• Title/Summary/Keyword: Analytical Validation

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Evaluation of Analytical Vibration Characteristics for Triple Cylindrical Shells Filled with Fluid (유체로 채워진 삼중 원통셸의 해석적 진동 특성 평가)

  • 지용관;이영신
    • Transactions of the Korean Society for Noise and Vibration Engineering
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    • v.12 no.2
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    • pp.150-160
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    • 2002
  • The free vibration characteristics of the triple cylindrical shells filled with fluid are investigated. The triple cylindrical shells are filled with compressible fluid. The boundary condition is clamped at both ends. Analytical method is developed to evaluate natural frequencies of triple cylindrical shells using Sanders' shell theory and courier series expansion by Stokes' transformation. Their results are compared with those of finite element method to verify the validation of the method developed. The modal characteristics of shells filled with fluid at region 1, 2 and 3 are evaluated.

Semi-analytical Method for Predicting Shaft Voltage in Field-excited Synchronous Generators

  • Doorsamy, Wesley;Cronje, Willem A.
    • Journal of Power Electronics
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    • v.14 no.5
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    • pp.859-865
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    • 2014
  • This study presents an electromagnetic model for predicting shaft voltages in a 2-pole field-excited synchronous generator. After the first observations on shaft voltages were made more than a century ago, extensive work has been conducted on eliminating, mitigating, and integrating the aforementioned phenomena. Given that emphasis has been placed on modeling shaft- and bearing-induced voltages in AC motors driven by variable frequency drives, similar efforts toward a model that is dedicated to generators are insubstantial. This work endeavors to improve current physical interpretation and prediction methods for shaft-induced voltages in generators through semi-analytical derivation. Aside from the experimental validation of the model, investigations regarding the behavior of shaft voltages under varying machine complexities and operating conditions clarify previous uncertainties regarding these phenomena. The performance of the numerical method is also assessed for application in eccentricity fault diagnosis.

Isolation of Constituents of Lihtospermum erythrorhizon and Development of an Analytical Method of its Constituents by HPLC-UV (자근의 성분 분리 및 이들 성분의 HPLC-UV 동시분석법 개발)

  • Hong, Eun-Young;Kyung, Min-Ji;Whang, Wan-Kyunn
    • YAKHAK HOEJI
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    • v.59 no.5
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    • pp.222-229
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    • 2015
  • Lithospermi radix, the dried roots of Litospermum erythrorhizon Sieboid et Zuccarini (Boraginaceae), has long been used to treat detoxification and inflammation. In this study, we isolated two main quinoid compounds, ${\beta}$-hydroxyisovalerylshikonin (1) and acetylshikonin (2) from L. erythrorhizon. As acetylshikonin is considered as a marker compound of L. erythrorhizon, a rapid analysis method for the simultaneous determination of quinoid compounds including 2 was also developed by HPLC (High Performance Liquid Chromatography) and validation of this analytical method. By the developed method, two quinoid marker compounds (${\beta}$-hydroxyisovalerylshikonin and acetylshikonin) were successfully quantified in 31 commercial samples which were collected from different regions. The contents were 0.20% (${\beta}$-hydroxyisovalerylshikonin) and 0.22% (acetylshikonin), respectively.

Analytical Approach and Experimental Verification for the Cogging Torque Reduction of Permanent Magnet Machines with Multi-pole Rotor (다극 회전자를 갖는 영구자석 기기의 코깅토크 저감을 위한 해석적 접근 및 실험적 검증)

  • Jang, Seok-Myeong;Choi, Jang-Young;Ko, Kyoung-Jin
    • Proceedings of the KIEE Conference
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    • 2007.07a
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    • pp.1031-1032
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    • 2007
  • In order to reduce the cogging torque, by predicting the variation of the cogging torque according to pole arc/pitch ratio by analytical and FE methods, pole arc/pitch ratio which makes the cogging torque minimum are determined. And then, the measurements of cogging torque for permanent magnet generators with determined pole arc/pitch ratio are presented. The reasons for the error between predicted and measured value are discussed fully in terms of the shape of permanent magnet. Finally, by confirming that predicted results for cogging torque according to pole arc/pitch ratio and skew are shown in good agreement with those obtained from measured one, the validation of analysis results is confirmed.

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Strength of prestressed concrete beams in torsion

  • Karayannis, Chris G.;Chalioris, Constantin E.
    • Structural Engineering and Mechanics
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    • v.10 no.2
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    • pp.165-180
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    • 2000
  • An analytical model with tension softening for the prediction of the capacity of prestressed concrete beams under pure torsion and under torsion combined with shear and flexure is introduced. The proposed approach employs bilinear stress-strain relationship with post cracking tension softening branch for the concrete in tension and special failure criteria for biaxial stress states. Further, for the solution of the governing equations a special numerical scheme is adopted which can be applied to elements with practically any cross-section since it utilizes a numerical mapping. The proposed method is mainly applied to plain prestressed concrete elements, but is also applicable to prestressed concrete beams with light transverse reinforcement. The aim of the present work is twofold; first, the validation of the approach by comparison between experimental results and analytical predictions and second, a parametrical study of the influence of concentric and eccentric prestressing on the torsional capacity of concrete elements and the interaction between torsion and shear for various levels of prestressing. The results of this investigation presented in the form of interaction curves, are compared to experimental results and code provisions.

