall recovery yields of PBBs range between 77 and 111% under these experimental conditions.

• Journal of the Korean Society for Nondestructive Testing
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• v.35 no.3
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• pp.206-214
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• 2015

In this study, low-velocity impact damage (LVID) in glass fiber reinforced plastic (GFRP) was investigated using pulse thermography (PT) and lock-in thermography (LIT) techniques. The main objective of this study was to evaluate the detection performance of each technique for LVID in GFRP. Unidirectional and cross-ply GFRPs were prepared with four energy levels using a drop weight impact machine and they were inspected from the impact side, which may be common in actual service conditions. When the impacted side was used for both inspection and thermal loading, results showed that the suggested techniques were able to identify the LVID which is barely visible to the naked eye. However, they also include limitations that depend on the GFRP thickness at the location of the delamination produced by the lowest impact energy of five joule.

• Journal of the Korean Society for Precision Engineering
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• v.33 no.11
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• pp.905-910
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• 2016

Infrared (IR) optic lens can be fabricated by a single point diamond turning (SPDT) machine without subsequent polishing process. However, this machining process often leaves micro-cracks that deteriorate the surface quality. In this work, we propose an experimental design to remove micro-cracks on IR lens. The proposed design gathered data between cutting process condition and Rt surface roughness. This is of great importance because the scale of micro-cracks is a few micrometer. Rt surface roughness is suitable for analyzing maximum peak height signals of the profile. The experimental results indicate that feed per revolution variable is one of the most dominant variable, affecting the generation micro-cracks on IR lens surfaces.

• Analytical Science and Technology
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• v.13 no.4
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• pp.484-493
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• 2000

The simultaneous analysis of alkylphenols, chlorophenols and bisphenol A in biota samples was performed by gas chromatography-mass spectrometry-selected ion monitoring mode. The phenols were extracted from sample with organic solvent and Forisil and Silica columns for clean-up procedure were compared. Recovery studies were performed at 1-ppm level of phenols added to each biota sample. Their recoveries ranged between 83 and 116% with coefficient of variations of 2.4-11.9%. To improve the detection limits of phenols, trimethylsilyl (TMS) derivatization was applied. The gas chromatographic properties of free phenols and TMS derivatized phenols were also investigated.

• Analytical Science and Technology
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• v.8 no.4
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• pp.623-630
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• 1995

Silicone rubber-based sodium-selective membranes are developed for solid-state ion sensors. It was shown that the potetiometric performance of SR-based membranes are greatly dependent on the type of neutral carriers employed; among the three ionophores, N,N,N',N'-tetracyclohexyl-1,2-phenylenedioxydiacetamide (ETH 2120), bis[(12-crown-4)methyl]dodecylmethylmalonate (D12C4DMM) and monensin methyl ester (MME), examined, only ETH 2120 was compatible with the SR-based matrix. Addition of about 20 wt% plasticizer to the SR-based matrix provided the resulting membranes with potentiometric properties essentially equivalent to those of the corresponding PVC-based membranes. Owing to the strong adhesive strength of SR-based membranes, the CWEs coated \vith those membranes exhibited long lifetime with conventional electrode-like performance. Blending of PU into the SR matrix increased the lifetime of CWEs from two weeks to one month.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.20 no.5
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• pp.322-333
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• 2019

The purpose of the current study was to investigate the level of market size and market share of domestic research equipments for analyzing the difference of the number and amount of construction by the manufacturing countries in the basic and analytical science fields based on the information of the research equipment invested by the Korean government for the past 14 years. As of January 1 2019, from 2005 to 2018, 20,687 research facilities & equipments (main equipment with a construction cost of 30 million won or more) built in the basic and analytical science fields were selected for this study and their components, standard classification, number of construction, and amount of construction by country of manufacture were analyzed. Differences of the number and amount of construction among manufacturing countries were tested using a single sample chi-square test and one-way analysis of variance, followed by Bonferroni's post-hoc test. As a result of this study, the number of construction (p<.001) and construction amount (p<.05) were statistically different for each manufacturing country. The level of market size and market share was significantly different according to the equipment standard classification (p<.05). Therefore, differentiated strategies of the government and policy research projects will be required for each type of equipment and amount in order to support the policy for the localization of research equipment.

• Proceedings of the Petrological Society of Korea Conference
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• 1998.09a
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• pp.39-39
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• 1998