• Journal of Welding and Joining
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• v.12 no.4
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• pp.141-150
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• 1994

The residual stress is inevitably introduced into composites because of the mismatch of the coefficient of thermal expansion, and it is different in each phase. The X-ray technique can detect separately the stress in each phase, so will wield useful information for analyzing the toughening mechanisms of composites. In order to apply the law of mixture to alloy steels with composite microstructures, two phase stainless steel, consisted of ferrite (.alpha.-Fe) and austenite (.gamma.-Fe) structures, was selected. The tensile elastic deformation was loaded, and then the X-ray diffraction technique was used to measure the X-ray elastic constants, the X-ray stress constants and the phase stresses. The law of mixture was investigated and the separation of macrostress and microstress was carried out. The phase stresses (the residual stresses of phase) in each phase, which were measured by X-ray technique, was directly proportional to the applied stress. The macrostress calculated from the phase stresses by using the law of mixture was nearly equal to the applied stress.

• Journal of Ocean Engineering and Technology
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• v.14 no.2
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• pp.65-69
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• 2000

This study is to investigate the characteristics of fatigue crack propagation in rolled super duplex stainless steel that was changed austenite-ferrite volume fraction by heat treatment. It was used two kinds of specimen the rolling and the transverse directions δ-phase fraction affected sound velocity hardness and Young's modulus. Characteristics of fatigue crack propagation was affected by anisotropy and (δ+γ) phase volume fractions.

• Journal of Powder Materials
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• v.25 no.3
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• pp.220-225
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• 2018

The microstructure and mechanical characteristics of SUS630 specimens fabricated using the direct energy deposition (DED) process are investigated. In DED, several process parameters such as laser scan speed, chamber gas flow, powder carrier gas flow, and powder feed rate are kept fixed; the laser power is changed as 150 W, 180 W, and 210 W. As the laser power increases, the surface becomes smooth, the thickness uniformity improves, and the size and number of pores decreases. With the increase in laser power, the hardness deviation decreases and the average hardness increases. The microstructure of the material is columnar; pores are formed preferentially along the columnar interface. The lath-martensite phase governs the overall microstructure. The volumetric fraction of the retained austenite phase is measured to increase with the increase of laser input power.

• Korean Journal of Metals and Materials
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• v.50 no.6
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• pp.419-425
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• 2012

The purpose of this research was to develop a low Ni austenitic cast iron through replacing Ni by Cu and Mn because they are cheaper than Ni. The effect of the Cu content (6-12 wt%) on the microstructure characteristics was investigated in Fe-3%C-16%(Ni+Cu+Mn) cast iron. Contrary to general effect of the Cu on cast iron, the result of the microstructure analysis indicated that bainite and cementite were formed in high Cu content (>8 wt%Cu). A crystallized Cu-solution (Cu-Mn) phase and MnS in the Cu-solution were formed. The quantity of those phases increased as the Cu content increased. Consequently, the high Cu content in the composition ratio (Ni+Cu+Mn=16%) caused the formation of Cu-Mn/MnS and those phases decreased the effect of Cu and Mn on austenite formation. For this reason, bainite and cementite were formed in high Cu content.

• Journal of Welding and Joining
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• v.18 no.1
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• pp.59-69
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• 2000

The purpose of the present study was to investigate weld metallurgical phenomena such as primary solidification mode, microstructural evolution and hot cracking susceptibility in nitrogen-bearing austenitic stainless steel GTA welds. Eight experimental heats varying nitrogen content from 0.007 to 0.23 wt.% were used in this study. Autogenous GTA welding was performed on weld coupons and the primary solidification mode and their microstructural characteristics were investigated from the fusion welds. Varestraint test was employed to evaluate the solidification cracking susceptibility of the heats and TCL(Total Crack Length) was used as cracking susceptibility index. The solidification mode shifted from primary ferrite to primary austenite with an increase in nitrogen content. Retained delta ferrite exhibited a variety of morphology as nitrogen content varied. The weld fusion zone exhibited duplex structure(austenite+ferrite) at nitrogen contents less than 0.10 wt.% but fully austenitic structure at nitrogen contents more than 0.20 wt.%. The weld fusion zone in alloys with about 0.15 wt.% nitrogen experienced primary austenite + primary ferrite solidification (mode AF) and contained delta ferrite less than 1% at room temperature. Regarding to solidification cracking susceptibility, the welds with fully austenitic structure exhibited high cracking susceptibility while those with duplex structure low susceptibility. The cracking susceptibility increased slowly with an increase in nitrogen content up to 0.20 wt.% but sharply as nitrogen content exceeded 0.20 wt.%, which was attributed to solidification mode shift fro primary ferrite to primary austenite single phase solidification.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.21 no.2
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• pp.267-275
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• 2012

