• Title/Summary/Keyword: BET monolayer moisture content

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Studies on Stability for the Quality of Ginseng Products -3. Determination of Sorption Properties and Optimum Moisture Contents in Extract, Extract Powder and Extract Tea of Red Ginseng- (인삼제품(人蔘製品)의 품질안정성(品質安定性)에 관한 연구(硏究) -3. 홍삼정(紅蔘精), 정분(精粉) 및 정차(精茶)의 흡습특성(吸濕特性)과 적정수분함량(適正水分含量) 기준설정(基準設定)-)

  • Choi, Jin-Ho;Byun, Dae-Seok;Park, Kil-Dang;Kim, Mu-Nam
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.13 no.2
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    • pp.215-221
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    • 1984
  • To investigate stability for the quality of selected ginseng products, their sorption properties were clarified in red ginseng extract(RGEP), and red ginseng extract powder(RGEP), and red ginseng extract tea(RGET). Simultaneously, the BET monolayer value of each product was determined in order to inquire out the possibility of establishment as a criterion for the optimum moisture content of the ginseng products. Based on the BET monolayer moisture level of spray dried RGEP which ranged from 4.08 to 4.65%, it would be desirable to establish the optimum moisture content of the products at 4.4${\pm}$0.3%. This is 1.3 to 1.9% lower than the criter on, "less than 6.0%". The optimum moisture level for RGET of which monolayer value ranged 0.93 to 1.37% would be 1.2${\pm}$0.17%. In this case, the maximum permissible limit of moisture content could presumably be raised up to 1.37% in place of current criterion, "less than l.2%". From the results of a study on the growth of molds, the optimum moisture content for RGE assumed to be extended up to 40.0${\pm}$1.07 despite 36.0${\pm}$1.0% of the present criterion. On the other hand, a storage study under the maltreated condition, $48{\pm}2^{\circ}C$ 75%RH, was also carried out in order to make it clear whether the BET monolayer values were able to be used as indices for optimum moisture level of the products. In all samples tested adsorption occurred at even higher levels of moisture than the monolayer values. However, since there are many other possible factors affecting the quality of products the optimum moisture content is preferable to be reduced to the monolayer value. As a result, it was proved that the optimum level of moisture for both RGEP and RGET could be established by the monolayer values.

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Study on the Drying Characteristics of Wild Vegetables (산채의 건조 특성에 관한 연구)

  • Rhim, Jong-Whan;Hwang, Keum-Taek
    • Korean Journal of Food Science and Technology
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    • v.27 no.3
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    • pp.358-364
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    • 1995
  • In order to determine the moisture content level for safe storage of wild vegetables, drying characteristics and water vapor sorption characteristics of four vegetables, i.e., zucchini slice, sweet potato stem, taro stem, and platycodon, were investigated. The drying curves of these vegetables were consisted of three characteristic stages which were the initial settling down period, the constant drying rate period, and the falling drying rate period. And the falling rate period of the vegetables showed 2 or 3 parts of falling rate. All of the falling rate curves of the vegetables showed upwardly convex shape which is known as a characteristic pattern for the drying of fibrous food materials. The critical moisture contents of the vegetables were $8.29{\sim}9.75,\;10.40{\sim}15.08,\;9.51{\sim}14.52\;and\;3.29{\sim}3.56g\;H_2O/g$ dry solids for zucchini slice, sweet potato stem, taro stem, and platycodon, respectively. Activation energy values of drying rate during falling rate period were 2.30, 2.11, 4.97, and 2.80 kcal/mol for zucchini slice, sweet potato stem, taro stem, and platycodon respectively. The BET monolayer moisture contents of the vegetables were $10.05{\sim}13.59,\;9.49{\sim}12.69,\;9.50{\sim}16.48\;and\;5.01{\sim}5.44g\;H_2O/g$ dry solids for zucchini slice, sweet potato stem, taro stem, and platycodon, respectively. And these values were found to be very compatible with the values of the critical moisture content. Consequently, it was found that the moisture of these vegetables should be removed below the BET monolayer moisture content or below the critical moisture content for the long term storage.

