• Title/Summary/Keyword: Al-Si coated

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Electromagnetic Properties of Siver Coated Iron based Alloy Powders Prepared by Chemical Reduction Method

  • Lee, Byoung-Yoon;Lee, Jae-Wook;Yun, Yeo-Chun;Jeong, In-Bum;Moon, Joo-Ho
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.1213-1214
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    • 2006
  • The synthesis of silver coated iron base alloy (Sendust : Fe-Si-Al) powder having the both effects of shielding and suppressing of electromagnetic wave was studied. Depending on thickness of silver coating layer, the electromagnetic properties of the dispersed particles complexed with organic binder were examined. It is proposed that the silver coated sendust flake powders with controlled electrical properties and thickness can be used as thin microwave absorbers in quasi-microwave frequency band.

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The Effect of Far Infrared Radiation of $\beta$-Spodumene Glass-Ceramics Flims Coated on Iron Substrate by Sol-Gel Technique (졸-겔법에 의한 금속기판상의 $\beta$-spodumene 결정성유리의 박영도포와 원적외선상세성)

  • 양중식;신현택;박종옥
    • Journal of the Korean institute of surface engineering
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    • v.27 no.2
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    • pp.99-108
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    • 1994
  • Films of glass-ceramics $Li_2O-Al_2O_3-SiO_2$(LAS)system were prepared on substrate of an iron plate(SCP) by sol-gel technique using metal alkoxide such as Si$(OC_2H_5)_4$,Al$(OC_2H_9)_3$) and Ti$(OC_2H_6)_4$). Sol which was made by means of simple spray coating, on the substrate was hydrolyzed at 75~$80^{\circ}C$ in moisture cabinet (80~90 % humidity) to form the multicomponent gel. The films up to about 0.8~1.0$mu extrm{m}$ in thickness can be obtained by repeating operation, spraylongrightarrowhydrolysis and condensationlongrightarrowdryinglongrightarrowheating and crystallization at $700^{\circ}C$ for 3~5min. The far-infrared radiation spectra of the coated films on substrate were examined by FT-IR and of films was also observed by scanning electron micrograph technique. The thermal evaluation of the gel-film is followed by TG/DTA measurements. The structure evaluation is followedd X-ray diffraction. These results suggest that this process is applicable to far-infrared radiat at thin film technique.

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Luminescent Properties of $SrTiO_3:Pr^{3+}$ Phosphor Coated with $SiO_2$ and $Al_2O_3$ by Sol-Gel Method (졸-겔법에 의한 $SrTiO_3:Pr^{3+}$ 형광체의 $SiO_2$$Al_2O_3$ 코팅에 따른 발광특성)

  • Lee, Dong-Kyu;Lim, Mun-Hyuk;Lee, Jin-Hwa;Kim, Tae-Young
    • Journal of the Korean Applied Science and Technology
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    • v.23 no.3
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    • pp.243-251
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    • 2006
  • Field emission display(FED) is actively investigated in view of the development of full color flat-panel display, which can replace some cathode-ray tube(CRT). Thus, the development of new phosphors appropriate for FED is urgently needed and has been actively investigated. In this work, $SrTiO_3:Pr^{3+}$ phosphor was prepared by sol-gel method and the coating was applied by sol-gel method combined with sonication on these phosphor's surface into diluted precursor solution. It was found that very fine particles of coating material were formed on phosphor's surface. The luminescent intensity of $SrTiO_3:Pr^{3+}$ phosphor coated with $SiO_2$ and $Al_2O_3$ was considerably increased without any noticeable change in color chromaticity. The optimum concentration of coating material was found to be 1wt% and the optimum pH value of the solution was 10.

Effect of Siliceous Slury Coating on Microstructure of Concrete under Damp Environment (규산질미분말혼합시멘트계도포방수재료가 습윤환경하의 콘크리트의 미세조직에 미치는 영향)

  • 오상근
    • Proceedings of the Korea Concrete Institute Conference
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    • 1992.10a
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    • pp.1-4
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    • 1992
  • This paper deals with the effect of siliceous slurry coating on concrete microstructure under damp environment. This material is mixed inorganic powder consisted of silica, cement and fine sand and water. Water pressure was given on the coated surface of concrete. for estimation on effect of siliceous slurry coating, microstructure of coated concrete was observed through SEM, and chemical components of crystals were analyzed with X-ray diffraction and EDX. A number of needle and fibrous crystals were produced in microstructure. And based on X-ray diffraction and EDX, needle crystal mainly consist of Al, Si, and Ca, and it is concluded to be ettringite. Fibrous crystals consist of Ca and Si, and it to be calcium silicate hydrate.

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A Study on the Optical Property of Al-N-codoped p-type ZnO Thin Films Fabricated by DC Magnetron Sputtering Method

  • Liu, Yan-Yan;Jin, Hu-Jie;Park, Choon-Bae
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2009.06a
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    • pp.319-320
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    • 2009
  • In this study, high-quality Al-N doped p-type ZnO thin films were deposited on n-type Si (100) wafer or Si coated with buffer layer by DC magnetron sputtering in the mixture of $N_2$ and $O_2$ gas. The target was ceramic ZnO mixed with $Al_2O_3$ (2 wt%). The p-type ZnO thin film showed higher carrier concentration $2.93\times10^{17}cm^{-3}$, lower resistivity of $5.349\;{\Omega}cm$ and mobility of $3.99\;cm^2V^{-1}S^{-1}$, respectively. According to PL spectrum, the Al donor energy level depth ($E_d$) of Al-N codoped p-type ZnO film was reduced to about 51 meV, and the N acceptor energy level depth ($E_a$) was reduced to 63 meV, respectively.

