• Journal of the Korean Physical Society
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• v.73 no.9
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• pp.1340-1345
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• 2018

Mo-10 at.% Cu nanocomposite powders were fabricated by using planetary ball-milling (PBM), a mechanical alloying technique for preparing nanocomposite alloy powders of metals with mutual insolubility, and the variations in the physical and the chemical characteristics with the process conditions were investigated. We observed that Mo-10 at.% Cu was an appropriate composition to ensure a good alloying grade and minimal welding between particles. The influences of the temperature and the milling conditions on the mechanical alloying process and the phase change of Mo-10 at.% Cu composite powders were investigated, and the particle and the grain sizes of the powders after mechanical alloying were confirmed. The Mo-10 at.% Cu powders showed homogeneous elemental distributions and no phase changes up to $1200^{\circ}C$; their compositions were retained after the mechanical alloying process. The finest grain size obtained was about 5 nm for powders processed using optimum PBM processing conditions: ball-to-powder weight ratio of 5 : 1, ambient air atmosphere, a milling time of 20 h, a rotation speed of 200 rpm, and a stearic acid content of 4 wt.% produced superfine-grained Mo-10 at.% Cu nanocomposite powders with an average grain size of 5 nm (which is smaller than that of other similar materials reported in the literature). The analytical results confirmed that the PBM technique presented here is a promising method for preparing superfine-grained Mo-10 at.% Cu powders with improved properties.

• Korean Journal of Materials Research
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• v.28 no.3
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• pp.148-158
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• 2018

This study investigated the effect of the grinding media of a ball mill under various conditions on the raw material of copper powder during the milling process with a simulation of the discrete element method. Using the simulation of the three-dimensional motion of the grinding media in the stirred ball mill, we researched the grinding mechanism to calculate the force, kinetic energy, and medium velocity of the grinding media. The grinding behavior of the copper powder was investigated by scanning electron microscopy. We found that the particle size increased with an increasing rotation speed and milling time, and the particle morphology of the copper powder became more of a plate type. Nevertheless, the particle morphology slightly depended on the different grinding media of the ball mill. Moreover, the simulation results showed that rotation speed and ball size increased with the force and energy.

• Journal of the Korean Magnetics Society
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• v.24 no.1
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• pp.1-10
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• 2014

$Co_2Z$-type barium ferrites ($Ba_3Co_2Fe_{24}O_{41}$) were synthesized using variation method. First, M-type, $Co_2Y$-type and $Co_2Z$-type synthesized by hydrothermal method. Second, M- and Y-type precursors for synthesis of $Co_2Z$ hexaferrite by hydrothermal and ball milling method. the morphology, structure and magnetic properties of the barium ferrite particles were characterized using XRD, FESEM, VSM, impedance. As a result, Single phase of M-type and $Co_2Y$-type were obtained. Manufactured powders of M+Y ball milling, M+Y hydrothermal were similar to single phase of $Co_2Z$-type hexaferrite, all powders were obtained theoretical magnetization (50 emu/g). The largest initial permeability were obtained $Co_2Z$ hexaferrite synthesized by reagent precusor, With increasing calcination temperature was lowered the initial permeability. In another synthesis didn't almost that little change could be found.

• Korean Journal of Materials Research
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• v.26 no.11
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• pp.611-622
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• 2016

Particle morphology change and different experimental condition analysis during composite fabrication process by traditional ball milling with discrete element method (DEM) simulation were investigated. A simulation of the three dimensional motion of balls in a traditional ball mill for research on the grinding mechanism was carried out by DEM simulation. We studied the motion of the balls, the ball behavior energy and velocity; the forces acting on the balls were calculated using traditional ball milling as simulated by DEM. The effect of the operational variables such as the rotational speed, ball material and size on the flow velocity, collision force and total impact energy were analyzed. The results showed that increased rotation speed with interaction impact energy between balls and balls, balls and pots and walls and balls. The rotation speed increases with an increase of the impact energy. Experiments were conducted to quantify the grinding performance under the same conditions. Furthermore, the results showed that ball motion affects the particle morphology, which changed from irregular type to plate type with increasing rotation speed. The evolution was also found to depend on the impact energy increase of the grinding media. These findings are useful to understand and optimize the particle motion and grinding behavior of traditional ball mills.

