• Title/Summary/Keyword: Area of particle

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Effect of Reaction Factors on the Fabrication of Nano-Sized Indium Oxide Powder by Spray Pyrolysis Process (분무열분해공정에 의한 인듐 산화물 나노 분말 제조에 미치는 반응인자들의 영향)

  • Yu Jae-Keun
    • Journal of Powder Materials
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    • v.11 no.6 s.47
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    • pp.493-502
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    • 2004
  • In this study, nano-sized indium oxide powder with the average particle size below 100 nm is fab-ricated from the indium chloride solution by the spray pyrolysis process. The effects of the reaction temperature, the concentration of raw material solution and the inlet speed of solution on the properties of powder were studied. As the reaction temperature increased from 850 to $1000^{\circ}C$, the average particle size of produced powder increased from 30 to 100 nm, and microstructure became more solid, the particle size distribution was more irregular, the intensity of a XRD peak increased and specific surface area decreased. As the indium concentration of the raw material solution increased from 40 to 350 g/l, the average particle size of the powder gradually increased from 20 to 60 nm, yet the particle size distribution appeared more irregular, the intensity of a XRD peak increased and spe-cific surface area decreased. As the inlet speed of solution increased from 2 to 5 cc/min., the average particle size of the powder decreased and the particle size distribution became more homogeneous. In case of the inlet speed of 10 cc/min, the average particle size was larger and the particle size distribution was much irregular compared with the inlet speed of 5 cc/min. As the inlet speed of solution was 50 cc/min, the average particle size was smaller and microstructure of the powder was less solid compared with the inlet speed of 10 cc/min. The intensity of a XRD peak and the variation of specific area of the powder had the same tendency with the variation of the average par-ticle size.

Mobile Object Tracking Algorithm Using Particle Filter (Particle filter를 이용한 이동 물체 추적 알고리즘)

  • Kim, Se-Jin;Joo, Young-Hoon
    • Journal of the Korean Institute of Intelligent Systems
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    • v.19 no.4
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    • pp.586-591
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    • 2009
  • In this paper, we propose the mobile object tracking algorithm based on the feature vector using particle filter. To do this, first, we detect the movement area of mobile object by using RGB color model and extract the feature vectors of the input image by using the KLT-algorithm. And then, we get the first feature vectors by matching extracted feature vectors to the detected movement area. Second, we detect new movement area of the mobile objects by using RGB and HSI color model, and get the new feature vectors by applying the new feature vectors to the snake algorithm. And then, we find the second feature vectors by applying the second feature vectors to new movement area. So, we design the mobile object tracking algorithm by applying the second feature vectors to particle filter. Finally, we validate the applicability of the proposed method through the experience in a complex environment.

Pore Characteristics of Porous Alumina Ceramics Fabricated from Boehmite Hydrosol and Alumina Particles (Boehmite 수화졸의 알루미나로 제조한 다공성 알루미나 세라믹스의 기공특성)

  • 오경영
    • Journal of the Korean Ceramic Society
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    • v.33 no.5
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    • pp.547-555
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    • 1996
  • Porous alumina ceramics were fabricated by pseudo-boehmite phydosol-gel process within/without commercial $\alpha$-alumina particles average 1 and 40 micron respectively. The pore characteristics of fired specimens were studied by the measurement of bulk density total porosity thyermal analysis pore volume pore distribution BET area XRD and SEM. with increasing of firing temperature pore volume and BET surface area were decreased and the average pore size was increased to approximately 146$\AA$ upto 80$0^{\circ}C$ by de-watering of [OH] and formation of $\alpha$-alumina. The fired relative density of the alumina-dispersed specimen with average 1 micron particle was increased with the amounts of dispersed particle by bimodal packing theory which is compared to the ones of specimen including of average 40 micron particle. It was confirmed that the percola-tion threshold in porous ceramics with coarser particle (40 micron) has formed between the transformed-alumina from hydrogel and dispersed-alumina of above 50 vol% particle and the total porosity was increased at the threshold point above.

