• Title/Summary/Keyword: Atomic vapor

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Synthesis of Diamond Thin Film by Helicon Plasma Chemical Vapor Deposition

  • Hyun, Jun-Won;Kim, Yong-Kin
    • Transactions on Electrical and Electronic Materials
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    • v.1 no.1
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    • pp.1-5
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    • 2000
  • Diamond films have been achieved on Si(100) substrates using helicon plasma chemical vapor deposition(HPCVD), Gas mixtures with methane and hydrogen have been used. The growth characteristics were investigated by means of X-ray photoelectroton spectroscopy, Atomic force microscopy and X-ray diffraction. We obtained a plasma density as high as 10$\^$10/~10$\^$11/ cm$\^$-3/ by helicon source. The smooth(100) faces of submicron diamond crystallites were found to exhibit pyramidal shaped architecture, The XPS spectrum for the nucleation layer indicates the presence of diamond at 285.4 eV, close to the reported value of 285.5 eV for diamond , XRD results demonstrates the existence of polycrystalline diamond as the diamond (111) and (220) peaks.

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Investigation on HT-AlN Nucleation Layers and AlGaN Epifilms Inserting LT-AlN Nucleation Layer on C-Plane Sapphire Substrate

  • Wang, Dang-Hui;Xu, Tian-Han
    • Journal of the Optical Society of Korea
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    • v.20 no.1
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    • pp.125-129
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    • 2016
  • In this study, we have investigated a high-temperature AlN nucleation layer and AlGaN epilayers on c-plane sapphire substrate by low-pressure metal-organic chemical vapor deposition (LP-MOCVD). High resolution X-ray diffraction (HRXRD), atomic force microscopy (AFM), scanning electron microscope (SEM) and Raman scattering measurements have been exploited to study the crystal quality, surface morphology, and residual strain of the HT-AlN nucleation layer. These analyses reveal that the insertion of an LT-AlN nucleation layer can improve the crystal quality, smooth the surface morphology of the HT-AlN nucleation layer and further reduce the threading dislocation density of AlGaN epifilms. The mechanism of inserting an LT-AlN nucleation layer to enhance the optical properties of HT-AlN nucleation layer and AlGaN epifilm are discussed from the viewpoint of driving force of reaction in this paper.

Crystallographic Relationships of (Ba, Sr) $TiO_3$Thin Film Prepared by Metal-Organic Chemical Vapor Deposition on (111) Textured Pt Electrode

  • Yoo, Dong-Chul;Lee, Jeong-Yong
    • Journal of the Korean Ceramic Society
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    • v.37 no.11
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    • pp.1126-1129
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    • 2000
  • The crystallographic orientations of $Ba_{0.6}$S $r_{0.4}$Ti $O_3$(BST) thin film deposited by a metal-organic chemical vapor deposition on (111) textured Pt electrode were studied with a transmission electron microscopy. The fully crystallized BST thin film (50nm) has (100) and (110) preferred orientations. A high resolution transmission electron microscopy study has revealed the crystallographic orientation relationships between BST thin film and Pt electrode. These relationships explained the preferred orientation of BST film on (111) textured Pt electrode. With these results, we could represent the atomic arrangement at the BST/Pt interface.e.e.

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Hot Filament Chemical Vapor Deposition of Crystalline Boron Films

  • Soto, Gerardo
    • Journal of the Korean Ceramic Society
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    • v.56 no.3
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    • pp.269-276
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    • 2019
  • This article reports on the conditions required for the growth of crystalline boron films on silicon substrates by hot filament chemical vapor deposition method. The reactive gas was 3% diborane diluted in hydrogen. The films were characterized by optical, electronic, and atomic force microscopies; x-ray diffraction; and energy dispersive, electron energy loss, Raman, x-ray photoelectron, and Auger spectroscopies. The parameters that affect the morphologies of the films have been investigated. It was concluded that faceted crystals are produced at low B2H6 flows and working pressures below 200 mT. α-boron is produced between 530 and 600℃. Deposition outside this range produces thin films with a wide variety of morphologies. This result indicates that the films crystallize through a process called "abnormal or discontinuous grain growth." It is assumed that this is due to the anisotropic surfaces of boron allotropes.

