• 제목/요약/키워드: Age hardening

검색결과 144건 처리시간 0.056초

플라이애쉬를 대량 사용한 고강도 콘크리트에 관한 실험적 연구 (The Experimental Study on High Strength Concrete of High Volume Fly-Ash)

  • 이동하;서동훈;전판근;백민수;임남기;정상진
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 2002년도 가을 학술발표회 논문집
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    • pp.275-280
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    • 2002
  • To study of high volume fly -ash concrete replace cement and fine aggregate together. Proportion consideration economy cost and performance improve replacement high volume fly-ash. Experimentation study of high-strength which cement about fly-ash replacement maximum 50%Flash concrete tested slump, air contest, setting and Hardening concrete tested day of age 1, 3, 7, 28, 91 compression strength in underwater curing. Purpose of study is consultation materials in field that variety of fly ash replacement concrete mix proportion comparison and valuation.

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폴리머 콘크리트의 초기경화특성에 관한 실험적 연구 (An Experimental Study on Hardening Performance at Early Age of Polymer Concrete)

  • 오병환;이형준;차수원;장제욱
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 1993년도 가을 학술발표회 논문집
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    • pp.162-166
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    • 1993
  • 폴리머 콘크리트에 대한 연구는 세계 각국에서 오래전부터 수행하여 구조물에 적용한다든가 보수재로 사용하고 있는데 비해 국내에서의 연구는 최근에 시작되었으며, 폴리머 콘크리트에 대한 재료의 기초적 특성 연구가 활발히 진행되고 있으나 체계적인 연구 결과나 실용화 실적이 적다. 따라서 본연구에서는 폴리머 콘크리트의 초기경화 특성을 고찰하여 콘크리트 포장의 보수재료로서의 폴리머 콘크리트의 활용 토대를 구축하고자 한다.

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저발열 콘크리트 수화열 평가의 실험적 연구 (Belite rich 시멘트 중심) (An Experimental Study on the Evaluation of Hydration Heat of Low Heat Concrete (in case of Belite rich Cement))

  • 현석훈;박춘근;신영인;김용호
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 1996년도 가을 학술발표회 논문집
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    • pp.352-357
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    • 1996
  • In hardening massive concrete, the heat of hydation gives rise to considerable thermal gradientsand thermal stresses, which might cause early age cracking. This paper deals with the results of evaluation of hydration heat of low hear concrete, using Belite rich cement (low heat cement) and compared with OPC, slag added cement and fly ash addedcement. Result of evaluation of hydration are presented in this paper. The concrete made with Belite rich cement gets low temperature of center point and low thermal gradients between surface and center points.

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Strength Development of High-Strength Concrete in Structure

  • Msuda, Yochihiro
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 2000년도 가을 학술발표회논문집(I)
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    • pp.31-45
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    • 2000
  • Because of the high unit cement content in the concrete mix, major concrete temperature rises are observed in the initial stages of hardening in structural members with large cross-sections made of high-strength concrete. While this temperature rise in the initial stages of hardening contributes to the initial development of the concrete strength, it also causes thermal cracking and obstructs medium to long-term increases of the concrete strength. In the study reports below, investigations were made on the effects of the concrete temperature rise in the initial stages of hardening on the medium to long-term development of the strength of structural concrete between the ages of 28 and 91 days. In the study, comparisons were made, for example, between the compressive strength of a control specimen subjected to standard curing at 28 days and the compressive strength of core specimens taken from structural members, and observations were made on the methods of evaluating the concrete strength in structure, defined here as the compressive strength of core specimens at 91 days. The results obtained indicate that, when the maximum temperature of the concrete is the structure does not exceed $60^{\circ}C$, the concrete strength in structure at the age of long-term will generally be greater than the compressive strength of the standard-curing specimens at 28 days, allowing one to evaluate the strength of the structural concrete in terms of the compressive strength of the 28-days standard-curing specimens. When, on the other hand, the maximum temperature of the concrete in the structure exceeds $60^{\circ}C$, the strength in concrete structure may be smaller than the compressive strength of the 28-days standard-curing specimens, creating risks in the evaluation of the concrete strength in structure by latter.