Austenite stainless steel 304 has properties of high resistance to corrosion and temperature changes. Therefore, this material is widely used in various of industries. However, when the material is subjected to heating and cooling cycles the forming accuracy, for example, the right angle associated with a sharp bend such as corner is lost. This phenomenon is caused by the reversion of the deformation-induced martensite into austenite when the temperature in increased. This result in misfit of a structure or an assembly, and an increase in residual stress. Hence, it is important to understand this process. In this study, to evaluate the mechanical behavior of the deformation-induced martensite and reversed austenite, a scanning acoustic spectroscope including the capability of obtaining both phase and amplitude of the ultrasonic wave (i.e., the complex V(z) curve method) was used. Then, the velocities of the SAW propagating within the specimens made in different conditions were measured. The experimental differences of the SAW velocities obtained in this experiment were ranging from 2,750 m/s to 2,850 m/s, and the theoretical difference was 3.6% under the assumption that the SAW velocity was 2,800 m/s. The error became smaller as the martensite content was increased. Therefore, the SAW velocity may be a probe to estimate the marternsite content.

• Journal of the Korean Society for Heat Treatment
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• v.10 no.1
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• pp.1-9
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• 1997

The variation of the mechanical properties and the formation of retained austenite with heat treatment conditions in austempered Si bearing carbon steels has been investigated. In the case of a steel containing 0.35C-1.48Si-0.95Mn, it has been found that a feather shape bainite structure of lath are obtained under a isothermal treated condition at just below the Ms temperature, and the martensite, bainitic ferrite and retained austenite of second phase particles on the ferrite matrix for a isothermal treated steels after intercritical annealing are precipitated in a linked shape. The retained austenite with $2{\mu}m$ size induced as TRIP is found to increase with increasing the formation rate of retained austenite for the intercritical annealing and high Si containing steels. The tensile strength is increased as austempering temperature increases in all isothermal treatment temperature, whereas the elongation is shown to roughly decrease as the tensile strength increases. The values of tensile strength-elongation balance have showed a marked dependence upon the elongation rather than the tensile stregth, and their values are increased for high Si containing steels and intercritical annealing condition. The most optimum result has been shown to be the tensile stregth-elongation balance of $2882.4kgf/mm^2.%$ and the elongation of 33.3% for a "B" steel in the heat treating temperature range of $780{\sim}370^{\circ}C$.

• Journal of Powder Materials
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• v.3 no.3
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• pp.174-180
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• 1996

Microstructure and phase transformation of mechanically alloyed TiNi powders added to aluminium matrix for enhancing the damping properties were studied. Four compositions between 48.5 and 51.5 at% Ti intermetallic compounds were selected to control the fraction of martensite phase. Mechanically alloyed TiNi powders were heat-treated at vacuum of $10^{-6}$ torr for crystallization. Ball milled AI/TiNi composite powders were swaged at room temperature and rolled at 450 $^{\circ}C$. After mechanical alloying for 10 hours, Ti and Ni elements were alloyed completely and amorphous phase was formed. Amorphous phase was crystallized to martensite (Bl9') and austenite(B2) after heat treating for 1 hour at the temperature of 850 $^{\circ}C$, and TiNi$_3$, intermetallic compound was partially formed. Considerable amount of martensite phase was remained after swaging and rolling.

• Journal of Welding and Joining
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• v.26 no.3
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• pp.51-60
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• 2008

This paper is to evaluate fracture characteristics of API 2W Gr.50 TMCP steel weldment typically applied for offshore structures, with the focus on the influence of heat input arising from flux cored arc welding. Based on the results and insights developed from this study, it is found that the toughness for both CTOD and impact exhibits a tendency to decrease as the weld heat input increases. The reheated zone of weldmetal exhibit lower hardness than solidified zone and microstructure that are liable to affect the toughness are acicular ferrite and martensite-austenite constituents (M-A). In particular, M-A is a more effective micro-phase for CTOD toughness than impact toughness.

• Transactions of Materials Processing
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• v.14 no.3 s.75
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• pp.215-223
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• 2005

A numerical analysis program is developed by FDM scheme for the prediction of microstructural transformation during heat treatment of steels. In this study, multi-phase model was used fur description of diffusional austenite transformations in low-alloy hypoeutectoid steels during cooling after austenitization. A fundamental property of the model consisting of coupled differential equations is that by taking into account the rate of austenite grain growth, it permits the prediction of the progress of ferrite, pearlite, and bainite transformations simultaneously during quenching and estimate the amount of martensite also by using K-M eq. In order to simulate the microstructural evolution during tempering process, another Avrami-type eq. was adopted and method for vickers hardness prediction was also proposed. To verify the developed program, the calculated results are compared with experimental ones of casting product. Based on these results, newly designed heat treatment process is proposed and it was proved to be effective for industry.