• Transactions of the Korean Society of Machine Tool Engineers
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• v.14 no.3
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• pp.8-15
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• 2005

A new measuring method for tool deflection has been developed when sculptured surface is processed in ball-end milling. Since the vibration due to cutting forces has low frequencies, an electromagnetic sensor is used for measuring the exact vibration displacement. The amplitude and direction of vibration displacement during the cutting process is presented as orbital plot. In this study, it assumes that the vibration displacement is proportional to the length of cutting chip. Therefore, tool deflection is calculated by summing up the vibration displacement of unit chip length for engaged chip length. In addition, computer programs has been developed to predict the deflection of tools when machining sculptured surface. This developed program predicts the tool deflection per block of NC data, so that it can easily identify the parts which have the possibility of machining errors.

• Journal of the Korean Society for Precision Engineering
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• v.23 no.3 s.180
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• pp.171-178
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• 2006

The sonication mettled is widely used with surfactants to suspend individual single-walled carbon nanotubes in solution, and it is well known that sonication-induced tube cutting occurs. Recently, it is found out that ultrasonicated nanotubes yield simultaneous separation by tube length and diameter. Nanotubes that have been cut shortest possess the greatest enrichments of large-diameter species. In this study, single-walled carbon nanotubes are cut using a ball milling method. Similar fracture behavior is observed fur the ball milled nanotubes: i.e., large diameter tubes are cut shorter. The ability to separate carbon nanotubes by diameter and length will contribute to tile development of nanotube-based applications.

• Proceedings of the KSME Conference
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• 2003.04a
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• pp.1148-1153
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• 2003

An adequate method for the prediction of machining errors is essential to improve productivity and product quality. But it is known that there is a remarkable difference between values calculated by conventional roughness model and measured values of actual machined surfaces under high efficient cutting condition. This paper introduces the theoretical analysis of characteristic lines of cut remainder to evaluate a geometrical surface roughness accurately. In this study, analytic equations of the characteristic lines are derived from the surface generation mechanism of ball end milling considering the actual trochoidal trajectories of cutting edges. The predicted results are compared with the results of conventional roughness model.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 1996.04a
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• pp.125-129
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• 1996

In this study, a method is proposed for the cutting force prediction of Ball-end milling process using Z-map is proposed. Any types of cutting area generated from previous cutting process can be expressed in z-map data. Cutting edge of a ball-end mill is divided into a set of finite cutting edges and the position of this edge is projected to the cross-section plane normal to the Z-axis. Comparing this projected position with Z-map data of cutting area and determining whether it is in the cutting region, total cutting force can be calculated by means of numerical integration. A series of experiments such as side cutting and upward/downard cutting was performet to verify the simulated cutting force.

• Journal of the Korean Society for Precision Engineering
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• v.17 no.1
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• pp.171-178
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• 2000

In this study, an indirect method to estimate the setup runout of a ball-end mill from cutting force signal is proposed. This runout makes cutting forces of each tooth of the milling cutter unequal. By transforming the cutting force model from time domain to frequency domain through time-convolution theorem, the magnitude and phase angle of runout can be explicitly expressed with material constants, cutting conditions, and force signal. The static setup runout can be obtained by extrapolating estimated effective runout, which is independent of feedrate but decreases linearly with increase in axial depth of cut. The setup runout estimated by slot cutting experiments, shows good agreement with the measured one.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.29 no.8
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• pp.516-521
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• 2016

Mo-Cu alloys have been widely used for heat sink materials, vacuum technology, automobile, and many other applications due to their excellent physical and electric properties. Especially, Mo-Cu composites with 5 ~ 20 wt.% copper are widely used for the heavy duty service contacts due to their excellent properties like low coefficient of thermal expansion, wear resistance, high temperature strength, and prominent electrical and thermal conductivity. In most of the applications, highly-dense Mo-Cu materials with homogeneous microstructure are required for better performance. In this study, Mo-Cu alloys were prepared by PBM (planetary ball milling) and SPS (spark plasma sintering). The effect of Cu with contents of 5~20 wt.% on the microstructure and thermal properties of Mo-Cu alloys was investigated.