• Title/Summary/Keyword: An extremely low temperature

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Development of Efficient Curing Sheet for Thermal Insulation Curing of Concrete in Cold Weather

  • Han, Cheon-Goo;Son, Myung-Sik;Choi, Hyun-Kyu
    • Journal of the Korea Institute of Building Construction
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    • v.12 no.3
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    • pp.291-298
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    • 2012
  • For cold weather concreting, frost damage at early age is generated in the concrete, and problems such as delaying of setting and hardening and lowering of strength manifestation emerge due to the low outside air temperature at the early stage of pouring, making the selection of an effective curing method critically important. Unfortunately, the tent sheet currently used as the curing film for heating insulation at work sites, not only has the problems of inferior permeability and extremely deteriorated airtightness, but a phenomenon of continuous fracturing is also generated along the direction of fabric of the material itself, presenting difficult circumstances for maintaining adequate curing temperature. The aim of this study was to develop an improved bubble sheet type curing film for heating insulation of cold weather concrete by combining mesh-tarpaulin, which has excellent tension properties, with bubble sheet, which offers superior insulation performance. The analysis showed that the improved curing film in which BBS1 is stacked to MT was a suitable replacement for curing films currently in use, as it has better permeability, tension property, and insulation performance than the T type film used at work sites today.

Multidimensional ZnO light-emitting diode structures grown by metal organic chemical vapor deposition on p-Si (p형 Si 기판위에 성장된 ZnO 다층형복합구조의 이종접합구조 LED 제작)

  • Kim, Dong-Chan;Kong, Bo-Hyun;Han, Won-Suk;Choi, Mi-Kyung;Cho, Hyung-Koun;Lee, Jong-Hun;Kim, Hong-Seung
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.06a
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    • pp.84-84
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    • 2008
  • A multidimensional ZnO light-emitting diode LEDstructure comprising film/nanorods/substrate was fabricated on a p-type Si substrate using metal organic chemical vapor deposition at relatively low growth temperature. The filmlike top layer used for the metal contact was continuously formed on the ZnO nanorods by varying the growth conditions and the resulting structure allowed us to utilize the nanorods with intense emission as an active layer. We investigated the performance of the resulting multidimensional LED. An extremely high breakdown voltage and low reverse leakage current as well as typical rectification behavior were observed in the I-V characteristics.

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Highly Conformal Deposition of Pure Co Films by MOCVD Using Co2(CO)8 as a Precursor (Co2(CO)8 (Dicobalt Octacarbonyl) 전구체를 이용한 MOCVD Co 박막의 균일한 증착 특성 및 높은 순도에 관한 연구)

  • Lee, Jeong-Gil;Lee, Jae-Gab
    • Korean Journal of Materials Research
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    • v.16 no.2
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    • pp.106-110
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    • 2006
  • We have investigated the effect of the experimental variables such as temperature and pressure on conformality of Co films deposited over high aspect ratio trenches using $Co_2(CO)_8$ as a precursor. The results show that the conformality of Co films is a strong function of temperature and process pressure. Lowering the pressure and temperature significantly improves the conformality. As the pressure decreases from 0.6 Torr to 0.2 Torr at $50^{\circ}C$, the bottom coverage of Co films over $0.2{\mu}m$ width trenches with an aspect ratio of 13 to 1 significantly increases to 85%. However, further increasing the temperature from 50 to $60^{\circ}C$ at the pressure of 0.2 Torr degrades the bottom coverage to 14%. In contrast, the extremely low pressure of 0.03 Torr allows the excellent conformal deposition of Co films up to $70^{\circ}C$. This can be attributed to the suppression of homogeneous reaction in the gas phase, which can create the intermediate products with high sticking coefficient. In addition, the Co films deposited at $50^{\circ}C$ show the low resistivity with negligible contamination. As a result, the newly developed Co process using MOCVD can be implemented into the next generation devices with complex shapes.

Nanoscale NiO for transparent solid state devices

  • Patel, Malkeshkumar;Kim, Joondong;Park, Hyeong-Ho
    • Proceedings of the Korean Vacuum Society Conference
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    • 2015.08a
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    • pp.243.2-243.2
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    • 2015
  • We report a high-performing nanoscale NiO thin film grown by thermal oxidation of sputtered Ni film. The structural, physical, optical and electrical properties of nanoscale NiO were comprehensively investigated. A quality transparent heterojunction (NiO/ZnO) was formed by large-area applicable sputtering deposition method that has an extremely low saturation current of 0.1 nA. Considerable large rectification ratio of more than 1000 was obtained for transparent heterojunction device. Mott-Schottky analyses were applied to develop the interface of NiO and ZnO by establishing energy diagrams. Nanoscale NiO has the accepter carrier concentration of the order of 1018 cm-3. Nanoscale NiO Schottky junction device properties were comprehensively studied using room temperature impedance spectroscopy.

