• Title/Summary/Keyword: Amorphous metal powder

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Development and Goals of smart EM wave absorber with heat radiating function

  • Choi, Dong Soo;Kim, Dong Il;Kim, Do Yeol;Choi, Dong Han
    • Proceedings of the Korean Institute of Navigation and Port Research Conference
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    • 2012.10a
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    • pp.125-127
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    • 2012
  • With the progress of electronics and radio communication technology, human enjoys greater freedom in communication. However, EMW (Electro-Magnetic wave) environments have became complicate and more difficult to control. Thus, international organizations, such as the American National Standard Institution (ANSI), Federal Communications Commission (FCC), the Comite Internationale Special des Perturbations Radio electrique (CISPR), etc, have provided standard for controlling the EM wave environments and for the countermeasure of the electromagnetic compatibility (EMC). In this paper, the status of EMW absorber and the goal of smart EMW absorber ifor the future were described. Furthermore, design method of the smart EM wave Absorber with heat radiating function was suggested. The designed smart EM wave Absorber has the absoption ability of more than 5 dB from 2 GHz to 2.45 GHz band, one optimum aperture (hole) size of which was 6 mm, 9 mm in adjacent hole space, and 6.5 mm in thickness, respectivly. Thus, it is repected that these results can be applied to various EMC devices in electronic, communication, and controlling systems.

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Synthesis of PSZ-seeding Mullite Composite from Metal Alkoxides and Its Characteristics of Sintered Body (금속 알콕사이드로부터 PSZ-seeding Mullite 복합체의 합성 및 소결체의 특성)

  • Yim, Going;Yim, Chai-Suk;Kim, Young-Ho
    • Korean Journal of Materials Research
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    • v.17 no.1
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    • pp.18-24
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    • 2007
  • Mullite-PSZ composite was prepared by sol-gel method using $Al(sec-OC_4H_9)_3,\;Si(OC_2H_5)_4,\;ZrOCl_2\;8H_2O\;and\;Y_2O_3$. The sinterability ana mechanical properties of powder compacts sintered at $1,650^{\circ}C$ for 4 hrs were investigated for various PSZ contents. In result Al-Si spinel formed at $980^{\circ}C$ from amorphous dried gel, and zirconia as well as mullite crystal formed above $1,200^{\circ}C$. The sintered body was densified to $97{\sim}98%$ except the specimen containing 25vol% PSZ which showed the relative density of about 95% obtained by sintering at $1,650^{\circ}C$ for 4 h. The flexural strength of the sintered body was a maximum value of 290 MPa in 20 vol% PSZ, which was also considerably larger than the value of 200 MPa without PSZ. The value of the fracture toughness increased linearly with increase of PSZ content and showed a maximum value of $4.3MPam^{1/2}$ in 25 vol% PSZ, Namely this value was remarkably larger than the $value(2.6MPam^{1/2})$ of pure mullite without PSZ.

Analysis and Mechanical Behavior of Coating Layer in Metallic Glass Matrix Composite (비정질 기지 복합재 코팅층의 미세조직 분석 및 기계적 거동)

  • Jang, Beom Taek;Yi, Seong Hoon
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.38 no.6
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    • pp.629-636
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    • 2014
  • For surface modification, bulk metallic glass coatings were fabricated using metallic glass powder and a mixture of a self-fluxing alloy or/and hard metal alloys with a heat-resisting property using a high velocity oxy-fuel coating thermal spraying process. Microstructural analyses and mechanical tests were carried out using X-ray diffraction, a scanning electron microscope, an atomic force microscope, a three-dimensional optical profiler, and nanoindenation. As a result, the monolithic metallic glass coating was found to consist of solid particle and lamellae regions that included many pores. Second phase-reinforced composite coatings with a self-fluxing alloy or/and hard metal alloy additives were employed with in-situ $Cr_2Ni_3$ precipitate or/and ex-situ WC particles in an amorphous matrix. The mechanical behaviors of the solid particles and lamella regions showed large hardness and elastic modulus differences. The mechanical properties of the particle regions in the metallic glass composite coatings were superior to those of the lamellae regions in the monolithic metallic glass coatings, but indicated similar trends in matrix region of all the coating layers.

A Process Optimization of HVOF on ALBC3 by Experiments Design (실험계획법을 이용한 ALBC3에 대한 고속화염용사의 최적 공정 설계)

  • Kim, Young-Moon;Lim, Byung-Chul;Kim, Min-Tae;Park, Sang-Heup
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.17 no.4
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    • pp.448-453
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    • 2016
  • Erosion and abrasion caused by cavitation damage occur in fluid equipment, such as ships or impellers. Similarly, the equipment damage from noise and vibration can shorten its life. This study analyzed the importance of the parameter characteristics of the process optimization of HVOF (High Velocity Oxygen Fuel spraying), which is generally used in a variety of industries for enhancing the resistibility from the cavitation phenomenon. The surface of the ALBC3 substrate was coated with an amorphous powder as a filler metal according to the experimental design using the Taguchi method, and then the characteristics with each parameter were analyzed using a porosity measurement test. The optimal process conditions was a combustion pressure of 80psi, coating distance of 270mm, gun speed of 200mm/s, and powder feed rate of 25g/min as a result of the HVOF coating by applying the experimental design. The combustion pressure, coating distance and powder feed rate were more than 25% and indicated a similar contribution rate, but the contribution rate of the gun speed was 19%, which was slightly less than the others. The contribution rate with each parameter was only slightly significant. On the other hand, all four parameters were found to be important in the contribution rate aspects of the HVOF coating process.