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수축저감제의 종류 및 혼입률에 따른 변형경화형 시멘트복합체의 역학적 특성 (Effects of Shrinkage Reducing Agent (SRA) Type and Content on Mechanical Properties of Strain Hardening Cement Composite (SHCC))

  • 한승주;장석준;길배수;최무진;윤현도
    • 콘크리트학회논문집
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    • 제28권1호
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    • pp.41-48
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    • 2016
  • 본 연구는 두 종류의 수축저감제를 혼입한 변형경화형 시멘트 복합체(SHCC)의 압축, 인장 및 휨 특성을 평가하기 위하여 계획되었으며, 재령과 수축저감제의 종류 및 혼입률을 변수로 진행되었다. SHCC는 설계기준압축강도 50 MPa이며, 섬유는 PVA 섬유를 2.2% 혼입하였다. 배합에 혼입된 수축저감제는 상변이 물질로 수화현상으로 발생되는 열을 흡수 또는 방출하여 급격한 수축 및 팽창을 제어하는 물질이다. 수축저감제의 혼입에 대한 영향은 선변형 길이변화 실험과 압축, 인장 및 휨 성능의 측면에서 평가되었으며, 수축저감제를 혼입할 경우 초기 재령에서의 수축량이 감소되었다. 또한 수축저감제를 혼입함에 따라 균열 분산 성능과 인장 및 휨 성능이 개선되었다.

Fabrication of Two-Layered $Al-B_4C$ Composites by Conventional Hot Pressing Uuder Nitrogen Atmosphere and Their Characterization

  • Bedir Fevzi
    • Journal of Mechanical Science and Technology
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    • 제20권7호
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    • pp.1002-1011
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    • 2006
  • In this study, we describe the conventional hot pressing (CHP) of layered $Al-B_4C$ composites and their characterization. The matrix alloy Al-5 wt.%Cu was prepared from elemental powder mixtures. The metal and B4C powders were mixed to produce either $Al-Cu-10vol.%B_4C$ or $Al-Cu-30vol.%B_4C$ combinations. Then, these powder mixtures were stacked as layers in the hot pressing die to form a two-layered composite. Hot pressing was carried out under nitrogen atmosphere to produce $30\times40\times5mm$ specimens. Microstructural features and age hardening characteristics of composites were determined by specimens cut longitudinally. The flexural strength of both layered composites and their monolithic counterparts were investigated via three point bending tests. In the case of layered specimens of both $10vol.%B_4C$ and $30vol.%B_4C$ containing layers were loaded for three-point test. The results show that a homogeneous distribution of $B_4C$ particles in the matrix alloy which is free of pores, can be obtained by CHP method. The ageing behavior of the composites was found to be influenced by the reinforced materials, i.e. higher hardness values were reached in 8 hrs for the composites than that for the matrix alloy. Flexural strength test showed that two-layered composites exhibited improved damage tolerance depending on layer arrangement. Microstructural investigation of the fracture surfaces of the bending specimens was performed by means of scanning electron microscope (SEM). While layer with lower reinforcement content exhibited large plastic deformation under loading, the other with higher reinforcement content exhibited less plastic deformation.

주조방법에 따른 주얼리 제품(14K yellow gold alloy)의 특성비교 및 열처리 전과 후 특성변화

  • 윤돈규;서진교;신소라;안용길;박종완
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2012년도 제42회 동계 정기 학술대회 초록집
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    • pp.238-238
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    • 2012
  • 현재 국내 주얼리(gold alloy) 제품을 생산함에 있어 주조 방법은 크게 대기 중 주조(흡입주조) 방법과 진공주조 방법으로 나누어진다. 국내 주얼리 제조업체의 약 90%이상이 대기 중에서 주조하는 흡입주조방법을 통해 제품을 제작하고 있고, 국외의 경우, 대다수 진공주조방법을 통해 제품을 제작하고 있다. 본 연구에서는 주얼리 제품을 생산할 때 사용되는 합금재료(master alloy)가 동일한 조건에서 주조방법을 달리하여 각각 24개씩 총 48개의 14K yellow gold alloy 제품을 제작한 후 열처리를 통해 각각의 기계적, 물리적 특성분석을 비교 분석하였다. EPMA (Electron Probe Micro Analysis)분석을 통해 합금재료 및 제품의 구성성분을 조사하였고, ICP-MS (Inductively Coupled Plasma Mass Spectroscopy)를 사용하여 성분에 대한 정량분석을 실시하였다. 용체화처리(solid solution treatment)는 $700^{\circ}C$, 30분의 조건으로 실시하였고, 시효경화처리(age-hardening)는 $200{\sim}300^{\circ}C$의 온도범위에서 $50^{\circ}C$ 간격으로 실시하였다. 열처리 전과 후 시료의 grain 들의 배열 및 size 변화를 관찰하기 위해 식각 후 OM (optical microscope) 및 SEM (Scanning Electron Microscope)를 통해 분석하였다. 열처리 전 제품의 경도측정결과 대기 중 흡입주조방법 및 진공 주조방법을 통해 제작된 제품이 각각 119 Hv, 126 Hv로 나타났고, 용체화 처리 후 98 Hv, 92 Hv로 감소하였다. 시효경화 처리 후의 경도변화는 대기 중 흡입주조 및 진공주조방법을 통해 제작된 제품 모두 $270^{\circ}C$에서 각각 154 HV, 166 HV로 가장 높은 경도 값을 나타내었고, $270^{\circ}C$ 이상에서는 과시효(over aging)현상으로 인해 경도 값이 다시 감소하는 경향을 나타내었다. EPMA mapping 분석을 통해 주조방법에 따라 각각 제품의 구성성분분포도를 확인하였다. 이를 통해 열처리 전 다소 불균일하게 분포되었던 성분들이 열처리 후 균일해짐을 확인할 수 있었다.

