• Title/Summary/Keyword: B4C grain

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Effects of the Precipitation of Carbides and Nitrides on the Texture Structures in Extra Low Carbon Steel Sheets containing B, Nb and Ti(ll) (B, Nb및 Ti를 함유한 극저탄소강에서 탄화물 및 질화물의 석출이 집합조직에 미치는 영향(ll))

  • Lee, Jong-Mu;Yun, Guk-Han;Lee, Do-Hyeong
    • Korean Journal of Materials Research
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    • v.3 no.2
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    • pp.131-139
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    • 1993
  • Abstract Alloying elements such as AI, Ti, Nb and B in the extra low carbon AI-killed steel precipitate as nitrides or carbides and change the recrystallization texture structure of the steel during heattreatment with the result of strong effects on the deep drawability of the steel sheet. In this study the effects of fine precipitates such as nitrides and carbides on the texture of extra low carbon steels into which Ti, Nb, B, P, Si and Mn were added as alloying elements were investigated by means of TEM, SEM and optical microscopic analyses. Fine N$b_2$C and T$i_2$AIN precipitates are mainly observed in the steel containing both Nb and Ti, while fine AIN and coarse BN precipitates are observed in the Nb~containing steel and coarse T${i_4}{N_3}$ and ${N_10}{N_22}$/T$i_68$ precipitates are observed in the Ti-containing steel. The grain size of the Ti containing steel is larger than that of the Nb containing steel and that of the one containing both Nb and Ti.

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Homogeneity of Microstructure and Mechanical Properties of Ultrafine Grained OFHC Cu Bars Processed by ECAP (ECAP 가공에 의해 제조된 초미세립 OFHC Cu 봉재의 미세조직 및 기계적 특성의 균질성)

  • Ji, Jung Hoon;Park, Lee-Ju;Kim, Hyung Won;Hwang, Si Woo;Lee, Chong Soo;Park, Kyung Tae
    • Korean Journal of Metals and Materials
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    • v.49 no.6
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    • pp.474-487
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    • 2011
  • Bars of OFHC Cu with the diameter of 45 mm were processed by equal channel angular pressing up to 16 passes via route $B_c$, and homogeneity of their microstructures and mechanical properties was examined at every four passes which develop the equiaxed ultrafine grains. In general, overall hardness, yield strength and tensile strength increased by 3, 7, and 2 times respectively compared with those of unECAPed sample. Cross-sectional hardness exhibited a concentric distribution. Hardness was the highest at the center of bar and it decreased gradually from center to surface. After 16 passes, overall hardness decreased due to recovery and partial recrystallization. Regardless of the number of passage, yield strength and tensile strength were quite uniform at all positions, but elongation showed some degree of scattering. At 4 passes, coarse and ultrafine grains coexisted at all positions. After 4 passes, uniform equiaxed ultrafine grains were obtained at the center, while uniform elongated ultrafine grains were manifested at the upper half position. At the lower half position, grains were equiaxed but its size were inhomogeneous. It was found that inhomogeneity of grain morphology and grain size distribution at different positions are to be attributed to scattering in elongation but they did not affect strength. The present results reveal the high potential of practical application of equal channel angular pressing on fabrication of large-sized ultrafine grained bars with quite homogeneous mechanical properties.

The Formation and Transition of 2212 and 2223 Phase in BPSCCO System (BPSCCO System에서 2212 및 2223 phase의 생성.전이)

  • Park, Y.P.;Wang, J.B.;Kim, H.C.;Kim, W.G.;Lee, J.U.
    • Proceedings of the KIEE Conference
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    • 1991.11a
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    • pp.311-315
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    • 1991
  • The formation and transition of 2212 and 2223 phase have been studied in BPSCCO system. The 2212 phase formed in early sintering state reacts on $Ca_2PbO_4,\;Ca_2CuO_3$ and CuO during sintering process and thus produces the 2223 phase. A long sintering period is need to fabricate the superconductor with large volume fraction of 2223 phase. Also, the thin plate-like grains composed of Bi, Sr, Ca and Cu contribute to 2223 phase formation. Though the sample has lower volume fraction of 2223 phase, the critical temperature is measured highly in case of the grain grown to plate-like shape. In this work, the critical temperature of the sample sintered for 264 hr in air was measured 108 K. Microstructure of the sample was varied with condition of heat treatment after sintering process and the sample annealed with $500^{\circ}C$ for 5 hr showed excellent charateristics of 2223 phase formation.

