• 제목/요약/키워드: Al plate

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Antibacterial, Anti-Diarrhoeal, Analgesic, Cytotoxic Activities, and GC-MS Profiling of Sonneratia apetala (Buch.-Ham.) Seed

  • Hossain, Sheikh Julfikar;Islam, M Rabiul;Pervin, Tahmina;Iftekharuzzaman, M;Hamdi, Omer AA;Mubassara, Sanzida;Saifuzzaman, M;Shilpi, Jamil Ahmad
    • Preventive Nutrition and Food Science
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    • 제22권3호
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    • pp.157-165
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    • 2017
  • Fruits of Sonneratia apetala (Buch.-Ham.), (English: mangrove apple, Bengali: keora) both seeds and pericarps, are largely consumed as food besides their enormous medicinal application. The fruit seeds have high content of nutrients and bioactive components. The seeds powder of S. apetala was successively fractionated using n-hexane, diethyl ether, chloroform, ethyl acetate, and methanol. The fractions were used to evaluate antibacterial, anti-diarrhoeal, analgesic, and cytotoxic activities. Methanol fraction of seeds (MeS) stronly inhibited Escherichia coli strains, Salmonella Paratyphi A, Salmonella Typhi, Shigella dysenteriae, and Staphylococcus aureus except Vibrio cholerae at $500{\mu}g/disc$. All the fractions strongly inhibited castor oil induced diarrhoeal episodes and onset time in mice at 500 mg extract/kg body weight (P<0.001). At the same concentration, MeS had the strongest inhibitory activity on diarrhoeal episodes, whereas the n-hexane fraction (HS) significantly (P<0.05) prolonged diarrhoeal onset time as compared to positive control. Similarly, HS (P<0.005) inhibited acetic acid induced writhing in mice at 500 mg extract/kg, more than any other fraction. HS and diethyl ether fractions of seed strongly increased reaction time of mice in hot plate test at 500 mg extract/kg. All the fractions showed strong cytotoxic effects in brine shrimp lethality tests. Gas chromatography-mass spectrometry analysis of HS led to the identification of 23 compounds. Linoleic acid (29.9%), palmitic acid (23.2%), ascorbyl palmitate (21.2%), and stearic acid (10.5%) were the major compounds in HS. These results suggest that seeds of S. apetala could be of great use as nutraceuticals.

Application of multimodal surfaces using amorphous silicon (a-Si) thin film for secondary ion mass spectrometry (SIMS) and laser desorption/ionization mass spectrometry (LDI-MS)

  • Kim, Shin Hye;Lee, Tae Geol;Yoon, Sohee
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2016년도 제50회 동계 정기학술대회 초록집
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    • pp.384.1-384.1
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    • 2016
  • We reported that amorphous silicon (a-Si) thin film provide sample plate exhibiting a multimodality to measure biomolecules by secondary ion mass spectrometry (SIMS) and laser desorption/ionization mass spectrometry (LDI-MS). Kim et al.1 reported that a-Si thin film were suitable to detect small molecules such as drugs and peptides by SIMS and LDI-MS. Recently, bacterial identification has been required in many fields such as food analysis, veterinary science, ecology, agriculture, and so on.2 Mass spectrometry is emerging for identifying and profiling microbiology samples from its advantageous characters of label-free and shot-time analysis. Five species of bacteria - S. aureus, G. glutamicum, B. kurstaki, B. sphaericus, and B. licheniformis - were sampled for MS analysis without lipid extraction in sample preparation steps. The samples were loaded onto the a-Si thin film with a thickness of 100 nm which did not only considered laser-beam penetration but also surface homogeneity. Mass spectra were recorded in both positive and negative ionization modes for more analytical information. High reproducibility and sensitivity of mass spectra were demonstrated in a mass range up to mass-to-charge ratio(m/z) 1200 by applying the a-Si thin film in mentioned above MS. Principle component analysis (PCA) - a popular statistical analysis widely used in data processing was employed to differentiate between five bacterial species. The PCA results verified that each bacterial species were readily distinguished and differentiated effectively from our MS approach. It shows a new opportunity to rapid bacterial profiling and identification in clinical microbiology. More details will be discussed in the presentation.

