• Title/Summary/Keyword: Average grain size

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Effect of Grain Size and Heat-treating Atmosphere on the Phase Stability of Y-TZP (입자크기와 열처리 분위기 변화에 따른 Y-TZP에서의 상안정성 변화)

  • Chung, Tai-Joo;Ahn, Seung-Su;Song, Eun-Wha;Oh, Kyung-Sik;Lee, Jong-Sook;Kim, Young-Sik
    • Journal of Powder Materials
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    • v.13 no.5 s.58
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    • pp.360-365
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    • 2006
  • The phase stability of tetragonal phase in Y-TZP was investigated in terms of the distribution of grain sizes and heat-treating atmosphere. Y-TZP with various grain sizes were prepared using duration time at $1600^{\circ}C$ as experimental parameter. Accumulated grain size distributions were built from the SEM micrographs and the amount of tetragonal phase were measured using XRD. Both results were compared to determine the critical grain size before and after heat-treatment in vacuum. The critical grain size drastically decreased compared with the small increase of average grain size due to the autocatalytic effect which critically affects the tetragonal to monoclinic phase transformation. After heat-treatment in reductive atmosphere critical grain size relatively increased due to the stabilization of tetragonal phase. The formation of oxygen vacancies during heat-treatment was ascribed to the increase of stability.

Pore Filling Theory of Liquid Phase Sintering and Microstrcture Evolution (액상소결의 기공채움 이론과 미세구조 발달)

  • 이성민
    • Journal of Powder Materials
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    • v.6 no.1
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    • pp.81-87
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    • 1999
  • Based on the pore filling theory, the microstructure evolution during liquid-phase sintering has been analyzed in terms of interrelationship between average grain size and relative density. For constant liquid volume fraction, the microsturucture trajectories reduced to a single curve in a grain size(x)-density(y) map, regardless of grain growth constant. The slope of curves in the map was inversely proportional to average pore size, while it increased fapidly with liquid volume fraction. Increase in pore volume fraction retarded the densification considerably, but showed marginal effect on the slope. The activation energy of densification was predicted to be the same as that of grain growth as long as the liquid volume fraction is constant for any temperature range studied. The present analyses on microstricture evolution may demonstrate the usefulness of pore filling theory and provide a guideline for process optimization of liquid-phase sintering.

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Characteristics of specific grinding energy depending on grain size (연삭입자크기에 따른 비연삭에너지 특성)

  • Lee H.G.;Lee Y.M.;Yang S.H.;Bae D.W.;Kim H.K.
    • Proceedings of the Korean Society of Machine Tool Engineers Conference
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    • 2005.05a
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    • pp.319-323
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    • 2005
  • As a new approach to analyze grinding energy, this paper introduces a specific grinding energy model based on the average grain. Using this model, grinding characteristics such as specific grinding energy of SM45C were investigated with changing variables such as grain size, workpiece velocity(v) and apparent depth of cut(Z) in down-surface grinding. From the experimental results, the specific grinding energy decreases as the maximum undeformed chip thickness increases. And also the specific grinding energy increases as the grit size increases.

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Microstructural Changes of AA1100 According to the Processing Number of Multi-Axial Diagonal Forging (MADF) (다축대각단조(MADF) 가공횟수에 따른 AA1100의 미세조직 변화)

  • Kwon, S.C.;Kim, S.T.;Kim, D.V.;Kim, M.S.;Lee, S.;Choi, S.H.;Jeong, H.T.
    • Transactions of Materials Processing
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    • v.28 no.2
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    • pp.63-70
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    • 2019
  • This study investigates the effects of multi-axial diagonal forging (MADF) processing number on the microstructures of AA1100 fabricated using MADF processes. The cast AA1100 was annealed at $400^{\circ}C$ for 3hrs in $N_2$ atmosphere and cut into $25mm^3$ cubes for the MADF processes. The MADF process consist of plane forging with a thickness reduction of 30% and a diagonal forging with a diagonal forging angle of 135 degrees. In order to analyze the microstructural variations based on the number of repetitions, 1, 2, 3 and 4 cycles of the MADF process were performed. AA1100 specimens were successfully deformed without cracking of the surface for up to 4 cycles of MADF. The grain size, average misorientation and average grain orientation spread (GOS) of MADF processed materials were analyzed using EBSD technique. The results showed that MADF process effectively refined the microstructure of AA1100 with an initial average grain size of $337.4{\mu}m$. The average grain sizes of specimens which were MADF processed for 2, 3, 4 cycles were refined to be $1.9{\mu}m$, $1.6{\mu}m$, $1.4{\mu}m$, respectively. The grain refinement appeared saturated when AA1100 got MADF processed over 2 cycles. When the specimen was subjected to two or more cycles of MADF, the degree of decrease in the average grain size drastically decreased with an increase in the number of cycle due to the softening phenomena such as dynamic recovery or dynamic recrystallization during processing.