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열분석법에 의한 Al-2.1Li-2.9Cu합금이 석출현상에 미치는 In 첨가의 영향 (Effects of In on the Precipitation Phenomena of Al-2.1Li-2.9Cu Alloy by Differential Scanning Calorimetry)

  • 박태원;송영범;이용연
    • 열처리공학회지
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    • 제10권4호
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    • pp.237-245
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    • 1997
  • A study was conducted to examine the effects of In addition on the precipitation behaviors of Al-2.1Li-2.9Cu alloy by differential scanning calorimetry, transmission electron microscopy and micro-hardness tester. DSC analysis was measured over the temperature range of $25{\sim}550^{\circ}C$ at a heating rate of $2{\sim}20^{\circ}C$/min. The heat evolution peaks due to the formation of GP zone and ${\delta}$'phase shift to higher temperature and the peaks to $T_1$ and ${\theta}$'phases shift to lower temperature by In addition. From this result, it was proved that the formation of GP zone and ${\delta}$'phase is suppresed whereas that of $T_1$ and ${\theta}$'phases are accelerated by the In addition of 0.15wt%. The age hardening curve aged at $190^{\circ}C$ showed that the In bearing alloy(alloy B) has more faster age hardening response and a higher peak hardness than In-free alloy(alloy A), attributed to the fine and homogeneous distribution of $T_1$ and ${\theta}$'phases. The activation energies for the formation of ${\delta}$'phase in In-free and In-bearing alloys are 22.3kcal/mol and 18.6kcal/mol, respectively. Those for $T_1(+{\theta}^{\prime})$ phase of In-free and In-bearing alloys are 24.3 and 37.5kcal/mol, respectively. Quenched-in excess vacancies play an important role to the formation of precipitates.

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Effects of Cu and Ag Addition on Nanocluster Formation Behavior in Al-Mg-Si Alloys

  • Kim, Jae-Hwang;Tezuka, Hiroyasu;Kobayashi, Equo;Sato, Tatsuo
    • 한국재료학회지
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    • 제22권7호
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    • pp.329-334
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    • 2012
  • Two types of nanoclusters, termed Cluster (1) and Cluster (2) here, both play an important role in the age-hardening behavior in Al-Mg-Si alloys. Small amounts of additions of Cu and Ag affect the formation of nanoclusters. Two exothermic peaks were clearly detected in differential scanning calorimetry(DSC) curves by means of peak separation by the Gaussian method in the base, Cu-added, Ag-added and Cu-Ag-added Al-Mg-Si alloys. The formation of nanoclusters in the initial stage of natural aging was suppressed in the Ag-added and Cu-Ag-added alloys, while the formation of nanoclusters was enhanced at an aging time longer than 259.2 ks(3 days) of natural aging with the addition Cu and Ag. The formation of nanoclusters while aging at $100^{\circ}C$ was accelerated in the Cu-added, Ag-added and Cu-Ag-added alloys due to the attractive interaction between the Cu and Ag atoms and the Mg atoms. The influence of additions of Cu and Ag on the clustering behavior during low-temperature aging was well characterized based on the interaction energies among solute atoms and on vacancies derived from the first-principle calculation of the full-potential Korrinaga-Kohn-Rostoker(FPKKR)-Green function method. The effects of low Cu and Ag additions on the formation of nanoclusters were also discussed based on the age-hardening phenomena.