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Numerical Simulation for Dispersion of Anthropogenic Pollutant in Northern Masan Bay using Particle Tracking Model (입자추적모델을 이용한 마산만 북부 해역에서의 육상오염물질 확산 수치모의)

  • KIM, Jin-Ho;JUNG, Woo-Sung;HONG, Sok-Jin;LEE, Won-Chan;CHUNG, Yong-Hyun;KIM, Dong-Myung
    • Journal of Fisheries and Marine Sciences Education
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    • v.28 no.4
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    • pp.1143-1151
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    • 2016
  • To study the dispersion process and residence time of anthropogenic pollutant in Masan bay, a three-dimensional hydrodynamic model coupled to a particle tracking model, EFDC, is applied. Particle tracking model simulated the instantaneous release of particles emulating discharge from river and wastewater treatment plant to show the behaviour of pollutant in terms of water circulation and water exchange. Modelled outcomes for water circulation were in good agreement with tidal elevation and current data. The results of particle tracking model show that over half of particles released from northern Masan bay transport to out of area while the particles from Dukdong wastewater treatment plant transport to northern area. This meant pollution source from inside and outside of the northern area can affect water quality of northern Masan bay.

Effects of Particle Shapes on Unipolar Diffusion Charging of Non-Spherical Particles (비구형 입자의 형상에 따른 단극 확산 하전 특성)

  • Oh, Hyun-Cheol;Park, Hyung-Ho;Kim, Sang-Ho
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.28 no.5
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    • pp.501-509
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    • 2004
  • Unipolar diffusion charging of non-spherical particles was investigated for various particle shapes. We researched with TiO$_2$agglomerates produced by the thermal decomposition of titanium tetraisopropoxide (TTIP) vapor. TTIP was converted into TiO$_2$, in the furnace reactor and was subsequently introduced into the sintering furnace. Increasing the temperature in the sintering furnace, aggregates were restructured into higher fractal dimensions. The aggregates were classified according to their mobility using a differential mobility analyzer. The projection area and the mass fractal dimension of particles were measured with an image processing technique performed by using transmission electron microscope (TEM) photograph. The selected aggregates were charged by the indirect photoelectric-charger and the average number of charges per particle was measured by an aerosol electrometer and a condensation particle counter. For the particles of same mobility diameter, our results showed that the particle charge quantity decreases as the sintering temperature increases. This result is understandable because particles with lower fractal dimension have larger capacitance and geometric surface area.

Influence of Heat-treatment on Physical Properties of Nanocrystalline Indium Tin Oxide (ITO) Particle (나노급 인듐 주석 산화물 입자의 물성에 미치는 열처리의 영향)

  • 홍성제;한정인;정상권
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.17 no.7
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    • pp.747-753
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    • 2004
  • In this paper, nanocrystalline indium tin oxide (ITO) particles were fabricated by using synthesis without harmful elements. The synthetic method is to eliminate the chloridic and nitridic elements which are included in the current wet type synthetic method. Therefore, it is possible to lower synthetic temperature below 600 $^{\circ}C$ to eliminate the harmful elements. Accordingly, fine particle can be achieved by applying the process. Particle size, surface area, crystal structure, and composition ratio of the synthesized nanocrystalline ITO particle by using the method were analyzed with high resolution transmission electron microscopy (HRTEM), BET surface area analyzer, X-ray diffraction (XRD), and energy dispersion spectroscopy (EDS). As a result, its particle size is less than 10 nm, and the surface area exceeds 100 m$^2$/g. The XRD analysis indicates that the cystal structure of the powder is cubic one with orientation of <222>, <400>, <440>. Also, the analysis of the composition demonstrates that the around 8 wt% tin is uniformly included in In$_2$O$_3$ lattice of the nanoparticle.

Pore-Controlled Synthesis of Mesoporous Silica Particles by Spray Pyrolysis from Aqueous Silicic Acid (규산 수용액으로부터 분무열분해법에 의한 기공 특성이 제어된 메조기공의 다공성 실리카 분말 합성)

