• Title/Summary/Keyword: Atomic resolution

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A Simulation Study of Atomic Resolution TEM images for Two Dimensional Single Layer and Bilayer Graphene Crystal (2차원적인 단층 및 복층 그래핀 결정에 대한 원자분해 투과전자현미경 영상 시뮬레이션 연구)

  • Kim, Hwang-Su
    • Applied Microscopy
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    • v.40 no.1
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    • pp.21-28
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    • 2010
  • In a simulation study of atomic resolution transmission electron microscope images of single layer and bilayer graphene, it is demonstrated that the conventional Bloch wave formulations can be used when high-order Laue zone reflections are properly taken into account in the theory. The simulated images for bilayer graphene show 3-fold rotational lattice symmetry rather than the 6-fold one under certain conditions. This result can be understood as revealed the 3-fold rotational lattice symmetry of bilayer graphene in three dimensions along [0001]. For single layer graphene the observed phase images showing 3-fold rotational lattice symmetry were particularly noted. This phenomenon has been explained by an assumption of the re-configuration of electron density on the surface of graphene. And the matching images have been obtained as simulated with up to the second order Laue zone reflections only, reflecting the re-configuration of electrons on the surface.

MEASUREMENT OF NUCLEAR FUEL ROD DEFORMATION USING AN IMAGE PROCESSING TECHNIQUE

  • Cho, Jai-Wan;Choi, Young-Soo;Jeong, Kyung-Min;Shin, Jung-Cheol
    • Nuclear Engineering and Technology
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    • v.43 no.2
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    • pp.133-140
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    • 2011
  • In this paper, a deformation measurement technology for nuclear fuel rods is proposed. The deformation measurement system includes a high-definition CMOS image sensor, a lens, a semiconductor laser line beam marker, and optical and mechanical accessories. The basic idea of the proposed deformation measurement system is to illuminate the outer surface of a fuel rod with a collimated laser line beam at an angle of 45 degrees or higher. For this method, it is assumed that a nuclear fuel rod and the optical axis of the image sensor for observing the rod are vertically composed. The relative motion of the fuel rod in the horizontal direction causes the illuminated laser line beam to move vertically along the surface of the fuel rod. The resulting change of the laser line beam position on the surface of the fuel rod is imaged as a parabolic beam in the high-definition CMOS image sensor. An ellipse model is then extracted from the parabolic beam pattern. The center coordinates of the ellipse model are taken as the feature of the deformed fuel rod. The vertical offset of the feature point of the nuclear fuel rod is derived based on the displacement of the offset in the horizontal direction. Based on the experimental results for a nuclear fuel rod sample with a formation of surface crud, an inspection resolution of 50 ${\mu}m$ is achieved using the proposed method. In terms of the degree of precision, this inspection resolution is an improvement of more than 300% from a 150 ${\mu}m$ resolution, which is the conventional measurement criteria required for the deformation of neutron irradiated fuel rods.

Development of hand-held coded-aperture gamma ray imaging system based on GAGG(Ce) scintillator coupled with SiPM array

  • Jeong, Manhee;Hammig, Mark
    • Nuclear Engineering and Technology
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    • v.52 no.11
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    • pp.2572-2580
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    • 2020
  • Emerging gamma ray detection applications that utilize neutron-based interrogation result in the prompt emission of high-energy (>2 MeV) gamma-rays. Rapid imaging is enabled by scintillators that possess high density, high atomic number, and excellent energy resolution. In this paper, we evaluate the bright (50,000 photons/MeV) oxide scintillator, cerium-doped Gd2Al2Ga3O12 (GAGG(Ce)). A silicon photomultiplier (SiPM) array is coupled to a GAGG(Ce) scintillator array (12 × 12 pixels) and integrated into a coded-aperture based gamma-ray imaging system. A resistor-based symmetric charge division circuit was used reduce the multiplicity of the analog outputs from 144 to 4. The developed system exhibits 9.1%, 8.3%, and 8.0% FWHM energy resolutions at 511 keV, 662 keV, and 1173.2 keV, respectively. In addition, a pixel-identification resolution of 602 ㎛ FWHM was obtained from the GAGG(Ce) scintillator array.

