• 제목/요약/키워드: Average grain size

검색결과 610건 처리시간 0.023초

입자크기와 열처리 분위기 변화에 따른 Y-TZP에서의 상안정성 변화 (Effect of Grain Size and Heat-treating Atmosphere on the Phase Stability of Y-TZP)

  • 정태주;안승수;송은화;오경식;이종숙;김영식
    • 한국분말재료학회지
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    • 제13권5호
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    • pp.360-365
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    • 2006
  • The phase stability of tetragonal phase in Y-TZP was investigated in terms of the distribution of grain sizes and heat-treating atmosphere. Y-TZP with various grain sizes were prepared using duration time at $1600^{\circ}C$ as experimental parameter. Accumulated grain size distributions were built from the SEM micrographs and the amount of tetragonal phase were measured using XRD. Both results were compared to determine the critical grain size before and after heat-treatment in vacuum. The critical grain size drastically decreased compared with the small increase of average grain size due to the autocatalytic effect which critically affects the tetragonal to monoclinic phase transformation. After heat-treatment in reductive atmosphere critical grain size relatively increased due to the stabilization of tetragonal phase. The formation of oxygen vacancies during heat-treatment was ascribed to the increase of stability.

액상소결의 기공채움 이론과 미세구조 발달 (Pore Filling Theory of Liquid Phase Sintering and Microstrcture Evolution)

  • 이성민
    • 한국분말재료학회지
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    • 제6권1호
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    • pp.81-87
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    • 1999
  • Based on the pore filling theory, the microstructure evolution during liquid-phase sintering has been analyzed in terms of interrelationship between average grain size and relative density. For constant liquid volume fraction, the microsturucture trajectories reduced to a single curve in a grain size(x)-density(y) map, regardless of grain growth constant. The slope of curves in the map was inversely proportional to average pore size, while it increased fapidly with liquid volume fraction. Increase in pore volume fraction retarded the densification considerably, but showed marginal effect on the slope. The activation energy of densification was predicted to be the same as that of grain growth as long as the liquid volume fraction is constant for any temperature range studied. The present analyses on microstricture evolution may demonstrate the usefulness of pore filling theory and provide a guideline for process optimization of liquid-phase sintering.

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연삭입자크기에 따른 비연삭에너지 특성 (Characteristics of specific grinding energy depending on grain size)

  • 이현구;이영문;양승한;배대원;김학균
    • 한국공작기계학회:학술대회논문집
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    • 한국공작기계학회 2005년도 춘계학술대회 논문집
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    • pp.319-323
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    • 2005
  • As a new approach to analyze grinding energy, this paper introduces a specific grinding energy model based on the average grain. Using this model, grinding characteristics such as specific grinding energy of SM45C were investigated with changing variables such as grain size, workpiece velocity(v) and apparent depth of cut(Z) in down-surface grinding. From the experimental results, the specific grinding energy decreases as the maximum undeformed chip thickness increases. And also the specific grinding energy increases as the grit size increases.

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다축대각단조(MADF) 가공횟수에 따른 AA1100의 미세조직 변화 (Microstructural Changes of AA1100 According to the Processing Number of Multi-Axial Diagonal Forging (MADF))

  • 권상철;김순태;김다빈;김민성;이성;최시훈;정효태
    • 소성∙가공
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    • 제28권2호
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    • pp.63-70
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    • 2019
  • This study investigates the effects of multi-axial diagonal forging (MADF) processing number on the microstructures of AA1100 fabricated using MADF processes. The cast AA1100 was annealed at $400^{\circ}C$ for 3hrs in $N_2$ atmosphere and cut into $25mm^3$ cubes for the MADF processes. The MADF process consist of plane forging with a thickness reduction of 30% and a diagonal forging with a diagonal forging angle of 135 degrees. In order to analyze the microstructural variations based on the number of repetitions, 1, 2, 3 and 4 cycles of the MADF process were performed. AA1100 specimens were successfully deformed without cracking of the surface for up to 4 cycles of MADF. The grain size, average misorientation and average grain orientation spread (GOS) of MADF processed materials were analyzed using EBSD technique. The results showed that MADF process effectively refined the microstructure of AA1100 with an initial average grain size of $337.4{\mu}m$. The average grain sizes of specimens which were MADF processed for 2, 3, 4 cycles were refined to be $1.9{\mu}m$, $1.6{\mu}m$, $1.4{\mu}m$, respectively. The grain refinement appeared saturated when AA1100 got MADF processed over 2 cycles. When the specimen was subjected to two or more cycles of MADF, the degree of decrease in the average grain size drastically decreased with an increase in the number of cycle due to the softening phenomena such as dynamic recovery or dynamic recrystallization during processing.

