• 한국재료학회지
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• 제11권12호
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• pp.1057-1062
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• 2001

We investigated the change of mechanical properties for TiNi shape memory alloy by heat treatment. 6061Al matrix composites with TiNi shape memory alloy as reinforcement were fabricated by vacuum casting. TiNi alloy has the maximum tensile strength at 673K treated and there is no change of tensile strength and hardness at 448K treated. The composites, prepared by vacuum casting, showed good interface bonding by vacuum casting. It was about 3$\mu\textrm{m}$ of thickness of the diffusion layer. Tensile strength of the composite was in higher than that of 6061Al alloy as increased value of about 70MPa at room temperature and about 110MPa at 363K. We thought that the increase of the tensile strength at 363K was due to reverse transformation of the TiNi shape memory alloy.

• 비파괴검사학회지
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• 제18권2호
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• pp.103-111
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• 1998

입자 보강 복합재료의 부피분율을 평가하기 위한 초음파 비파괴 방법을 제시하였다. 제안된 방법은 복합재의 미시구조를 설명할 수 있는 이론 모델과 초음파의 속도 측정을 필요로 한다. 측정한 속도를 이론예측값과 같게 두면 미지의 입자 부피분율이 계산된다. Mori-Tanaka 방법에 기초한 탄성계수 해석 모델이 소개되어 있다. 이러한 접근 방법을 SiC 입자 보강 Al 기지 ($SiC_p/Al$) 복합재에 적용하였다. 이 방법으로 보강재의 부피분율을 비교적 정확하게 결정할 수 있었다. 또한 금속간 화합물이 부피분율 평가에 미치는 영향을 논하였다. 이 방법은 입자 보강 금속기지 복합재의 생산현장에서 복합재의 품질 평가를 위하여 적용될 수 있다.

• 대한금속재료학회지
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• 제50권2호
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• pp.176-182
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• 2012

The main purpose of this study was to evaluate the endurance against Al alloy melts and wear resistance of an in-situ synthesized titanium matrix composite (TMC) sleeve for aluminum alloy die-casting. The conventional die-casting shot sleeve material was STD61 tool steel. TMCs have great thermal stability, wear and oxidation resistance. The in-situ reaction between Ti and $B_4C$ leads to two kinds of thermodynamically stable reinforcements, such as TiBw and TiCp. To evaluate the feasibility of the application to a TMCs diecasting shot sleeve, the interfacial reaction behavior was examined between Al alloys melts with TMCs and STD61 tool steel. The pin-on-disk type dry sliding wear test was also investigated for TMCs and STD61 tool steel.

• 한국세라믹학회지
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• 제25권3호
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• pp.284-292
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• 1988

Alumina-zirconia composite powders for the purpose of improving fracture toughness and thermal shock resistance of alumina were prepared by the emulsion-kerosene drying method. The average particle size of composite powders was less then 1 $\mu\textrm{m}$ and their shapes were spherical. It was shown that the average particle size of composite powders decreased with the concentration of metal-salt in solution and the amount of span 80 added when preparing emulsions. The structure of all zirconia in composite powders heat-treated at 1200$^{\circ}C$ was a tetragonal form at room temperature. This result implied that fine zirconia particles were homogeneously dispersed in the alumina matrix.

• 소성∙가공
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• 제19권7호
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• pp.423-428
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• 2010

Carbon nanotubes(CNTs) are expected to be ideal reinforcements of metal matrix composite materials used in aircraft and sports industries due to their high strength and low density. In this study, a high pressure torsion(HPT) process at an elevated temperature(473K) was employed to achieve both powder consolidation and grain refinement of aluminummatrix nanocomposites reinforced by 5vol% CNTs. CNT/Al nanocomposite powders were fabricated using a novel molecular-level mixing process to enhance the interface bonding between the CNTs and metal matrix before the HPT process. The HPT processed disks were composed of mostly equilibrium grain boundaries. The CNT-reinforced ultrafine grained microstructural features resulted in high strength and good ductility.

• 한국분말재료학회지
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• 제9권6호
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• pp.394-408
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• 2002