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Moisture Sorption Characteristics and a Prediction Model of Anchovy Powder with Particle Size (입자크기에 따른 분말멸치의 흡습특성 및 예측모델)

  • Youn, Kwang-Sup
    • Food Science and Preservation
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    • v.17 no.4
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    • pp.513-518
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    • 2010
  • This study was carried out to estimate the moisture sorption characteristics and prediction model of anchovy powders with different particle size as above 80 mesh, 80-60 mesh and 40-60 mesh. The equilibrium moisture content had higher values at lower storage temperatures, and higher water activity. The monolayer moisture content calculated using the GAB equation showed a higher level of significance than that of BET equation. The estimated monolayer moisture content was 0.024-0.052 g $H_2O/g$ dry solid. The absorption enthalpy was calculated with different particle size and various water activities. It showed that the absorption energy was decreased with increasing water activity but no difference was found on particle size increasement. The fitness of the isotherm curve was shown to be in the order of Khun, Halsey, Caurie and Oswin model. The prediction model equations for the moisture content were established by ln(time), water activity, and temperature, respectively. The model equation will be helpful for future work on drying and storage of anchovy powder.

Processing Conditions of Expanded Anchovy Snack and Monolayer Moisture Content of the Products (멸치 팽화스낵의 제조조건과 제품의 단분자층 수분함량)

  • Jo, Jin-Ho;Oh, Se-Wook;Lee, Nam-Hyouck;Do, Jeong-Ryong
    • Korean Journal of Food Science and Technology
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    • v.31 no.2
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    • pp.380-384
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    • 1999
  • For the effective utilization of anchovy as a food source, processing conditions of expanded anchovy snack and monolayer moisture content of the products were investigated. Ground anchovy was mixed with 50% of wheat flour, 2.5% of NaCl and 3.0% of onion. The mixture were rolled, cut, dried and finally deep-fried with soybean oil. When 50% of wheat flour was mixed with ground anchovy, expansion rate showed the highest value among the treatments and organoleptic quality of the product was also high. Dried base with 6.4% of moisture content showed the maximum expansion rate and good crispness and brittleness when fried at $200^{\circ}C$. Monolayer moisture content of the expanded products was calculated as 2.77% by BET equation.

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Absorption Characteristics of Persimmon Powder Depending on Temperature Changes and Drying Methods (건조방법과 온도변화에 따른 감 분말의 흡습특성)

  • 이원영;김종국
    • Journal of the East Asian Society of Dietary Life
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    • v.11 no.6
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    • pp.479-484
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    • 2001
  • The absorption characteristics of persimmon powder related to different drying methods and various storage temperatures was investigated. The physical properties of persimmon powder by different drying methods displayed the largest amount of porosity in the freeze-dried sample, and the smallest in hot air dried sample. Equilibrium moisture was reached in 6 days. Monolayer moisture contents were predicted to 0.09687~0.19712(freeze drying), 0.07820~0.18617(vacuum drying) and 0.07715~0.18056(hot air drying) g H2O/g solid respectively using the BET equation. BET equation for isothermal absorption curve showed over 0.95 R-square for all dried methods. Monolayer moisture contents were increased as storage temperature was incremented because water molecular movement was more active and there was a greater chance to clash with the absorption surface area.

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Absorption Characteristics of Korean Yam Powder by Different Drying Methods (건조방법에 따른 분말마의 흡습특성)

  • 차원섭;박준희;오상룡;조영제;이원영
    • Journal of Life Science
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    • v.10 no.3
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    • pp.229-235
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    • 2000
  • The absorption characteristics of Korean yam powder according to different drying methods were investigated. The physical properties of yam powder by different drying methods were showed the biggest porosity in freeze drying sample, while the smallest in hot air drying sample. No difference was founded in proximate compositions of yam powder by various drying methods. The amount of total phenolic compound and Vit C were showed the bigger decrement in freeze dried sample than other drying methods. The time reaching to equilibrium moisture content were determined in 12 days. Monolayer moisture contents were predicted to 0.0508∼0.0588 by BET equation and 0.0705∼0.0811 g H2O/g solid by GAB equation. BET equation for isothermal absorption curve showed over 0.95 R-square for every drying methods. GAB equation showed over 0.99 in vacuum and freeze drying but a poor R-square in hot air drying.