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프리스트레스트 콘크리트 박스 거더의 종방향 프리스트레싱에 의한 슬래브의 횡방향 응력 (Transverse Stress of Slabs due tp Longitudinal Prestressing in Prestressed Concrete Box Girders)

  • 양인환
    • 콘크리트학회논문집
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    • 제15권5호
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    • pp.679-688
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    • 2003
  • 종방향 텐던이 경사진 복부에 배치되는 박스 거더의 경우 프리스트레스 힘은 종방향 뿐만 아니라 횡방향 거동에도 영향을 미친다. 본 논문에서는 종방향 프리스트레싱에 의해 유발되는 횡방향 효과를 산정하는 기법을 제안하였다. 박스 거더의 유한요소 정식화 및 종방향 프리스트레싱 해석에 의해 프리스트레스 분포를 산정한 후, 이를 이용하여 횡방향 등가하중을 산정한다. 제안기법에 의한 수치해석결과와 기존의 접판법에 의한 수치해석결과는 유사하며, 이는 본 기법이 합리적임을 나타낸다. 제안기법을 이용하여 박스 거더 슬래브의 횡방향 거동을 분석하였다. 수치분석은 복부경사각, 텐던 편심에 대한 경간 길이비 등과 같은 주요 변수를 통해 수행되었다. 전형적인 단면 조건에서 종방향 프리스트레싱 효과만을 고려할 때, 박스 거더 슬래브의 횡방향 응력은 크지 않은 것으로 나타난다. 그러나, 복부 경사각이 50도 이하로 과도하게 작아지거나 텐던 편심에 대한 경간 길이비가 28이하로 작아지는 경우에는 교량 설계시 횡방향 응력의 크기를 고려할 필요가 있다고 사료된다.

Radiopacity of restorative composites by conventional radiograph and digital images with different resolutions

  • Dantas, Raquel Venancio Fernandes;Sarmento, Hugo Ramalho;Duarte, Rosangela Marques;Meireles Monte Raso, Sonia Saeger;de Andrade, Ana Karina Maciel;Dos Anjos-Pontual, Maria Luiza
    • Imaging Science in Dentistry
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    • 제43권3호
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    • pp.145-151
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    • 2013
  • Purpose: This study was performed to evaluate and compare the radiopacity of dentin, enamel, and 8 restorative composites on conventional radiograph and digital images with different resolutions. Materials and Methods: Specimens were fabricated from 8 materials and human molars were longitudinally sectioned 1.0 mm thick to include both enamel and dentin. The specimens and tooth sections were imaged by conventional radiograph using #4 sized intraoral film and digital images were taken in high speed and high resolution modes using a phosphor storage plate. Densitometric evaluation of the enamel, dentin, restorative materials, a lead sheet, and an aluminum step wedge was performed on the radiographic images. For the evaluation, the Al equivalent (mm) for each material was calculated. The data were analyzed using one-way ANOVA and Tukey's test (p<0.05), considering the material factor and then the radiographic method factor, individually. Results: The high speed mode allowed the highest radiopacity, while the high resolution mode generated the lowest values. Furthermore, the high resolution mode was the most efficient method for radiographic differentiation between restorative composites and dentin. The conventional radiograph was the most effective in enabling differentiation between enamel and composites. The high speed mode was the least effective in enabling radiographic differentiation between the dental tissues and restorative composites. Conclusion: The high speed mode of digital imaging was not effective for differentiation between enamel and composites. This made it less effective than the high resolution mode and conventional radiographs. All of the composites evaluated showed radiopacity values that fit the ISO 4049 recommendations.

연강 판재에 대한 연강 구의 고속경사충돌 수치해석 (Numerical Simulation of High-Velocity Oblique Impact of Mild Steel Spheres Against Mild Steel Plates)

  • 유요한;장순남;정동택
    • 대한기계학회논문집A
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    • 제26권3호
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    • pp.576-585
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    • 2002
  • A three-dimensional Lagrangian explicit time-integration finite element code for analyzing the dynamic impact phenomena was developed. It uses four node tetrahedral elements. In order to consider the effects of strain rate hardening, strain hardening and thermal softening, which are frequently observed in high-velocity deformation phenomena, Johnson-Cook model is used as constitutive model. For more accurate and robust contact force computation, the defense node contact algorithm was adopted and implemented. In order to evaluate the performance of the newly developed three-dimensional hydrocode NET3D, numerical simulations of the oblique impact of mild steel plate by mild steel sphere were carried out. Ballistic limit about various oblique angle between 0 degree and 80 degree was estimated through a series of simulations with different initial velocities of sphere. Element eroding by equivalent plastic strain was applied to mild steel spheres and targets. Ballistic limits and fracture characteristics obtained from simulation were compared with experimental results conducted by Finnegan et al. From numerical studies, the following conclusions were reached. (1) Simulations could successfully reproduce the key features observed in experiment such as tensile failure termed "disking"at normal impacts and outwards bending of partially formed plus segments termed "hinge-mode"at oblique impacts. (2) Simulation results fur 60 degrees oblique impact at 0.70 km/s and 0.91 km/s were compared with experimental results and Eulerian hydrocode CTH simulation results. The Lagrangian code NET3D is superior to Eulerian code CTH in the computational accuracy. Agreement with the experimentally obtained final deformed cross-sections of the projectile is excellent. (3) Agreement with the experimental ballistic limit data, particularly at the high-obliquity impacts, is reasonably good. (4) The simulation result is not very sensitive to eroding condition but slightly influenced by friction coefficient.