Comparative Measurement of Transverse Nuclear Magnetization of Polarized 129Xe and 131Xe by Spin-exchange Optical Pumping

  • Yu, Ye Jin;Min, Seong Ho;Moon, Han Seb
    • Current Optics and Photonics
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    • v.4 no.6
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    • pp.466-471
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    • 2020
  • We analyze the transverse nuclear magnetizations of 129Xe and 131Xe in a vapor cell containing natural Xe, 87Rb, and buffer gases. Th e Xe atoms are polarized th rough spin-exch ange optical pumping (SEOP) with Rb atoms under low-magnetic-field conditions. From the free-induction-decay (FID) signal, we measure the nuclear magnetization of the Xe atoms in the Xe-Rb vapor cell. Furthermore, we measure the dependence of the gyromagnetic ratio on the magnetization of 129Xe and 131Xe by examining the amplitude of the FID signal of each isotope, and we evaluate the relationship between the magnetic field gradient and transverse relaxation rate for both of the 129Xe and 131Xe isotopes.

Investigation of molten fuel coolant interaction phenomena using real time X-ray imaging of simulated woods metal-water system

  • Acharya, Avinash Kumar;Sharma, Anil Kumar;Avinash, Ch.S.S.S.;Das, Sanjay Kumar;Gnanadhas, Lydia;Nashine, B.K.;Selvaraj, P.
    • Nuclear Engineering and Technology
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    • v.49 no.7
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    • pp.1442-1450
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    • 2017
  • In liquid metal fast breeder reactors, postulated failures of the plant protection system may lead to serious unprotected accidental consequences. Unprotected transients are generically categorized as transient overpower accidents and transient under cooling accidents. In both cases, core meltdown may occur and this can lead to a molten fuel coolant interaction (MFCI). The understanding of MFCI phenomena is essential for study of debris coolability and characteristics during post-accident heat removal. Sodium is used as coolant in liquid metal fast breeder reactors. Viewing inside sodium at elevated temperature is impossible because of its opaqueness. In the present study, a methodology to depict MFCI phenomena using a flat panel detector based imaging system (i.e., real time radiography) is brought out using a woods metal-water experimental facility which simulates the $UO_2-Na$ interaction. The developed imaging system can capture attributes of the MFCI process like jet breakup length, jet front velocity, fragmented particle size, and a profile of the debris bed using digital image processing methods like image filtering, segmentation, and edge detection. This paper describes the MFCI process and developed imaging methodology to capture MFCI attributes which are directly related to the safe aspects of a sodium fast reactor.

DEVELOPMENT OF A WALL-TO-FLUID HEAT TRANSFER PACKAGE FOR THE SPACE CODE

  • Choi, Ki-Yong;Yun, Byong-Jo;Park, Hyun-Sik;Kim, Hee-Dong;Kim, Yeon-Sik;Lee, Kwon-Yeong;Kim, Kyung-Doo
    • Nuclear Engineering and Technology
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    • v.41 no.9
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    • pp.1143-1156
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    • 2009
  • The SPACE code that is based on a multi-dimensional two-fluid, three-field model is under development for licensing purposes of pressurized water reactors in Korea. Among the participating research and industrial organizations, KAERI is in charge of developing the physical models and correlation packages for the constitutive equations. This paper introduces a developed wall-to-fluid heat transfer package for the SPACE code. The wall-to-fluid heat transfer package consists of twelve heat transfer subregions. For each sub-region, the models in the existing safety analysis codes and the leading models in literature have been peer reviewed in order to determine the best models which can easily be applicable to the SPACE code. Hence a wall-to-fluid heat transfer region selection map has been developed according to the non-condensable gas quality, void fraction, degree of subcooling, and wall temperature. Furthermore, a partitioning methodology which can take into account the split heat flux to the continuous liquid, entrained droplet, and vapor fields is proposed to comply fully with the three-field formulation of the SPACE code. The developed wall-to-fluid heat transfer package has been pre-tested by varying the independent parameters within the application range of the selected correlations. The smoothness between two adjacent heat transfer regimes has also been investigated. More detailed verification work on the developed wall-to-fluid heat transfer package will be carried out when the coupling of a hydraulic solver with the constitutive equations is brought to completion.