The Electrical Conductivity and Electrochemical Characteristics of Amphiphilic Milecules Multilayer Film confined with Hetero Type (양친매성 다중층막의 전기적 도전성 및 전기적 특성)

  • 최인희;박수길;임기조;이주성
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1996.05a
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    • pp.269-272
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    • 1996
  • The electrochemical behavior of Ru complex and PD complex monolayer, deposited on conductive substrate by the Langmuir-Blodgett(LB) technique as monolayer and multilayer, has been studied by cyclic voltammetry. Monolayer films show stable reversible state. Atomic resolution imaging of LB highly-conductive, environmently stable organic films has been obtained by atomic force microscopy (AFM) showing their closely packed structure,

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Commissioning of neutron triple-axis spectrometers at HANARO

  • Hiraka, Haruhiro;Lee, Jisung;Jeon, Byoungil;Seong, Baek-Seok;Cho, Sangjin
    • Nuclear Engineering and Technology
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    • v.52 no.9
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    • pp.2138-2150
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    • 2020
  • We report the status of the cold neutron triple-axis spectrometer (Cold TAS) and thermal neutron triple-axis spectrometer (Thermal TAS) installed at HANARO. Cold TAS, whose specifications are standard across the world, is in the final phase of commissioning. Proper instrument operation was confirmed through a feasibility study of phonon measurements and data analyses with resolution convolution. In contrast, Thermal TAS is in the initial phase of commissioning, and improvement of the monochromator drum is now in progress from the viewpoint of radiation shielding. In addition, we report recent activities in the development of neutron basic elements, that is, film-coated Si-wafer collimators, which are promising for use in triple-axis spectroscopy, particularly in Cold TAS.

Cold Atomic Beam Extracted by Zeeman Effect (제만 효과를 이용한 저온 원자빔)

  • Kim, Kihwan;Noh, Heung-Ryoul;Wonho Jhe
    • Proceedings of the Optical Society of Korea Conference
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    • 2001.02a
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    • pp.250-251
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    • 2001
  • There is a considerable interest in the generation of a cold atomic beam having a narrow velocity spread that can be used in various experiments in physics such as ultrahigh resolution atomic and molecular spectroscopy, atom optics, atom interferometry, study of solid surfaces, and low energy collision experiments. The invention of the techniques of laser cooling has stimulated developments in the production of cold and bright atomic beams. (omitted)

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Retention Behavior of Transition Metal ions with Some Complexing Agents on Cation Exchanger

  • Park, Yang-Soon;Joe, Kih-Soo;Lee, Gae-Ho;Han, Sun-Ho;Eom, Tae-Yoon
    • Bulletin of the Korean Chemical Society
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    • v.14 no.6
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    • pp.692-696
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    • 1993
  • Prediction of retention times in transition metal-mandelate and transition metal-tartrate complex systems were studied on the cation exchanger. Plots of k' vs [mandelate] and k' vs [tartrate] were obtained under the condition of a constant competing cation concentration. The equation to predict the retention time of transition metal ion was derived from the ion exchange equilibria. Individual capacity factors (${k_1}',\;{k_2}'$) and stability constants ($K_1,\;K_2$) of the complexes were calculated from the non-linear least square method. Good resolution of the transition metals was predicted by the stepwise equation in the gradient method. The values of retention times from the calculation and the experiment agreed well each other.