수직진동 사용성 기준을 고려한 바닥판 두께 제안 (Probability Based Determination of Slab Thickness Satisfying Floor Vibration Criteria)

  • 이민정;남상욱;한상환
    • 콘크리트학회논문집
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    • 제17권5호
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    • pp.687-694
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    • 2005
  • 건설 재료와 기술의 발달로 건축물이 장스팬화 ·경량화 되어 가고 있다. 이로 인해 건축물 바닥의 고유진동수(Frequency)와 감쇠비(damping ratio)가 감소함에 따라 거주자들의 바닥판의 수직진동에 대한 문제가 발생하고 있다 그러나 현행 사용성 기준은 바닥판의 최대 정적 처짐에 의해 결정하고 있다. 하지만 선행연구(Han et al., 2003)에서 현행 기준을 만족하는 바닥이 수직진동에 대한 사용성 기준을 만족하지 못하는 것을 볼 수 있다. 따라서 본 연구에서는 거주자들의 뒤꿈치 충격하중에 대한 수직진동 사용성 기준을 만족하는 바닥 두께를 제안하고자 하였다. 슬래브 재료의 특성과 뒤꿈치 충격하중 및 마감 고정하중의 불확실성을 고려하기 위해 Monte Carlo Simulation을 사용하여 확률적으로 접근하였다. 그 결과 4변 단순지지의 경우 두께가 스팬 길이의 $1/14\~1/17$에서, 4변 고정지지의 경우 스팬 길이의 $1/18\~1/25$인 경우에 초과 확률이$0\%$에 도달하였다.

외측 도달법을 이용한 관절내 종골 골절의 수술적 치료 (Surgical Treatment Using a Lateral Approach in Intra-articular Fractures of the Calcaneus)

  • 고영도;정훈;권영삼
    • Journal of Trauma and Injury
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    • 제18권1호
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    • pp.64-69
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    • 2005
  • Purpose: We report the radiologic and the clinical results for surgical treatment of calcaneal fractures involving the subtalar joint. Methods: We evaluated the findings of radiographs and computed tomographs of 39 patients (40 cases) with intra-articular calcaneal fractures. The fractures were treated with open reduction via an extended lateral approach and internal fixation using a plate. We assessed the radiologic results, such as the $B{\ddot{o}}hler$ angle, the Gissane angle, and the height/width ratio. We assessed the clinical results based on the critieria of Salama et al. Results: According to the Essex-Lopresti classification, 9 cases were classified as tongue type and 31 cases as joint depression type. According to the Sanders classification, 10 cases were classified as type IIA, 4 cases as IIB, 16 cases as IIIAB, 4 cases as IIIAC, and 6 cases as type IV. The mean preoperative $B{\ddot{o}}hler$ angle was 7.7, the mean postoperative $B{\ddot{o}}hler$ angle was 21.1, and the mean last follow-up $B{\ddot{o}}hler$ angle was 16.8. Clinical results classified as 10 excellent, 13 good, 11 fair, and 6 poor. Conclusion: In the treatment of intra-articular fractures of the calcaneus, open reduction via an extended lateral approach seems to be a useful method in that it can provide direct exposure of the subtalar joint with little morbidity.

