• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2006년도 춘계학술대회 논문집
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• pp.57-58
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• 2006

The effects of lowering ECAP temperature during ECAP process and Post-ECAP annealing on microstructure, texture and mechanical properties of the AZ31 alloys have been investigated in the present study. The as-extruded materials were ECAP processed to 2 passes at 553K prior to subsequent pressing up to 6 passes at 523K or 493K. When this method of lowering ECAP temperature during ECAP was used, the rods could be successfully deformed up to 6 passes without any surface cracking. Grain refinement during ECAP process at 553K might have helped the material to endure further straining at lower deformation temperatures probably by increasing the strain accommodation effect by grain boundary sliding, causing stress relaxation. Texture modification during ECAP has a great influence on the strength of Mg alloys because HCP metals have limited number of slip systems. As slip is most prone to take place on basal planes in Mg at room temperature, the rotation of high fraction of basal planes to the directions favorable for slip as in ECAP decreases the yield stress appreciably. The strength of AZ31 Mg alloys increases with decrease of grain size if the texture is constant though ECAP deformation history is different. A standard positive strength dependence on the grain size for Mg alloys with the similar texture (Fig. 1) supports that the softening of ECAPed Mg alloys (a negative slope) typically observed despite the significant grain refinement is due to the texture modification where the rotation of basal planes occurs towards the orientation for easier slip. It could be predicted that if the original fiber texture is restored after ECAP treatment yielding marked grain refinement, yield stress as high as 500 MPa will be obtained at the grain size of ${\sim}1{\mu}m$. Differential speed rolling (DSR) with a high speed ratio between the upper and lower rolls was applied to alter the microstructure and texture of the AZ31 sheets. Significant grain refinement took place during the rolling owing to introduction of large shear deformation. Grain size as small as $1.4{\mu}m$ could be obtained at 423K after DSR. There was a good correlation between the (0002) pole intensity and tensile elongation. This result indicates that tensile ductility improvement in the asymmetrically rolled AZ31 Mg alloys is closely related to the weakening of basal texture during DSR. Further basal texture weakening occurred during annealing after DSR. According to Hall-Petch relation shown in Fig. 1, the strength of the asymmetrically rolled AZ31 is lower than that of the symmetrically rolled one when compared at the same grain size. This result was attributed to weakening of fiber texture during DSR. The DSRed AZ31, however, shows higher strength than the ECAPed AZ31 where texture has been completely replaced by a new texture associated with high Schmid factors.

• 한국자동차공학회논문집
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• 제13권6호
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• pp.128-134
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• 2005

In order to fabricate the aluminum alloys with good drawability, the textures evolution of the AA5182 sheets after rolling and annealing was studied. The measurement of the deformation textures was carried out for the sheets which were cold rolled with high reduction ratio by using the symmetric roll. In addition, the change of the recrystallization texture was investigated after heat-treatments of the rolled sheets with various heat treatment conditions. Rolling without lubrication and subsequent annealing led to the formation of favorable $rot-C_{ND}\;\{001\}<110>\;and\;{\gamma}-fiber ND//<111>$ textures in AA5182 sheets. From the results, the ${\gamma}$-fiber ND//<111> component well evolved during rolling at highest reduction ratio (over $90\%$, l/d parameter of 6.77). Among shear deformation textures, the ${\gamma}$-fiber ND//<111> was not rotated in holding time of $180\~7,200$ seconds at $350^{\circ}C$. The Monte-Carlo technique was used and could be representatively simulated these textures evolution during recrystallization.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2001년도 춘계학술대회 논문집
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• pp.176-179
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• 2001

A simple cold pressing procedure which allows shear deformations on sheet metals is proposed by designing dies with grooves and applied to aluminum 3003 sheets. shear deformation led to the formation of preferred orientation along <100>//RD, and the effect of initial tortures on the formation of shear textures was also studied Rectangular shaped dislocation cells formed in the deformed microstructure and boundaries of dislocation cells gradually rounded with the increased plastic strain. Upon subsequent annealing textures inherited deformation textures. Recrystallized grains consisted of a large number of fully recovered subgrains with well defined boundaries which persisted even after annealing at a higher temperature.

• 한국초전도학회:학술대회논문집
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• 한국초전도학회 1999년도 High Temperature Superconductivity Vol.IX
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• pp.292-295
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• 1999

We investigated the effects of Pd impurities on cube-textures in cold rolled and recrystallized PtPd tapes The sample were made from Pt$_{1-x}Pd_x$ alloys (x from 0 to0.34) by rolling at low temperature. The thickness of the tapes were about 100 ${\mu}$m. The PtPd[111] pole figures of X-ray Diffraction for all the samples indicated similar deformed textures. But the recrystallized textures after annealing showed that a better cube texture was formed in the sample of larger x. The final textures were sensitive to annealing time and temperature when x was increased.