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Studies on the Foliar Application of Urea as Nitrogen Source of Rice Plant Nutrition (요소엽면살포(尿素葉面撒布)에 따른 수도(水稻)의 질소영양(窒素營養)에 관(關)한 연구(硏究))

  • Cho, Seoung-Jin
    • Applied Biological Chemistry
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    • v.9
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    • pp.125-147
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    • 1968
  • This experiment was carried out as a part of the studies on reasonable application of nitrogen in rice plant to determine: (I) Nitrogen absorption. and rooting of rice seedlings as affected by urea foliar application at late seedling stage (II) Effect of leaf prunning and foliar application of urea at late heading stage on the maturation and yield of rice (III) Effect of foliar application of urea and its time during the stage of ear formation on yield of rice plant. Results obtained are summarized as follows. Exp.I: Nitrogen absorption and rooting of rice seedlings as affected be urea foliar application at late seedling stage. 1 : The foliar application of urea plots$(T_{1},T_2)$ snowed mare N-content than non-urea foliar application plot(T0) at lane seedling stage, being significant among treatments and foliar application of urea seemed more effective in increasing the N-content of seedlings. and promoted root settlement and early growth alter the transplanting. 2 : The carbon contents of the plants of $T_1$, and $T_2$ at late seedling stage increased than T0, and the carbon contents. of $T_1$ and $T_2$ plots became higher in amount in proportion to the nitrogen absorption as compared with those of $T_0$. 3 : C/N ratio appeared significant among soil application plots($N_1, \;N_2$) and foliar application of urea plots ($T_1$, $T_2$ and $T_0$). C/N ratio was lower in case of increased amount of nitrogen. The higher contents of nitrogen and carbon and lower C/N ratio resulted in the increment of root numbers and root lengths. Exp.II: Effect of leaf prunning and foliar application of urea at late heading stage on the maturation and yield of rice. 1 : There was a highly significant decrease in the maturing rate by severe leaf prunning. In the mean time, significant increase in maturing rate was observed with urea foliar application and it was found the more frequent application the more effective for higher maturing rate with a moderate significance. A correlationship between the level of prunning and maturing rate was enumerated to 0.961 of correlation coefficient, which indicated an increased maturing rate by the increased number of remaining leaves. 2 : The 1.000 grain weight, grain weight and hulled rice yield increased by leaf prunning in order (plot a$A_1$, $A_3$, $A_2$ and $A_0$ were 89.8%, 89.4%, 87.8% and 87.5% respectively, showing the highest of rate in $A_1$ and $A_3$ in methods of ear fertilization and being highly significant between its treatment. 3 : 1000 grain weights were highly significant between time of application, showing a tendency of increase of weights with the time lagging until days before earings as that of maturing rates. High significance was recognized between methods of ear fertilization, showing the highest in $A_2$ 23.18 gr. 4 : Yields per $3.3m^2$ were not significant between time of ear fertilization, whereas were highly significant between methods of ear fertilization. Those of $A_1$, $A_3$, $A_2$ and $A_0$ were 1.486 kg, 1.491 kg, 1.381 kg and 1.328 kg, respectively, showing the highest in $A_1$ and $A_3$. 5 : Hulling ratios showed significant different between time of ear fertilization, showing the highest in $T_2$, whereas those of methods of ear fertilization were highly significant between its treatment, Those of $A_1$, $A_3$, $A_2$ and $A_0$ were 84.72%, 84.06%, 83.29%, and 82.56% respectively, showing the highest m $A_2$ and $A_3$ among others. 6 : Yields of hulled rice per $3.3m^2$ showed significant different between time of ear fertilization, showing the highest in $T_1$ 1.192 kg. Whereas, those were highly significant between methods of ear fertilization. Those of $A_1$, $A_3$, $A_2$ and $A_0$ were 1.259 kg, 1.254 kg, 1.149 kg and 1.095 kg, respectively, showing the highest in $A_1$ and $A_2$. 7 : Contents of nitrogen on rice plant increased in case of nitrogen application as ear fertilizer and showed that the case of urea foliar application was more effective than that of soil application, showing the increased nitrogen content of rice plant was accompanied by carbon content.