Measurement of WC Grain Size in Nanocrystalline WC-10Co Hardmetal

  • Chenguang, Lin;Guansen, Yuan
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.344-345
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    • 2006
  • The linear intercept (LI) method was used to quantitatively measure the intercepts of WC grains in nano-grained WC-10Co hardmetal. When the surveyed intercept numbers of WC grain exceeded 200, the statistic data for the mean grain size of WC were reproduced. The discriminative minimal grain size of used LI method was 12 nm; the maximum intercept of WC grain was 109 nm; the average intercept of WC grains was 45 nm and the corresponding 3D mean grain size of WC was 70 nm which is agreeable with the XRD outcome.

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근동질유전자 계통인 찰벼와 메벼의 전엽과 절영처리에 따른 등숙특성 비교 (Comparison of Grain Filling Characteristics by Source-Sink Size Control in Glutinous and Non-glutinous Near Isogenic Line of Rice)

  • 김춘송;안종국;정일민;강항원;이재생;고지연;박성태
    • 한국작물학회지
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    • 제49권3호
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    • pp.243-250
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    • 2004
  • 본 시험은 찰벼의 수량제한요인을 알아내기 위하여 찰$.$메근동질유전자 계통인 화청찰벼와 와청벼를 공시하여 공급부위(잎)와 수용부위(영화)의 조절이 등숙에 미치는 영향을 구명함으로써 찰벼의 수량증대를 위한 기초자료를 얻고자 수행하였으며, 그 결과는 다음과 같다. 1. 이삭당 총립중과 편균립중의 감소경향은 두 품종 모두 차엽처리구 < 지엽처리구 < 상위 1, 3엽처리구 < 상위 1,2엽처리구 < 상위 1, 2, 3엽처리구 순이었다. 상위 1, 2, 3엽 제거에 의한 총립중과 평균립중의 감소율은 화청찰벼에 비하여 화청벼에서 컸다. 2. 화청벼와 화청찰벼 모두 전엽처리에 의한 고밀도립비율과 등숙율이 2차지경보다 1차지경에서 높았다. 3. 화청벼와 화청찰벼 모두 영화의 절제처리에 의하여 이삭당 총립수와 총립중이 대조구에 비하여 감소한 반면 평균입중과 등숙율은 증가되었다. 대조구와 비교한 평균입중의 증가율은 1, 2차지경립 및 상$.$하위지경립의 절제구 모두에서 화청찰벼가 화청벼보다 높았다. 4. 영화의 조절의 의하여 두 품종 모두 고밀도립비율과 등숙립비율이 증가되었으며 고밀도립비율은 화청찰벼가 화청벼에 비하여 높았던 반면에, 등숙립비율은 화청벼에서 높은 결과를 보였다.

Co 액상 내에 공존하는 (Ti,W)(C,N)과 WC입자의 성장 거동 (Growth Behavior of (Ti,W)(C,N) and WC grains in a Co Matrix)

  • 이보아;윤병권;강석중
    • 한국분말재료학회지
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    • 제11권2호
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    • pp.165-170
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    • 2004
  • Growth behavior of two different types of grains, faceted and rounded, in a liquid matrix has been studied in the (75WC-25TiCN)-30Co system. Powder samples were sintered above the eutectic temperature for various times under a carbon saturated condition. (Ti,W)(C,N) grains with a rounded shape and WC grains with a faceted shape coexisted in the same Co based liquid. With increasing sintering time, the average size of (Ti.W)(C,N) grains increased continuously and very large WC grains appeared. The growth of rounded (Ti,W)(C,N) grains followed a cubic law, r^3-r^3_0$=kt, where r is the average size of the grains, $r_0$ the initial average size, k the proportionality constant and t the sintering time. indicating a diffusion-controlled growth. On the other hand, the growth of the faceted WC grains resulted in a bimodal grain size distribution, showing an abnormal grain growth. These observations show that the growth behavior of different types of grains is governed by their shape, faceted or rounded, even in the same liquid matrix.