• 한국초전도저온공학회:학술대회논문집
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• 한국초전도저온공학회 2003년도 학술대회 논문집
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• pp.72-74
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• 2003

We fabricated textured Ag substrates for coated conductor and evaluated the effects of annealing temperature on microstructural evolution, texture formation, and surface morphology. A strong {110}〈110〉 textured Ag substrate was obtained by cold rolling and annealing at 80$0^{\circ}C$: the full-width at half-maximum(FWHM) value of {110}〈110〉 poles was as sharp as 10$^{\circ}$. Surface morphology was evaluated by using Atomic force microscopy(AFM). Root-mean-square(RMS) roughness of the substrate annealed at 80$0^{\circ}C$ was 39.2 nm. The substrate of strong texture and smooth surface, fabricated in our study, is considered to be suitable for use as a substrate for deposition of superconductor films.

• 동력기계공학회지
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• 제22권1호
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• pp.87-93
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• 2018

Specimens were machined out from hot-rolled AZ31 magnesium alloy, and deformed at 623K with rolling reduction of 30%. After hot rolling, specimens were annealed at various range of temperature and time. In this study, static recrystallization was occurred during heat treatment, however, variation of main component and intensity of texture was not revealed. The results of microstructure observation, damping capacity test and dislocation mechanism indicated that increasing of damping capacity was caused by grain growth. It means that grain size is effective factor to damping capacity.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 1997년도 추계학술대회논문집
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• pp.198-201
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• 1997

Aluminum alloy sheets are considered as one of the high potential substitutes for steel sheets considering weight reduction of automobiles. However, aluminum alloy sheets have drawbacks in higher prices and inferior formability compared to steel sheets. In order to achieve good deep drawability, it is imperative to obtain well developed {111} texture which gives rise to higher plastic strain ratio. It is difficult to obtain this texture from conventional rolling and annealing processes. Therefore, an unconventional rolling process which enhances shear deformation has been experimentally studied to obtain the well developed {111} texture, which in turn gives rise to a substantial increase in plastic strain ratio.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2008년도 춘계학술대회 논문집
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• pp.408-410
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• 2008

The evolution of texture and microstructure during recrystallization was tracked after different cold rolling of aluminum sheets. Texture of the sheet center were differentiated by different strain states due to prior deformation. The evolution of recrystallization texture was studied with the amount of shear applied during cold rolling. The final grain size after recrystallization annealing was varied due to the effective strain during deformation.

• 한국정밀공학회지
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• 제28권9호
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• pp.1086-1093
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• 2011

To fabricate the aluminum alloys with good drawability, the textures evolution of the AA5182 sheets due to the change of lid parameter after rolling and subsequent annealing was studied. The measurement of the deformation textures was carried out for the sheets with high reduction ratio and the change of the recrystallization texture was investigated after heat-treatments of the rolled sheets in various I/d parameters. Rolling without lubrication and subsequent annealing led to the formation of favorable rot-$C_{ND}$ {001}<110> and ${\gamma}$-fiber ND//<111> textures in AA5182 sheets. From the results, the ${\gamma}$-fiber ND//<111> component well evolved during rolling at high lid parameter of 6.77. The initial shear deformation texture, especially, ${\gamma}$-fiber ND//<111> was not rotated during heat treatment in holding time of 180~7,200 seconds on AA5182 with I/d parameter of 6.77. Therefore, the AA5182 sheets were fabricated by controlling I/d parameter having well evolved ${\gamma}$-fiber ND//<111> which was advantageous in good drawability of the sheets.

• 자원리싸이클링
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• 제9권2호
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• pp.46-52
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• 2000

사용한 알루미늄 캔을 다시 캔으로 재활용 하는 단계는 폐캔의 수집, 폐쇄, 선별, 도료제거, 용해 및 2차지금을 제작하는 단계와 이 2차지금을 이용하여 열처리, 열간 및 냉간압연, 중간소둔처리 등을 거쳐 다시 캔을 성형하는 단계로 나눌수 있다. 본 연구에서는 2차지금에서 켄성형까지의 과정에서 중요한 요소인 미세조직 및 열간압연후의 집합조직에 미치는 합금원소의 영향을 조사하였다. 폐캔을 이용하여 다시 캔을 제조하기 위한 판재가공에서는 주조시 형성된 공석상들의 구형화와 $\alpha$상 ($Al_{12}(Fe, Mn)_3Si)$)으로의 상변화 제어가 필요한데, 열처리에 의한 석출거동을 조사하여 $615^{\circ}C$, 5시간 균질화 처리조건에서 최적의 미세조직을 얻을 수 있었다. 2차자금을 이용하여 캔소재를 제조한 결과, Mn량이 증가할수록 고용효과에 의해 전기전도도는 감소하고 집합조직의 발달이 억제되었다. Si 과 Fe는 금속간화합물 형태로 존재하며, 함량이 증가할수록 석출효과에 의해 전기전도도가 증가하고 변형집합조직의 발달이 촉진되었다. 캔은 냉간압연후 다른처리 없이 바로 제조되기 때문에 집합조직의 제어는 열간압연 및 소둔처리 단계에서 제어되어야 한다.