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Effect of F$e_2$P Addition on Microstructures of Sintered 4600 Steel (4600계 소결강의 조직에 미치는 F$e_2$P첨가의 영향)

  • Kim, Dong-Uk;Lee, Wan-Jae
    • Korean Journal of Materials Research
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    • v.2 no.6
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    • pp.428-435
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    • 1992
  • AISI 4600 Iron powder was mixed with 0~1.0% phosphor as F$e_2$P powder and/or 0~0.8% carbon as graphite powder in rotating mixer. Mixed powder was pressed 800MPa in double-punch mould. Compacts were sintered at 115$0^{\circ}C$for 30 min. in vacuum or mixed hydrogen and nitrogen gas. Sintered compacts were ground and polished, and etched by 2% nital etchant. The microstructure was observed by image analyzer and optical microscope. Density and microhardness were tested by ASTM B3l2 and Microvickers hardness tester. The results obtained were as follows : (1) As the amount of F$e_2$P powder increased, sintered microstructure showed more densified effect and the grain size was larger. (2) The shape of pore was rounded and the number of pore was decreased by F$e_2$P addition. But mean pore size was larger with F$e_2$P content. (3) Simultaneous alloying addition of F$e_2$P and graphite brought about larger grain growth than respective addition. (4) Sintering atmosphere did not affect the microstructure. (5) Hardness of sintered compact increased with phosphrous and carbon content.

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A Study on the Effect of Compaction Energy on Soil Compaction (흙의 다짐에너지가 다짐효과(效果)에 미치는 영향(影響)에 관(關)한 연구(硏究))

  • Kim, Sang Mok;Kang, Yea Mook
    • Korean Journal of Agricultural Science
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    • v.10 no.1
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    • pp.97-109
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    • 1983
  • In this study, the effects on the soil compaction were investigated through the various testing method by changing the number of layers, the number of blows per layer and drop height. The results obtained in this study were summarized as follows. 1. Soil compaction was largely influenced by maximum grain size of soil in case of small testing mold diameter. 2. The compaction effect showed best in the well graded soil. In this test, compaction effect showed the best value in the soil which contained about 30~40% of particles finer than No. 200 sieves although it would vary according to the content of coarse grained soil. 3. Though the compaction method was changed at the level of compaction energy fixed, the effect of soil compaction showed little. 4. The increment of compaction energy increased the effect of soil compaction, but over a certain limit the soil compaction showed little on the effect. 5. In the method to increase the compaction energy for the purpose of the most reasonable effect, the soil compaction effect was differently shown according to the grain size distribution of the soil.

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Apparent Densification Rate and Initial Permeability of NiCuZn Ferrite Depended on Relative Packing Density (NiCuZn Ferrite의 겉보기 고화속도와 초기투자율의 충진율 의존성에 관한 연구)

  • 류병환;이정민;고재천
    • Resources Recycling
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    • v.7 no.4
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    • pp.27-34
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    • 1998
  • In this research, the processing control of NiCuZn Ferrite (NCZF) had been studied. NiCuZn Ferrite, which calcined at $700^{\circ}C$ for 3 bours, was ball milled for about 60 hours to ill김ke a size of $0.5\mu\;extrm{m}$ followed by granulation using spray dryer Apparent densincatioo rate and initial permeability of NiCuZn Ferrite with an initial packing density had been investigated as f follows. 1.The relative packing density of NCZF green body increas$\xi$d in the range of 48.6-56.8% with an increased forming pressure of 20-170 MPa. 2. The higher the relative pac퍼ng density of NCZF and the sintering temperature are, the higher the initial densification rate. The increased bulk rlcnsity of NCZF was attributed to the densification rate with decreased open pore and increased closed pore as the relative packing density, sintering temperature, and sinteriog tim$\xi$ increased. 3. The initial P permeability of NCZF with constant composition is logarithmically proportional to the bulk density of NCZF sintered at $875~925^{\circ}C$ for 0-5h, and strongly depended on the relative packing density of NCZF green body. The empirical equation is as f follows; log $\mu$i=$G1{\times}BD$+$G2{\times}RPD$+b(0);where, G1, G2; gradient, B.D: bulk density, RPD; relative packing density, b(0); intercept.