Measurement of WC Grain Size in Nanocrystalline WC-10Co Hardmetal

  • Chenguang, Lin;Guansen, Yuan
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.344-345
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    • 2006
  • The linear intercept (LI) method was used to quantitatively measure the intercepts of WC grains in nano-grained WC-10Co hardmetal. When the surveyed intercept numbers of WC grain exceeded 200, the statistic data for the mean grain size of WC were reproduced. The discriminative minimal grain size of used LI method was 12 nm; the maximum intercept of WC grain was 109 nm; the average intercept of WC grains was 45 nm and the corresponding 3D mean grain size of WC was 70 nm which is agreeable with the XRD outcome.

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Comparison of Grain Filling Characteristics by Source-Sink Size Control in Glutinous and Non-glutinous Near Isogenic Line of Rice (근동질유전자 계통인 찰벼와 메벼의 전엽과 절영처리에 따른 등숙특성 비교)

  • 김춘송;안종국;정일민;강항원;이재생;고지연;박성태
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.49 no.3
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    • pp.243-250
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    • 2004
  • Two cultivars which are glutinous (Hawcheongchalbyeo) and non-glutinous (Hawcheongbyeo) near isogenic line of rice, were used for this study. The objective of this experiment was to gain the basic information for increasing grain yield of waxy rice by means of source and sink size control. In both Hwacheongbyeo and Hawcheongchalbyeo, the trend of decrease in total and average spikelet weight was ranked as follows; removal of penultimate leaf< removal of flag leaf< removal of flag leaf and 3ya leaf from the top < removal of flag leaf and penultimate leaf < removal of flag leaf, penultimate leaf, and 3rd leaf from the top. The reduction yale of total and average spikelet weight per panicle of Hwacheongbyeo was higher than those of Hwacheongchalbyeo according to the removal of flag leaf, penultimate leaf, and 3rd leaf from the top. In both cultivars, high-density grain ratio and grain filling ratio of the primary branches were higher Hun those of the secondary branches by leaf clipping treatment. The spikelet number and total spikelet weight per pinicle in both Hwacheongbyeo and Hwacheongchalbyeo were decreased by removal of spikelets on branches compared with control, whereas average spikelet weight and grain filling ratio were increased. The increase rate of average spikelet weight of Hwacheongchalbyeo was much higher than that of Hwacheongbyeo by sink size control. High-density grain ratio by removal of spikelets on branches was higher in Hwacheongchalbyeo, but filled grain ratio was higher in Hwacheongbyeo.

Growth Behavior of (Ti,W)(C,N) and WC grains in a Co Matrix (Co 액상 내에 공존하는 (Ti,W)(C,N)과 WC입자의 성장 거동)

  • 이보아;윤병권;강석중
    • Journal of Powder Materials
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    • v.11 no.2
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    • pp.165-170
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    • 2004
  • Growth behavior of two different types of grains, faceted and rounded, in a liquid matrix has been studied in the (75WC-25TiCN)-30Co system. Powder samples were sintered above the eutectic temperature for various times under a carbon saturated condition. (Ti,W)(C,N) grains with a rounded shape and WC grains with a faceted shape coexisted in the same Co based liquid. With increasing sintering time, the average size of (Ti.W)(C,N) grains increased continuously and very large WC grains appeared. The growth of rounded (Ti,W)(C,N) grains followed a cubic law, r^3-r^3_0$=kt, where r is the average size of the grains, $r_0$ the initial average size, k the proportionality constant and t the sintering time. indicating a diffusion-controlled growth. On the other hand, the growth of the faceted WC grains resulted in a bimodal grain size distribution, showing an abnormal grain growth. These observations show that the growth behavior of different types of grains is governed by their shape, faceted or rounded, even in the same liquid matrix.