Nanostructured high strength metastable Al-, Mg- and Ti-based alloys containing different amorphous, quasicrystalline and nanocrystalline phases are synthesized by non-equilibrium processing techniques. Such alloys can be prepared by quenching from the melt or by powder metallurgy techniques. This paper focuses on one hand on mechanically alloyed and ball milled powders containing different volume fractions of amorphous or nano-(quasi)crystalline phases, consolidated bulk specimens and, on the other hand. on cast specimens containing different constituent phases with different length-scale. As one example. $Mg_{55}Y_{15}Cu_{30}$- based metallic glass matrix composites are produced by mechanical alloying of elemental powder mixtures containing up to 30 vol.% $Y_2O_3$ particles. The comparison with the particle-free metallic glass reveals that the nanosized second phase oxide particles do not significantly affect the glass-forming ability upon mechanical alloying despite some limited particle dissolution. A supercooled liquid region with an extension of about 50 K can be maintained in the presence of the oxides. The distinct viscosity decrease in the supercooled liquid regime allows to consolidate the powders into bulk samples by uniaxial hot pressing. The $Y_2O_3$ additions increase the mechanical strength of the composites compared to the $Mg_{55}Y_{15}Cu_{30}$ metallic glass. The second example deals with Al-Mn-Ce and Al-Cu-Fe composites with quasicrystalline particles as reinforcements, which are prepared by quenching from the melt and by powder metallurgy. $Al_{98-x}Mn_xCe_2$ (x =5,6,7) melt-spun ribbons containing a major quasicrystalline phase coexisting with an Al-matrix on a nanometer scale are pulverized by ball milling. The powders are consolidated by hot extrusion. Grain growth during consolidation causes the formation of a micrometer-scale microstructure. Mechanical alloying of $Al_{63}Cu_{25}Fe_{12}$ leads to single-phase quasicrystalline powders. which are blended with different volume fractions of pure Al-powder and hot extruded forming $Al_{100-x}$$(Al_{0.63}Cu_{0.25}Fe_{0.12})_x$ (x = 40,50,60,80) micrometer-scale composites. Compression test data reveal a high yield strength of ${\sigma}_y{\geq}$700 MPa and a ductility of ${\varepsilon}_{pl}{\geq}$5% for than the Al-Mn-Ce bulk samples. The strength level of the Al-Cu-Fe alloys is ${\sigma}_y{\leq}$550 MPa significantly lower. By the addition of different amounts of aluminum, the mechanical properties can be tuned to a wide range. Finally, a bulk metallic glass-forming Ti-Cu-Ni-Sn alloy with in situ formed composite microstructure prepared by both centrifugal and injection casting presents more than 6% plastic strain under compressive stress at room temperature. The in situ formed composite contains dendritic hcp Ti solid solution precipitates and a few $Ti_3Sn,\;{\beta}$-(Cu, Sn) grains dispersed in a glassy matrix. The composite micro- structure can avoid the development of the highly localized shear bands typical for the room temperature defor-mation of monolithic glasses. Instead, widely developed shear bands with evident protuberance are observed. resulting in significant yielding and homogeneous plastic deformation over the entire sample.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2008년도 추계학술대회 논문집
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• pp.199-202
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• 2008

In this study, we investigated the thermal properties of $Zr_{66.4}Nb_{6.4}Cu_{10.5}Ni_{8.7}Al_{8.0}$ by using a differential scanning calorimeter (DSC), and then analyzed the composition of dendrite phase by using X-ray diffraction (XRD). A series of uniaxial compression tests has been performed under the strain rates between $10^{-5}/s$ and $10^{-2}/s$ at room temperature and near SLR. This BMGC has higher high temperature strength than other Zr-based monolithic BMGs because in-situ formed crystalline phases hinder a feasible viscous flow of amorphous matrix. Warm formability is also estimated by laboratory-scale extrusion test within supercooled liquid region. It was found that BMGC has poor formability compared with nother Zr-based bulk metallic glass composite presumably due to large volume fraction of 'brittle' crystalline phases distributed within amorphous matrix.

• 한국공작기계학회:학술대회논문집
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• 한국공작기계학회 1996년도 추계학술대회 논문
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• pp.52-57
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• 1996

Conductive Ceramic Matrix Composite(CMC) of TIC/Al2O3 and Metal Matrix Composite (MMC) of SiC/Al were experienced by the die sinking Electrical Discharge Machining(EDM) for different current and duty factor according to negative polarity. Inthis experimental study Material Removal Rate(MRR) maximum surface roughness four point bending stress distribution and Scanning Electron Microscopy(SEM) Photographs were analysed. the higher MRR was obtained for CMC than MMC but slowly decreased around duty factor of 0.67 for MMC and better surface morphology was found CMC than MMC. The SEM photographs of discharge traces for CMC showe uniform shape about 100 to 200${\mu}{\textrm}{m}$ in diameter but MMC showed irregular shape.

• Steel and Composite Structures
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• 제45권5호
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• pp.767-774
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• 2022

A geometrically nonlinear stability analysis of sandwich annular plates with cellular core and particle-reinforced composite layers has been performed in the present research. The particles are powders of graphene oxide (GOP) which act as nanoscale filler of epoxy matrix. To this regard, Halpin-Tsai micromechanical scheme has been used to define the material properties of the layers. A square shaped core has been considered for which the material properties have been defined based on the relative density concept. Large deflection theory of thin shells has been selected to develop the complete formulation of sandwich plate. The geometrically nonlinear stability analysis of sandwich annular plates has been carried out by indicating that the buckling load is dependent on particle amount, thickness of layer and core relative density.

• 한국복합재료학회:학술대회논문집
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• 한국복합재료학회 2002년도 춘계학술발표대회 논문집
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• pp.97-100
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• 2002

In this research, the impact behavior of the boundary between MMC-reinforced SiC whisker and Al alloy were studied. It is known that the resultant of the interfacial reaction between SiC whisker and Al alloy has brittle and low toughness property. In this paper, impact behavior of graded MMC & Al alloy shows the interfacial opening at the boundary. Generally this phenomenon is generated by thermal residual stress, brittle interfacial reaction resultant and difference of the deflection. So, these results may be interpreted as a macroscopic method of measuring the interfacial strength between matrix and reinforcement