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Quality and physicochemical characteristics of newly developed Sunsik products with germinated brown rice (발아현미 선식의 품질 및 이화학적 특성)

  • Bang, Yae-Sol;Jang, Eun Hee;Chung, Hyun-Jung
    • Korean Journal of Food Science and Technology
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    • v.49 no.5
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    • pp.513-518
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    • 2017
  • The quality and physicochemical characteristics of newly developed Sunsik products were investigated. Sunsik A, B, and C were prepared under different roasting temperatures and times (A: $220^{\circ}C$, 15 min; B: $220^{\circ}C$, 25 min; C, D, E: $230^{\circ}C$, 15 min). Sunsik D was prepared using grain flours passed through a 100 mesh screen, whereas the other products were passed through a 140 mesh screen. Sunsik E was prepared by the addition of germinated grains. The moisture content of Sunsik products ranged from 3.24-7.10%. The viscosity and sugar content ranged from 57-74 cP and $1.5-1.7^{\circ}Bx$, respectively. The pH values were similar among the samples. Sunsik D had the highest gelatinization enthalpy, whereas Sunsik C had the lowest. The viable cell counts were in the range from 3-4 log CFU/g and coliform groups were not detected. Sunsik B and E had higher scores for savory flavor and sweet taste than other Sunsik products.

Effect of Low Tempering Temperature on Corrosion Resistance of 420J2 Stainless Steel (420J2 스테인리스강의 내식성에 미치는 저온 템퍼링의 영향)

  • Jung, B.H.;Kim, H.J.;Kim, M.G.;Oh, I.S.;Kim, D.S.
    • Journal of the Korean Society for Heat Treatment
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    • v.17 no.1
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    • pp.29-35
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    • 2004
  • The effect of low tempering in a temperature range of $150{\sim}400^{\circ}C$ on corrosion resistance in 420J2 stainless steel austenitized at $1000^{\circ}C$ was investigated by the application of salt spray test, electrochemical pitting test in 3.5% NaCl solution and DL-EPR test for intergranular corrosion in 0.5M $H_2SO_4$+0.01M KSCN solution. In salt spray test, good corrosion resistance was obtained in a tempering temperature range of $150{\sim}250^{\circ}C$. Pitting potential was increased to the tempering temperature of $250^{\circ}C$, but decreased with the increase of temperature up to $400^{\circ}C$ And it was thought that the degradation of pitting corrosion resistance showed at the tempering temperature of around $400^{\circ}C$ was due to the precipitation of $Cr_7C_3$ of $M_7C_3$ type. The degree of sensitization showed increasing tendency with the increase of tempering temperature, and also Cr depletion phenomena were observed in the vicinity of grain boundary.

Static Pressure Drop as Affected by Moisture and Fine Material in Wheat (밀의 함수율과 미세립자가 정압강하에 미치는 영향)

  • Kim, Y.J.
    • Journal of Biosystems Engineering
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    • v.15 no.4
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    • pp.339-345
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    • 1990
  • 공기통풍 건조시 공기흐름(airflow)에 대한 곡물저항(grain resistance)은 송풍시스템에서 fan의 선정시 매우 중요하다. 지금까지는 공기흐름에 대한 곡물저항은 주로 Shedd의 curve에 준하여 정해졌다. 그러나 실제의 경우 곡물수확 또는 건조시 기계적 원인에 의하여 미세립자(fine material)가 생성된다. 이에 본 연구에서 밀(red hard winter wheat)을 대상으로 송풍량, 함수율, 미세립자량이 정압강하(static pressure drop)에 미치는 영향을 규명하였고, 이러한 변수가 포함된 수학적 모델을 개발하였다. 독립변수는 0.051로부터 $0.203m^3/m^2.sec$에 이르는 7단계의 각각 다른 송풍량과 3단계의 함수율 (11, 13, 15%w.b), 4단계의 미세립자량(0, 2, 4, 8%)이고, 종속변수는 정압강하이다. 정압강하와 test bed에서의 송풍량은 micromanometer를 사용하여 측정하였다. 결과는 독립변수(송풍량, 함수율, 미세립자량)는 모두 정압강하에 significant하게 영향을 미치는 것으로 나타났다. 규정된 범위내에서 함수율이 증가함에 따라 정압강하는 최고 45% 까지 감소되었고, 반면 미세립자량이 증가함에 따라 정압강하는 최고 195%까지 증가되었다. 수집된 data로서 다음과 같은 regression equation이 개발되었다($P=AV+BV^2+C(MO)V+D(FM)V$). 본 연구의 결과는 공기송풍시스팀에서 송풍량, 함수율, 미세립자량이 정압강하에 미치는 영향을 규명하였고, 에너지 절약적 송풍시스템을 설계하는 데 도움이 될 수 있을 것이다.

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