Research in Crystalization and Conductivity of Electricity of Ge-Se-Bi System Chalcogenide Glass (Ge-Se-Bi계 칼코게나이드 유리의 비정질 및 결정화에 따른 전기 전도도의 변화)

  • Lee, Myeong-Won;Gang, Won-Ho
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1992.11a
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    • pp.77-81
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    • 1992
  • The purpose of this research was th evaluate conductivity of electricity of Ge-Se-Bi system Chalcogenide glass as a amorphous semiconductor by observing its dissolution and crystallization. In this experiment. Ge-Se-Bi metal powder in the rage of $Ge_{12-25}$, $Se_{65-85}$, $Bi_{2.5-15}$ was used as the sample ore. The ore was. put into a vaccous quartz tube and then melted. The condition of heat treatment was to dispose it to $1000^{\circ}C$ heat for 10 hours and then rapidly quenched it at $3834^{\circ}C$/see. The crystallization of the fused sample ripened as the change of temperature and time, after the crystal core was formell. At that time it was possible to observe the state that $Bi_2Se_3$ and $GeSe_2$ were crystallized. In the experiment of making memberance, the memberance was produced by using the previously experimented bulk sample. And decrystalization was well progressed when Ge was over 15 at %, Se was over 70 at %, and Bi was under 10 at%. As for bulk. when Ge was fixed to 20 at %, the conducting of electricity was increased as Bi gained at %. In the case of memberance, the conductivity was much more increased than that of bulk sample as the increase of at the increase of at % of Bi. In the experiment on $Ge_{20}$, $Se_{77.5}$ and $Bi_{2.5}$, the crystallization sswas most vigorous when they were kept at $330^{\circ}C$ for 4 hours.

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Solidification of Molten Salt Waste by Gel-Route Pre-treatment (겔화 전처리법을 이용한 폐용융염의 고형화)

  • Park Hwan Seo;Kim In Tae;Kim Hwan Young;Ryu Seung Kon;Kim Joon Hyung
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.3 no.1
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    • pp.57-65
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    • 2005
  • This study suggested a new method for the solidification of molten salt waste generated from the electro-metallurgical process in the spent fuel treatment. Using binary material system, sodium silicate and phosphoric acid, metal chlorides were converted into metal phosphate in the micro-reaction module formed by SiO$_{2} particles. The volatile element in the reaction module would little vaporized below 1100$^{circ}$C After the gel product was mixed with borosilicate glass powder and thermally treated at 1000$^{circ}$C, li exists as Li$_{3}$PO$_4$ separated from glass phase and, Cs and Sr would be incorporated into an amorphous phase from XRD analysis. In case of the addition of ZrCl$_{4}$ to the binary system, the gel products were transformed into NZP structure considered as an prospective ceramic waste form after heat-treatment above 700 $^{circ}$C. From these results, the gel-route pretreatment can be considered as an effective approach to the solidincation of molten salt waste by the confirmed process or waste form and this also would be an alternative method on the ANL method using zeolites in USA by the confirmation of its chemical durability as an future work.

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Physical and Electrochemical Properties of Gallium Oxide (β-Ga2O3) Nanorods as an Anode Active Material for Lithium Ion Batteries (리튬이온전지용 산화갈륨 (β-Ga2O3) 나노로드 (Nanorods) 음극 활물질의 물리적.전기화학적 특성)

  • Choi, Young-Jin;Ryu, Ho-Suk; Cho, Gyu-Bon;Cho, Kwon-Koo;Ryu, Kwang-Sun;Kim, Ki-Won
    • Journal of the Korean Electrochemical Society
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    • v.12 no.2
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    • pp.189-195
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    • 2009
  • $\beta-Ga_{2}O_{3}$ nanorods were synthesized by chemical vapor deposition method using nickel-oxide nanoparticle as a catalyst and gallium metal powder as a source material. The average diameter of nanorods was around 160 nm and the average length was $4{\mu}m$. Also, we confirmed that the synthesis of nanorods follows the vapor-solid growth mechanism. From the results of X-ray diffraction and HR-TEM observation, it can be found that the synthesized nanorods consisted of a typical core-shell structure with single-crystalline $\beta-Ga_{2}O_{3}$ core with a monoclinic crystal structure and an outer amorphous gallium oxide layer. Li/$\beta-Ga_{2}O_{3}$ nanorods cell delivered capacity of 867 mAh/g-$\beta-Ga_{2}O_{3}$ at first discharge. Although the Li/$\beta-Ga_{2}O_{3}$ nanorods cell showed low coulombic efficiency at first cycle, the cell exhibited stable cycle life property after fifth cycle.