고온형 멤브레인을 사용한 메탄올 개질 연료전지의 개질기 일체형 평판 설계 (Planar fuel cell design integrated with methanol reformer by using a high temperature membrane)

  • 김성한;장재혁;길재형;이홍렬;차혜연;구보성;정창렬;쿤두;미씨;오용수
    • 한국신재생에너지학회:학술대회논문집
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    • 한국신재생에너지학회 2006년도 추계학술대회
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    • pp.467-470
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    • 2006
  • For a mobile application such as cellular phone, micro fuel cells should be extremely compact and thin. RHFC can be an alternative solution because RHFC gives higher power density than DMFC and does not need ahydrogen storage vessel In this paper, RHFC using methanol fuel is made as a novel planar design without a PROX. Both reformer and cell are made closely in a same plate to share the heater of reformer with the cell. The PBI membrane is used in the cell. The reason is that high temperature of reformer can cause a performance drop when perfluorosulfonic acid membrane such as Nafion is used such a high temperature operation also guarantees the higher CO tolerance to MEA catalyst. The cell is designed as an air-breathing type which the cathode of the cell is opened to the air. The commercial Cu/ZnO/Al2O3 steam reformer catalyst is packed in reformer channel. The active area of MEA is $11.9cm^2$ and the peak power density was $27.5mW/cm^2$.

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HACCP의 적용을 위한 피자 전문 레스토랑의 위생관리 기준 설정 -피자생산을 중심으로- (Establishment of Hygienic Standards for Pizza Restaurant Based on HACCP Concept -Focused on Pizza Production-)

  • 이복희;허경숙;김인호
    • 한국식품과학회지
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    • 제36권1호
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    • pp.174-182
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    • 2004
  • Hygienic standards for pizza specialty restaurant located in Seoul during summer, 2000 were established based on HACCP concept by measuring temperature, time, pH, $A_{w}$ and microbiological assessments of pizza, and evaluation of hygienic conditions of kitchens and workers. Kitchen and worker conditions were average 1.2 and 1.0 (3 point Sly's scale), respectively, Microbial contaminations occurred at $5-60^{\circ}C$, pH above 5.0, and $A_{w}$ (0.93-0.98). Microbial assessments for pizza processing revealed $1.5{\times}10^{2}-3.9{\times}10^{8}\;CFU/g$ of TPC and $0.5{\times}10^{1}-1.6{\times}10^{7}\;CFU/g$ of coliforms, exceeding standards ($TPC\;10^{6}\;CFU/g\;and\;coliform\;10^{3}\;CFU/g$) established by Solberg et al., although significantly decreased after baking. S. aureus was not discovered, but Salmonella was found in onions. Tools and containers such as pizza cutting knife, topping container, serving bowl, pizza plate, working board, and dough kneading board contained $6.2{\times}10^{2}-1.1{\times}10^{9}\;CFU/g$ of TPC, $2.0{\times}10^{1}-6.2{\times}10^{3}\;CFU/g$ of coliforms. Workers' hands contained $3.1{\times}10^{4}\;CFU/g$ of TPC and S. aureus as compared to safety standards of Harrigan and McCance (500 and 10 CFU/g of TPC and coliforms per $100cm^{2}$). CCPs (critical control points) were determined as receiving, topping, and baking according to CCP decision tree analysis. Results suggest purchase of quality materials, careful monitoring of time and temperature, hygienic use of tools and utensils, and sanitary practicer by workers are recommended as control points for safe pizza production.

Non linear soil structure interaction of space frame-pile foundation-soil system

  • Chore, H.S.;Ingle, R.K.;Sawant, V.A.
    • Structural Engineering and Mechanics
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    • 제49권1호
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    • pp.95-110
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    • 2014
  • The study deals with physical modeling of space frame-pile foundation and soil system using finite element models. The superstructure frame is analyzed using complete three-dimensional finite element method where the component of the frame such as slab, beam and columns are descretized using 20 node isoparametric continuum elements. Initially, the frame is analyzed assuming the fixed column bases. Later the pile foundation is worked out separately wherein the simplified models of finite elements such as beam and plate element are used for pile and pile cap, respectively. The non-linear behaviour of soil mass is incorporated by idealizing the soil as non-linear springs using p-y curve along the lines similar to that by Georgiadis et al. (1992). For analysis of pile foundation, the non-linearity of soil via p-y curve approach is incorporated using the incremental approach. The interaction analysis is conducted for the parametric study. The non-linearity of soil is further incorporated using iterative approach, i.e., secant modulus approach, in the interaction analysis. The effect the various parameters of the pile foundation such as spacing in a group and configuration of the pile group is evaluated on the response of superstructure owing to non-linearity of the soil. The response included the displacement at the top of the frame and bending moment in columns. The non-linearity of soil increases the top displacement in the range of 7.8%-16.7%. However, its effect is found very marginal on the absolute maximum moment in columns. The hogging moment decreases by 0.005% while sagging moment increases by 0.02%.