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The Properties of the Metal Hydride electrodes prepared by Silicon Sealant (Si-sealant를 이용하여 제조한 금속수소화물 전극의 특성)

  • CHOI, Jeon;PARK, Choong-Nyeon
    • Transactions of the Korean hydrogen and new energy society
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    • v.4 no.2
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    • pp.23-28
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    • 1993
  • The $(LM)Ni_{4.5}Co_{0.1}Mn_{0.2}Al_{0.2}$ hydrogen storage alloy powders were conducted 25wt% electroless copper plating in an acidic bath. For the preparation of a hydride electrodes, the copper coated alloy powder was mixed with Si-sealant(organosilicon) and compacted with $6t/cm^2$ at room temperature. The electrode characteristics were examined through electrochemical measurements in a half cell. As a sealant contents increased, the initial discharge capacity of si-sealant bounded electrode was lower and the activation rate in high current density was slower. For extended cycles, however, the electrodes with the Si-sealant were superior in a high rate discharge and useful range of temperature over the sealant-free electrode. In addition, the cycle life increased with increasing the amount of Si-sealant added. It can be suggested from the results that the Si-sealant as a binder could be applied to the preparation of the metal hydride electrode.

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Machining Characteristics of Ni-based Heat Resisting Alloy (니켈기 초내열합금의 절삭성에 관한 연구)

  • 강신호;김대은
    • Journal of the Korean Society for Precision Engineering
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    • v.15 no.4
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    • pp.27-35
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    • 1998
  • Ni-based heat resisting alloys are commonly used for high temperature applications such as in aircraft engines and gas turbines. In this work, the machinability of Nimonic 263 alloy is investigated with respect to optimum tool type and cutting conditions for both continuous and discontinuous machining as well as weld region. Among the five types of tools tested, K25 tool experienced the least of damage in machining the weld region. Furthermore, despite their superior high temperature hardness, Si-Al-O-N and CBN tools peformed poorly in machining Nimonic 263.

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Evaporation characteristics of materials from resistive heating sources(I) (저항가열원에 의한 물질의 증발특성(I))

  • 정재인;임병문;문종호;홍재화;강정수;이영백
    • Journal of the Korean institute of surface engineering
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    • v.24 no.1
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    • pp.25-30
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    • 1991
  • The evaporation characteristics of Ag, Al, Au, Cr. Cu, In, Mg, Mn, Pb, Pd, Si, SiO, Sn, Ti and Zn with the various resistive heating sources have been studied. The employed sources are refractory metal (Mo, Ta and W) boats, W-wire, ceramic (usually Al2O3)-coated and -barriered refractory metal boats, and special boats such as baffled boats and intermetallic boats (nitride compound and graphite). We investigated the melting mode, evaporation rate at a specific power, and lifetime of the sources. A special boat holder is also discussed which is needed to cool the sources at a large heat capacity.

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A Study on the Corrosion Mechanism by the Moisture on the Surface Layer of the Alloys Coated Steel Sheet (합금도금강판의 수적에 의한 표면층의 부식기구에 관한 연구)

  • Kim, Y.H.;Kim, S.K.;Jeon, E.C.
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.1 no.1
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    • pp.71-78
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    • 2002
  • Since the early 1980's the use of zinc-aluminum alloy-coated steel sheet(Galvalume) for vehicular corrosion protection has increased drastically. It is consisting of 55%Al-43.4% Zn-1.6%Si. Galvalume has a good corrosion resistance, heat reflectivity and shiny appearance, which has a dendritic structure of alloy layer. It has a good corrosion resistance due to dendritic structure. But, this also has a weak point against moisture during long period of transportation as sheeted and or coiled without any relation of chromating on the surface of steel sheet or not because of high humidity and temperature. Here, We studied the corrosion mechanism by the moisture.

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Characterization and hydrothermal surface modification of non-swelling property mica using nano silver (은나노를 이용한 비팽윤성 운모의 수열적인 표면개질 및 특성평가)

  • Seok, Jeong-Won;Park, Ra-Young;Kim, Pan-Chae
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.17 no.4
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    • pp.172-178
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    • 2007
  • Mica (muscovite) powders were synthesized by hydrothermal method (horizontal turning method). The hydrothermal conditions for the synthesis of mica were prepared by the ratio of $K_2O : Al(OH)_3 : SiO_2$ = 1 : 3 : 3 mol% as the starting materials with KOH (8 mol%) solution as the hydrothermal solvent and reaction temperature at $260^{\circ}C$ for 72hrs. The synthetic powder used for preparation of nano silver coated mica by vertical hydrothermal treatment. The hydrothermal conditions for the treated as nano silver coating were prepared by the synthetic powder as raw materials, triple distilled water ($0.5{\ell}$) solution as the hydrothermal solvent with nano silver sol (1,000 ppm) as the material of nano silver coating and reaction temperature at $160{\sim}260^{\circ}C$ for 72 hrs. After hydrothermal treatment, structural, judgment of nano silver coating and character of nano silver coated mica were examined by XRD, SEM, TEM-EDX and shake plask method.