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Nanocrystallization of Ibuprofen by Cryogenic Ball Milling II (극저온 볼 밀링을 통한 Ibuprofen 분말의 나노화II)

  • 조현갑;이경엽;백영남;박훈재;이상목
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2004.10a
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    • pp.442-446
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    • 2004
  • Reducing the particle size of drug materials down to submicron is an important matter in pharmaceutical industry. Cryogenic milling technology is one of the mechanical milling processes, which is mostly utilized in refining grain size of metal and ceramics at extremely low temperature environment. This technique has not been readily studied in application to medical and biotechnology. This paper, therefore, describes the application of cryogenic milling process to reduce particle size of Ibuprofen. The shape and size of the Ibuprofen particle before and after the cryogenic ball milling process were analyzed. XRD analysis was performed to examine a change in crystallinity of Ibuprofen by the cryogenic ball milling process. The results showed that the size of Ibuprofen particles was reduced to 1/10 or less of its initial size. The results also showed that the degree of crystallinity of Ibuprofen was slightly reduced after cryogenic ball milling with nitrogen

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Isolation ref Brevibacterium sp. CH1 and Properties of Its Enzyme (Brevibacterium sp. CH1의 분리 및 특성)

  • 장호남;이처영;황준식
    • Microbiology and Biotechnology Letters
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    • v.17 no.5
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    • pp.429-435
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    • 1989
  • A bacterial strain of Brevibaterium sp. CH1 was isolated and used to produce an enzyme (nitrile hydratase) necessary for earring out the bioconversion of acrylonitrile to acrylamide. The culture and reaction conditions, and medium optimization were studied for the strain. The conversion yield was nearly 100% with a trace amount of acrylic acid produced. The strain showed strong activity of nitrile hydratase toward acrylonitrile and extremely low activity of the amidase toward acrylamide. We sought optimum culture conditions for the formation of nitrile hydratase by Brevibacterium sp. CH1. The effects of temperature and pH on the activity of free and immobilized tells were investigated. The nitrite hydratase of Brevibacterium sp. CH1 acted not only on various aliphatic nitrites such as acrylonitrile, propionitrile and acetonitrile, but also on aromatic nitrile as nicotinonitrile.

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A Development of Solenoid Valve for Satellite Propulsion System (위성추진시스템 솔레노이드 밸브 개발)

  • Kim, Kyung-Sik;Baek, Ki-Bong;Park, Eun-Joo;Cho, Seung-Hwan;Kim, Su-Gyeom
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2011.11a
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    • pp.456-459
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    • 2011
  • The Dual-type Solenoid Valve was developed for a domestic production of a fuel-supply valve on the satellite attitude control thruster system. The satellite valve using a hydrazine as a fuel must fulfill the cycle life, shock, vibration and the environment of an extremely low temperature In addition to the basic performance of the response time, mass flow and leakage etc.. in this paper, the design, production and performance experiment using the nitrogen pneumatic equipment were conducted.

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Built-Up Edge Analysis of Orthogonal Cutting By Visco-Plastic Finite Element Method (점소성 유한요소법에 의한 이차원 절삭의 구성인선 해석)

  • 김동식
    • Proceedings of the Korean Society of Machine Tool Engineers Conference
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    • 1995.10a
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    • pp.60-63
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    • 1995
  • The behavior of the work materials in the chip-tool interface in extremely high strain rates and temperatures is more that of viscous liquids than that of normal solid metals. In these circumstances the principles of fluid mechanics can be invoked to describe the metal flow in the neighborhood of the cutting edge. In the present paper an Eulerian finite element model is presented that simulates metal flow in the vicinity of the cutting edge when machining a low carbon steel with carbide cutting tool. The work material is assumed to obey visco-plastic (Bingham solid) constitutive law and Von Mises criterion. Heat generation is included in the model, assuming adiabatic conditions within each element. the mechanical and thermal properties of the work material are accepted to vary with the temperature. The model is based on the virtual work-stream function formulation, emphasis is given on analyzing the formation of the stagnant metal zone ahead of the cutting edge. The model predicts flow field characteristics such as material velocity effective stress and strain-rate distributions as well as built-up layer configuration

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A Study on the Dispersion Characteristics of Carbon Nanotubes using Cryogenic Ball Milling Process (극저온 볼밀링 공정을 이용한 탄소나노튜브의 분산특성 연구)

  • Lee, Ji-Hoon;Rhee, Kyong-Yop
    • Journal of the Korean Society for Precision Engineering
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    • v.27 no.7
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    • pp.49-54
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    • 2010
  • The cryogenic ball milling was performed on carbon nanotubes (CNTs) at an extremely low temperature to increase the dispersion of CNTs. The effects of milling speed and time on the deagglomeration and structural changes of CNTs were studied. FESEM was used to analyze the dispersion and the change of particle size before and after milling process. Transmission electron microscopic (TEM) analysis was also investigated the effect of cryogenic ball milling on the morphological characteristics of CNTs. The structural changes by the cryogenic ball milling process were further confirmed by x-ray diffraction (XRD) and Raman spectroscopic analysis. The results showed that the agglomeration of CNTs was significantly reduced and amorphous structure was observed at high milling speed. However, the milling time has no great effect on the dispersion property and structural change of CNTs compared with milling speed.

Synthesis Polyurethane Coating Materials Containing Polysiloxane (Polysiloxane을 함유하는 Polyurethane Coating 재료의 합성)

  • Yoo, Young-Mi;Kim, Kong-Soo;Chun, Yong-Chul;Kang, Seog-Ho;Shin, Jae-Sup
    • Elastomers and Composites
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    • v.27 no.4
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    • pp.267-274
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    • 1992
  • Polydimethylsiloxane(PDMS)-containing polyurethane coating materials were synthesized because PDMS-based elastomers have unique properties including an extremely low glass transition temperature, good thermal and oxidative stability, and good dielectric properties. In this experiment a vinyl copolymer which consisted of vinyl chloride, vinyl acetate, vinyl alcohol, and maleic acid was used, and Coronate L was used as a polyisocyanate. PDMS-containing polyurethane was synthesized from polydimethylsiloxane, MDI, and 1,4-butanediol. Films were casted by reaction of viny copolymer, Coronate L, and PDMS-containing polyurethane. Thickness of tile films were $150-170{\mu}m$ and the films were characterized by IR, DSC, and Instron.

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