Transport and Deposition Characteristics of Coarse Grained Soil According to the Flow Velocity and Grain Size (유속 및 입경에 따른 조립토의 이동 및 퇴적 특성)

  • Bong, Tae-Ho;Son, Young-Hwan;Kim, Kyu-Sun;Park, Jae-Sung;Kim, Dong-Geun
    • Journal of The Korean Society of Agricultural Engineers
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    • v.58 no.1
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    • pp.11-17
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    • 2016
  • Dredging and land reclamation works has actively carried out for the efficient use of land and secure of agricultural and industrial site. During the reclamation, a portion of landfills are lost from the desired location due to a variety of causes. However, these causes has been rarely studied, and water flow velocity has a great influence on the movement of landfills. For the economical and efficient reclamation, it is important to predict the movement of landfills in water. In this paper, an experimental study was carried out to investigate the deposition distance according to the flow velocity and soil grain size. We have made a large open-channel apparatus that can reproduce a laminar flow, and the deposition test was carried out on the four grain size (0.638, 1.425, 3.375, 7.125 mm) and four flow velocity (0.1, 0.3, 0.5, 0.67 m/s) with high definition video recording. As a results, average deposition distance increased with the flow velocity, and its relationship is shown linearly. For the grain size, the average deposition distance were drastically increased as the grain size becomes smaller.

Effects of Grain Size on High Temperature Deformation Behavior of Sc added Al-Mg Alloy (Sc첨가한 Al-Mg 합금의 고온변형 거동에 미치는 결정립 크기의 영향)

  • Woo, K.D.;Kim, S.W.;Kim, H.S.;Yang, C.H.;Park, H.C.;MIURA, Y.;Park, K.T.
    • Korean Journal of Materials Research
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    • v.12 no.9
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    • pp.701-705
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    • 2002
  • High temperature tensile test has been performed at $450^{\circ}C$ at different strain rate with various grain size due to different reduction rate of Al-4wt%Mg-0.4wt%Sc alloy which is known to be one of useful superplastic alloys. The grain size of Al-4wt%Mg-0.4wt%Sc alloy is $67~100\mu\textrm{m}$ which is courser than that of the alloy which is commonly used as the superplastic material. The total elongation of the Al-4wt%Mg-0.4wt%Sc alloy is strongly dependent on the average grain size, and is a linear function of the inverse average grain size for the present alloy.

Inference Models for Tidal Flat Elevation and Sediment Grain Size: A Preliminary Approach on Tidal Flat Macrobenthic Community

  • Yoo, Jae-Won;Hwang, In-Seo;Hong, Jae-Sang
    • Ocean Science Journal
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    • v.42 no.2
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    • pp.69-79
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    • 2007
  • A vertical transect with 4 km length was established for the macrofaunal survey on the Chokchon macrotidal flat in Kyeonggi Bay, Incheon, Korea, 1994. Tidal elevation (m) and sediment mean grain size $(\phi)$ were inversely predicted by the transfer functions from the faunal assemblages. Three methods: weighted average using optimum value (WA), tolerance weighted version of the weighted average (WAT) and maximum likelihood calibration (MLC) were employed. Estimates of tidal elevation and mean grain size obtained by using the three different methods showed positively corresponding trends with the observations. The estimates of MLC were found to have the minimum value of sum of squares due to errors (SSE). When applied to the previous data $(1990\sim1992)$, each of three inference models exhibited high predictive power. This result implied there are visible relationships between species composition and faunas' critical environmental factors. Although a potential significance of the two major abiotic factors was re-affirmed, a weak tendency of biological interaction was detected from faunal distribution patterns across the flat. In comparison to the spatial and temporal patterns of the estimates, it was suggested that sediment characteristics were the primary factors regulating the distribution of macrofaunal assemblages, rather than tidal elevation, and the species composition may be sensitively determined by minute changes in substratum properties on a tidal flat.