유속 및 입경에 따른 조립토의 이동 및 퇴적 특성 (Transport and Deposition Characteristics of Coarse Grained Soil According to the Flow Velocity and Grain Size)

  • 봉태호;손영환;김규선;박재성;김동근
    • 한국농공학회논문집
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    • 제58권1호
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    • pp.11-17
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    • 2016
  • Dredging and land reclamation works has actively carried out for the efficient use of land and secure of agricultural and industrial site. During the reclamation, a portion of landfills are lost from the desired location due to a variety of causes. However, these causes has been rarely studied, and water flow velocity has a great influence on the movement of landfills. For the economical and efficient reclamation, it is important to predict the movement of landfills in water. In this paper, an experimental study was carried out to investigate the deposition distance according to the flow velocity and soil grain size. We have made a large open-channel apparatus that can reproduce a laminar flow, and the deposition test was carried out on the four grain size (0.638, 1.425, 3.375, 7.125 mm) and four flow velocity (0.1, 0.3, 0.5, 0.67 m/s) with high definition video recording. As a results, average deposition distance increased with the flow velocity, and its relationship is shown linearly. For the grain size, the average deposition distance were drastically increased as the grain size becomes smaller.

Sc첨가한 Al-Mg 합금의 고온변형 거동에 미치는 결정립 크기의 영향 (Effects of Grain Size on High Temperature Deformation Behavior of Sc added Al-Mg Alloy)

  • 우기도;김석원;김학신;양창호;박희찬;;박경태
    • 한국재료학회지
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    • 제12권9호
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    • pp.701-705
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    • 2002
  • High temperature tensile test has been performed at $450^{\circ}C$ at different strain rate with various grain size due to different reduction rate of Al-4wt%Mg-0.4wt%Sc alloy which is known to be one of useful superplastic alloys. The grain size of Al-4wt%Mg-0.4wt%Sc alloy is $67~100\mu\textrm{m}$ which is courser than that of the alloy which is commonly used as the superplastic material. The total elongation of the Al-4wt%Mg-0.4wt%Sc alloy is strongly dependent on the average grain size, and is a linear function of the inverse average grain size for the present alloy.

Inference Models for Tidal Flat Elevation and Sediment Grain Size: A Preliminary Approach on Tidal Flat Macrobenthic Community

  • Yoo, Jae-Won;Hwang, In-Seo;Hong, Jae-Sang
    • Ocean Science Journal
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    • 제42권2호
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    • pp.69-79
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    • 2007
  • A vertical transect with 4 km length was established for the macrofaunal survey on the Chokchon macrotidal flat in Kyeonggi Bay, Incheon, Korea, 1994. Tidal elevation (m) and sediment mean grain size $(\phi)$ were inversely predicted by the transfer functions from the faunal assemblages. Three methods: weighted average using optimum value (WA), tolerance weighted version of the weighted average (WAT) and maximum likelihood calibration (MLC) were employed. Estimates of tidal elevation and mean grain size obtained by using the three different methods showed positively corresponding trends with the observations. The estimates of MLC were found to have the minimum value of sum of squares due to errors (SSE). When applied to the previous data $(1990\sim1992)$, each of three inference models exhibited high predictive power. This result implied there are visible relationships between species composition and faunas' critical environmental factors. Although a potential significance of the two major abiotic factors was re-affirmed, a weak tendency of biological interaction was detected from faunal distribution patterns across the flat. In comparison to the spatial and temporal patterns of the estimates, it was suggested that sediment characteristics were the primary factors regulating the distribution of macrofaunal assemblages, rather than tidal elevation, and the species composition may be sensitively determined by minute changes in substratum properties on a tidal flat.