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Changes in Moisture Content and Quality of Chewing Gum during Storage (저장중 츄잉껌의 수분함량과 품질변화)

  • Chung, Duk-Ho;Lee, Yoon-Hyung;Yoo, Myung-Shik;Pyun, Yu-Ryang
    • Korean Journal of Food Science and Technology
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    • v.24 no.2
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    • pp.117-121
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    • 1992
  • The changes in sensory and mechanical texture of chewing gum during storage at various relative humidity were studied to define the quality index for the prediction of shelf-life. The initial moisture content of chewing gum was 2.57% (dry basis). The BET monolayer value at $a_{w}$ 0.19 was calculated to be 1.57% (dry basis). The sensory scores of chewing gum were closely correlated with moisture content and instrumental texture parameters with 0.1% significant level. Therefore the quality of stored chewing gum was directly related with moisture content above BET monolayer. The products became organoleptically acceptable in the range of moisture content $2.17{\sim}3.16%(dry basis)$. This range of moisture content ie equivalent to the ranges of instrumental parameter, fracture force$0.8{\sim}1.8{\times}10^{7}$, fracture modulus $1.1{\sim}2.4{\times}10^{8}$, puncture force $0.5{\sim}1.1{\times}10^{7}[dyne/cm^{2}]$ and brittleness $0.7{\sim}1.4{\times}10^{8}[dyne/cm^{3}]$, respectively.

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Absorption Characteristics and Prediction Model of Ginger Powder by Different Drying Methods (건조방법에 따른 생강분말의 흡습특성과 예측모델에 관한 연구)

  • Shin, Hae-Kyoung;Hwang, Sung-Hee;Youn, Kwang-Sup
    • Korean Journal of Food Science and Technology
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    • v.35 no.2
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    • pp.211-216
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    • 2003
  • Absorption characteristics of hot air-. vacuum-, and freeze-dried ginger powder were investigated. Monolayer moisture content as determined by GAB equation was $0.257{\sim}0.540\;H_2O/g$, showing higher significance than BET equation. Absorption enthalpy was calculated based on different drying methods and water activities. Absorption energy decreased with increasing water activity but was not affected by drying method. Isotherm curves showed a typical sigmoid form. Among models applied for predicting equilibrium moisture content, Caurie model was the best fit model for ginger powder, showing the lowest prediction deviation of $1.2{\sim}5.4%$, followed by Henderson then Bradley models. The prediction model equations for the moisture content were established by in(time), water activity, and temperature.

Moisture Sorption Isotherm Characteristics of Chaga Mushroom Powder as Influenced by Particle Size

  • Lee, Min-Ji;Lee, Jun-Ho
    • Food Science and Biotechnology
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    • v.16 no.1
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    • pp.154-158
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    • 2007
  • Adsorption isotherms for chaga mushroom powder as influenced by particle size were investigated using a gravimetric technique. Samples were equilibrated in desiccators containing sulfuric acid solutions of known water activity (0.11-0.93), then placed in temperature-controlled chambers for approximately ten days. Equilibrium moisture content (EMC) of chaga mushroom powder increased with water activity in all samples. EMC was slightly greater in the samples comprised of smaller particle size, however there was no marked difference in appearance between the three samples. The chaga mushroom powder exhibited Type II behavior. When the BET model was used to determine mean monolayer values, 0.077, 0.077, and 0.070 $H_2O/dry$ solid was observed for <250, 250-425, and $425-850\;{\mu}m$ sized samples, respectively, however mean monolayer values were 0.121, 0.111, and 0.101 $H_2O/dry$ solid, respectively, when the GAB model was used. The experimental EMC values were related to the computed values from Henderson's model. The coefficient of determination and standard error for the linear regression were 0.997 and 0.003, respectively.

Studies on Food Preservation by Controlling Water Activity 1. Measurement of Sorption Isotherm of Dried Filefish Muscle by Equilibration in Dynamic Stream of Conditioned Air (식품보장과 수분활성에 관한 연구 1. 조절기류에 의한 건조말쥐치육의 등온흡습곡선의 측정)

  • HAN Bong-Ho;CHOI Soo-Il
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.14 no.4
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    • pp.189-193
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    • 1981
  • An apparatus for continuous measurements of sorption isotherm of dried food was manufactured to shorten the time required for equilibration. The apparatus was so designed that the temperature, air velocity and relative humidity in the experimental chamber could be controlled. The use of dynamic stream of conditioned air with a velocity of 0.2m/sec, instead of static atmosphere, allowed a faster equilibration of dried filefish muscle at $25^{\circ}C$. The mean time necessary for the equilibration of dried filefish muscle at the water activity of a given state to a higher water activity was about 45 hours. The monolayer moisture content of dried filefish muscle calculated from BET-equation was 0.092 kg water /kg dry matter at $25^{\circ}C$.

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