Effective determination of nicotine enantiomers from e-liquids and biological fluids by high performance liquid chromatography (HPLC) using dispersive liquid-liquid microextraction (DLLME)

  • Song, Seunghoon;Myung, Seung-Woon
    • Analytical Science and Technology
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    • v.34 no.4
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    • pp.180-190
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    • 2021
  • This study compared the efficacy of chiral GC and chiral HPLC for the analysis of nicotine. To develop a suitable dispersive liquid-liquid microextraction (DLLME) method, the following parameters were optimized: pH, extraction solvent, dispersive solvent, type and quantity of salt, and laboratory temperature. The validation of the method was carried out by the established HPLC method. The LODs were 0.11 ㎍/mL and 0.17 ㎍/mL for the (S)- and (R)- enantiomers, respectively. The LOQs were 0.30 ㎍/mL and 0.44 ㎍/mL, respectively. The optimal calibration range was between 0.30-18 ㎍/mL and 0.44-4.40 ㎍/mL, respectively, and the correlation coefficient (r2) was 0.9978-0.9996. The intra-day accuracy was 79.9-110.6 %, and the intra-day precision was 1.3-12.0 %. The inter-day accuracy was 87.8-108.0 %, and the inter-day precision was 4.0-12.8 %. E-liquid and biological fluids (urine and saliva) were analyzed using the established method.

Development of a Mushroom Powder Certified Reference Material for Element Analysis

  • Betru, Tegegn Gizachew;Yim, Yong-Hyeon;Lee, Kyoung-Seok
    • Mass Spectrometry Letters
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    • v.11 no.4
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    • pp.108-112
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    • 2020
  • A certified reference material (CRM) for the analysis of nutrient elements in an edible mushroom (Ganoderma lyceum) powder has been developed (KRISS CRM 108-10-011). The mass fractions of calcium (Ca), iron (Fe), and zinc (Zn) were measured by isotope dilution inductively coupled plasma mass spectrometry (ID ICP/MS). To dissolve the fungi cell wall of mushroom consisted of chitin fibers, sample preparation method by single reaction chamber type microwave-assisted acid digestion with acid mixtures was optimized. The mean measurement results obtained from 12 sample bottles were used to assign as the certified values for the CRM and the between-bottle homogeneities were evaluated from the relative standard deviations. The certified values were metrologically traceable to the definition of the kilogram in the International System of Units (SI). This CRM is expected to be used for validation of analytical methods or quality control of measurement results in analytical laboratories when they determine the mass fractions of elements in mushroom or other similar samples.

Buckling and vibration of symmetric laminated composite plates with edges elastically restrained

  • Ashour, Ahmed S.
    • Steel and Composite Structures
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    • v.3 no.6
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    • pp.439-450
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    • 2003
  • The finite strip transition matrix technique, a semi analytical method, is employed to obtain the buckling loads and the natural frequencies of symmetric cross-ply laminated composite plates with edges elastically restrained against both translation and rotation. To illustrate the accuracy and the validation of the method several example of cross play laminated composite plates were analyzed. The buckling loads and the frequency parameters are presented and compared with available results in the literature. The convergence study and the excellent agreement with known results show the reliability of the purposed technique.

The Fundamental Requirements in the Application of Relaxed Eddy Accumulation Method for Measuring the Trace Gas Fluxes

  • Kim Ki-Hyun
    • Journal of Korean Society for Atmospheric Environment
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    • v.21 no.E1
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    • pp.37-39
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    • 2005
  • It is well perceived that micrometeorological approach is one of the most reliable method for the quantification of vertical fluxes of trace components in the atmosphere. In this study, the feasibility of relaxed eddy accumulation (REA) method is discussed with respect to its reliability in the field application. Knowing that the use of micrometeorological approaches requires validation of analytical uncertainties involved, the problems and issues associated with its application are discussed to stimulate the proper employment of such technique in the field study.

An analytical solution to the laminated piezoelectric beam under the electric field

  • Lin, Qirong;Jin, Zhanli;Liu, Zhengxing
    • Structural Engineering and Mechanics
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    • v.10 no.3
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    • pp.289-298
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    • 2000
  • Based on the two-dimensional constitutive relationship of the piezoelastic material, this paper derived an analytic solution to the elastic beam with the piezoelectric layer under the electric field, presented the explicit expressions of its displacement and stress. It is helpful for understanding the electrical and mechanical behavior of piezoelectric materials as actuators and the validation of the numerical methods such as FEM.