INVESTIGATIONS ON THE RESOLUTION OF SEVERE ACCIDENT ISSUES FOR KOREAN NUCLEAR POWER PLANTS

  • Kim, Hee-Dong;Kim, Dong-Ha;Kim, Jong-Tae;Kim, Sang-Baik;Song, Jin-Ho;Hong, Seong-Wan
    • Nuclear Engineering and Technology
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    • v.41 no.5
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    • pp.617-648
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    • 2009
  • Under the government supported long-term nuclear R&D program, the severe accident research program at KAERI is directed to investigate unresolved severe accident issues such as core debris coolability, steam explosions, and hydrogen combustion both experimentally and numerically. Extensive studies have been performed to evaluate the in-vessel retention of core debris through external reactor vessel cooling concept for APR1400 as a severe accident management strategy. Additionally, an improvement of the insulator design outside the vessel was investigated. To address steam explosions, a series of experiments using a prototypic material was performed in the TROI facility. Major parameters such as material composition and void fraction as well as the relevant physics affecting the energetics of steam explosions were investigated. For hydrogen control in Korean nuclear power plants, evaluation of the hydrogen concentration and the possibility of deflagration-to-detonation transition occurrence in the containment using three-dimensional analysis code, GASFLOW, were performed. Finally, the integrated severe accident analysis code, MIDAS, has been developed for domestication based on MELCOR. The data transfer scheme using pointers was restructured with the modules and the derived-type direct variables using FORTRAN90. New models were implemented to extend the capability of MIDAS.

SEPARATION OF GAMMA-RAYS PRODUCTION FROM $^{13}C(p,\;{\gamma})^{14}N,\;^{14}N({\gamma},\;{\gamma})^{14}N$ REACTIONS USING DOPPLER SHIFT EFFECT

  • Kim, Y.K.;Ha, J.H.;Youn, M.;Han, S.H.;Chung, C.E.;Moon, B.S.
    • Journal of Radiation Protection and Research
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    • v.26 no.3
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    • pp.287-290
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    • 2001
  • The 9.17MeV gamma-rays from the $^{13}C(p,\;{\gamma})^{14}N,\;^{14}N({\gamma},\;{\gamma})^{14}N$ reactions were measured. The incident 9.17MeV gamma-ray was produced from the $^{13}C(p,\;{\gamma})^{14}N$ reaction at Ep=1.75MeV resonance. The 1.75MeV proton beam was accelerated using the 3MV SNU-AMS Tandetron and 1.7MV KIGAM Tandem accelerators. The enriched 13C target was $121{\mu}g/cm^2$ self-supporting foil, and we used liquid nitrogen as a resonant absorption target. We used a HP-Ge detector with 30% efficiency and less 2keV energy resolution. We developed new method to detect the scattered 9.17MeV gamma-ray from the nitrogen target by using the energy difference between the Doppler shifted gamma-ray from the $^{13}C(p,\;{\gamma})^{14}N$ reaction and the resonant absorbed and rescattered gamma-ray from the $^{14}N({\gamma},\;{\gamma})^{14}N$ reaction.

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Microstructural characterization of accident tolerant fuel cladding with Cr-Al alloy coating layer after oxidation at 1200 ℃ in a steam environment

  • Park, Dong Jun;Jung, Yang Il;Park, Jung Hwan;Lee, Young Ho;Choi, Byoung Kwon;Kim, Hyun Gil
    • Nuclear Engineering and Technology
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    • v.52 no.10
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    • pp.2299-2305
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    • 2020
  • Zr alloy specimens were coated with Cr-Al alloy to enhance their resistance to oxidation. The coated samples were oxidized at 1200 ℃ in a steam environment for 300 s and showed extremely low oxidation when compared to uncoated Zr alloy specimens. The microstructure and elemental distribution of the oxides formed on the surface of Cr-Al alloys have been investigated by transmission electron microscopy (TEM) and X-ray photoelectron spectroscopy (XPS). A very thin protective layer of Cr2O3 formed on the outer surface of the Cr-Al alloy, and a thin Al2O3 layer was also observed in the Cr-Al alloy matrix, near the surface. Our results suggest that these two oxide layers near the surface confers excellent oxidation resistance to the Cr-Al alloy. Even after exposure to a high temperature of 1200 ℃, inter-diffusion between the Cr-Al alloy and the Zr alloy occurred in very few regions near the interface. Analysis of the inter-diffusion layer by high-resolution transmission electron microscopy (HRTEM) and energy dispersive X-ray spectroscopy (EDS) measurement confirmed its identity as Cr2Zr.