In-service Investigation on the Flow Dynamics of a Trayed Column from the Measurement of an Internal Density by using a Gamma Absorption Technique (Gamma Absorption Technique를 이용한 Trayed Column의 가동 중 내부 밀도분포 측정에 의한 유체 유동상태 진단)

  • Kim, Jae-Ho;Kim, Jong-Bum;Kim, Jin-Seop;Lee, Na-Young;Lee, Sung-Sik;Jang, Seok-Joon;Jung, Sung-Hee
    • Journal of Radiation Protection and Research
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    • v.33 no.1
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    • pp.35-40
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    • 2008
  • A distillation tower is one of the important facilities which separates and refines a crude oil stream according to certain boiling points. Its operation efficiency can affect the productivity of a refinery substantially. The objective of this study is to elucidate some operational information on the internal conditions of a distillation tower from a measurement of density profile by using a sealed gamma-ray source and a radiation detector. Gamma radiation counts were measured by a BGO detector positioned diametrically outside the tower-wall, opposite to the gamma source(Co-60) as the detector and the source were lowered concurrently. From the results, structural abnormality of the trays was not found inside the tower. Considering the flow distribution patterns, however, a vapor phase was dominantly formed at the upper part of the tower and a liquid phase at the lower part. From the gamma scanning of the distillation tower, it is anticipated that the gamma absorption technique can be used as an important tool for confirming the structural soundness of trays and investigating flow distribution in refinery facilities.

Comparison of Cold Vapor Atomic Absorption Spectrophotometry Analysis and EPA Method 101A for Measurement of Mercury in the Flue Gas (배출가스중 수은 측정을 위한 환원기화 원자흡광광도법과 EPA Method 101A의 비교 연구)

  • 김경희;최양일;박일수;홍지형;차준석;석광설;김대곤
    • Proceedings of the Korea Air Pollution Research Association Conference
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    • 1999.10a
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    • pp.92-93
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    • 1999
  • 수은은 상온에서 액체상태로 존재하는 유일한 금속으로서, 증기압이 매우 높기 때문에 가장 쉽게 휘발될 수 있는 중금속이다. 다른 중금속들은 거의 입자 상태로 변환되기 때문에 전기 집진기 등과 같은 일반적인 입자 제어시설에서 98%이상이 제거되지만, 증기압이 매우 높은 수은은 다단계 습식 스크러버, 활성탄을 사용하는 전기집진기/습식 스크러버가 결합된 특정한 방지시설에 없는 한 거의 대부분이 그대로 배출된다.(중략)

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Ultra-shallow Junction with Elevated SiCe Source/ Drain fabricated by Laser Induced Atomic Layer Doping (레이저 유도 원자층 도핑(Ll-ALD)법으로 성장시킨 SiGe 소스/드레인 얕은 접합 형성)

  • 장원수;정은식;배지철;이용재
    • Proceedings of the IEEK Conference
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    • 2002.06b
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    • pp.29-32
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    • 2002
  • This paper describes a novel structure of NMOSFET with elevated SiGe source/drain region and ultra-shallow source/drain extension(SDE)region. A new ultra-shallow junction formation technology. Which is based on damage-free process for rcplacing of low energy ion implantation, is realized using ultra-high vacuum chemical vapor deposition(UHVCVD) and excimer laser annealing(ELA).

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