  • Chang, Han Kwon;Lee, Jin Woo;Oh, Kyoung Joon;Jang, Hee Dong;Kil, Dae Sup;Choi, Jeong Woo
    • Particle and aerosol research
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    • v.8 no.2
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    • pp.89-95
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    • 2012
  • Spherical mesoporous silica particles, of which main pore diameter was 3.8 nm, were successfully prepared by spray pyrolysis from aqueous silicic acid. The effect of precursor concentration, reaction temperature, and the addition of urea and PEG on the particle diameter and pore properties such as pore diameter, total pore volume, and specific surface area were investigated by using FE-SEM, particle size analyzer, and nitrogen absorption-desorption analysis. With an increase of the precursor concentration from 0.2 M to 0.7 M, the average particle diameter, total pore volume, and specific surface area of the porous silica particles increased from 0.56 to $0.96\;{\mu}m$, 0.434 to $0.486\;cm^3/g$, 467.8 to $610.4\;m^2/g$, respectively. Within the temperature range $(600\;^{\circ}C{\sim}800\;^{\circ}C)$, there was no significant difference in the pore diameter, total pore volume, and specific surface area. In addition, the addition of urea as an expansion aid led to slight increases in particle diameter, pore diameter, and specific surface area. However, when the polyethylene glycol (PEG) as an organic template was used, the total pore volume of porous particles increased dramatically.

Fabrication of Nano-Sized Ni-ferrite Powder from Waste Solution Produced by Shadow Mask Processing (새도우마스크 제조공정 중 발생되는 폐액으로부터 니켈 페라이트 나노 분말 제조)

  • 유재근;서상기
    • Journal of Powder Materials
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    • v.10 no.4
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    • pp.262-269
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    • 2003
  • Nano-sized Ni-ferrite powder was fabricated by spray pyrolysis process using the waste solution resulting from shadow mask processing. The average particle size of the powder was below 100 nm. The effects of the concentration of raw material solution, the nozzle tip size and air pressure on the properties of powder were studied. As the concentration increased, the average particle size of the powder gradually increased and its specific surface area decreased, but size distribution was much wider and the fraction of the Ni-ferrite phase greatly increased as the concentration increasing. As the nozzle tip size increased from 1 mm to 2 mm, the average particle size of the powder decreased. In case of 3 mm nozzle tip size, the average particle size of the powder increased slightly. On the other hand, in case of 5 mm nozzle tip size, average particle size of the powder decreased. Size distribution of the powder was unhomogeneous, and the fraction of the Ni-ferrite phase decreased as the nozzle tip size increasing. As air pressure increased up to 1 kg/$cm^2$, the average particle size of the powder decreased slightly, on the other hand, the fraction of the Ni-ferrite phase was almost constant. In case of 3kg/$cm^2$ air pressure, average particle size of the powder and the fraction of the Ni-ferrite phase remarkably decreased, but size distribution was narrow.

A PTV Applied to Measuring the Solid Particle Velocity of Slurry Flow in a Vertical Pipe (PTV를 이용한 수직관 내 슬러리유동의 고체입자 속도계측 연구)

  • Yang, Chan-Kyu;Choi, Jong-Su;Hong, Sup
    • Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
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    • 2001.10a
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    • pp.213-219
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    • 2001
  • In this paper, particle velocity of slurry flow, a kind of solid-particle two phase flow, was measured by using a particle tracking velocimetry. Particles are modeled by sphere-shaped glass whose diameters are 3mm, 5mm, and 7mm At first, a particle which is falling in the water is captured and analyzed to give their free falling velocity. The falling velocity was very high up to about 4m/sec in the air, which needs special algorithm for the accurate measurement. For the upwelling slurry flow in the straight duct, there are some noises caused by cavity. However, the effect was so small that it does not affect the measurement of large particles. From the preliminary study of applying the PTV to measurement of particle movement in slurry flow, we could find out the optimum value of parameters: threshold value., searching area radius and correlation area size.

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Simultaneous Measurement of Fluid Velocity and Particle Velocity in a Particle-Containing Fluid Flow (입자가 포함된 유동장에서 유체속도와 입자속도의 동시 측정기법)

  • Jin Dong-Xu;Lee Dae-Young;Lee Yoon-Pyo
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.17 no.4
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    • pp.355-363
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    • 2005
  • A novel method for simultaneously measuring the fluid velocity and the large particle velocity in a particle-containing fluid flow is developed in this study. In this method, the fluid velocity and the large particle velocity are measured by PIV and PTV, respectively. The PIV and PTV images are obtained from the same flow images. Since a PIV result represents the average displacement of all particles in an interrogation area, it will include an error caused by the relative displacement between the large particles and the fluid. In order to reduce the false influence of large particles on the PIV calculation, the mean brightness of small PIV particle images is substituted to the locations of large particles in the PIV images. The simulation results showed that the new method significantly reduces the PIV error caused by the large particles even at the case where the large particles occupy area fraction as large as $20\%$ of the full image.