• Title/Summary/Keyword: Ag nano-powder

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Preparation of Ag Nano-Powder from Aqueous Silver Nitrate Solution through Reduction with Hydrazine Hydrate (Hydrazine Hydrate 환원(還元)에 의한 질산은(窒酸銀) 수용액(水溶液)으로부터 은(銀) 나노분말(粉末)의 제조(製造) 연구(硏究))

  • Lee, Hwa-Young
    • Resources Recycling
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    • v.15 no.4 s.72
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    • pp.19-26
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    • 2006
  • The preparation of Ag nano-powder from aqueous silver nitrate solution, which would be available for the recycling of silver bearing wastes, was investigated by a reductive precipitation reaction using hydrazine hydrate as a reducing agent. Silver solution was prepared by dissolving silver nitrate with distilled water, and then the dispersant, Tamol NN8906 or Tween 20, was also mixed to avoid the agglomeration of particles during the reductive reaction followed by the addition of hydrazine hydrate to prepare Ag nano-particles. Ag particles obtained from the reduction reaction from silver solution were characterized using the particle size analyzer and TEM to determine the particle size distribution and morphology. It was found that about 100% excess of hydrazine hydrate was required to reduce completely silver ions in the solution. Ag powders with very narrow distribution could be obtained when Tamol NN8906 was used as the dispersant. In case of Tween 20, the particle size distribution showed typically the bimodal or multimodal distribution and the morphology of Ag particles was found to be irregular shape in both cases.

Effect of Nano-Sized Silver Powders in CNT Paste on Field Emission Characteristics of Carbon Nanotube Cathode (탄소나노튜브 캐소드의 전계방출 특성에 미치는 CNT 페이스트용 나노입자 은분말의 영향)

  • An, Young-Je;Lee, Ji-Eon;Shin, Heon-Cheol;Cho, Young-Rae
    • Korean Journal of Materials Research
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    • v.18 no.1
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    • pp.12-17
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    • 2008
  • Carbon nanotube (CNT) cathodes were fabricated using nano-sized silver (Ag) powders as a bonding material between the CNTs and cathode electrodes. The effects of the powder size on the sintering behavior, the current density and emission image for CNT cathodes were investigated. As the diameter of the Ag powders decreases to 10 nm, the sintering temperature of the CNT cathode was lowered primarily due to the higher specific surface area of the Ag powders. In this study, it was demonstrated that nano-sized Ag powders can be feasibly used as a bonding material for a screen-printed CNT cathode, yielding a high current density and a uniform emission image.

The effects of nanofluid containing metal nano-powder on heat transfer (나노금속분말을 혼합한 용액이 열전달에 미치는 영향)

  • Kim, Hye-Min;Choi, Soon-Ho;Jeong, Jae-Hyun;Jeong, Jae-Hyun
    • Proceedings of the Korean Society of Marine Engineers Conference
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    • 2005.06a
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    • pp.177-182
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    • 2005
  • Many studies have been conducted to increase heat transfer in fluid. One of the various heat transfer enhancement techniques is to suspend fine metallic or nonmetallic solid powder in traditional fluid. Nanofluid is defined at a new kind of heat transfer fluid containing a very small quantity of nanometer particles that are uniformly and stably suspended in a liquid. In this study CuNi or CuAg nano particles are used to investigate heat transfer enhancement. The result shows the thermal conductivity of nanofluid is much higher than that of traditional fluid.

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Fabrication and Characterization of Ag-coated BCP Scaffold Derived from Sponge Replica Process (스폰지 복제법을 이용한 Ag 코팅 BCP 지지체의 제조 및 평가)

  • Kim, Min-Sung;Kim, Young-Hee;Song, Ho-Yeon;Min, Young-Ki;Lee, Byong-Taek
    • Korean Journal of Materials Research
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    • v.20 no.8
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    • pp.418-422
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    • 2010
  • As a starting material, BCP (biphasic calcium phosphate) nano powder was synthesized by a hydrothermal microwave-assisted process. A highly porous BCP scaffold was fabricated by the sponge replica method using 60 ppi (pore per inch) of polyurethane sponge. The BCP scaffold had interconnected pores ranging from $100\;{\mu}m$ to $1000\;{\mu}m$, which were similar to natural cancellous bone. To realize the antibacterial property, a microwave-assisted nano Ag spot coating process was used. The morphology and distribution of nano Ag particles were different depending on the coating conditions, such as concentration of the $AgNO_3$ solution, microwave irradiation times, etc. With an increased microwave irradiation time, the amount of coated nano Ag particles increased. The surface of the BCP scaffold was totally covered with nano Ag particles homogeneously at 20 seconds of microwave irradiation time when 0.6 g of $AgNO_3$ was used. With an increased amount of $AgNO_3$ and irradiation time, the size of the coated particles increased. Antibacterial activities of the solution extracted from the Ag-coated BCP scaffold were examined against gram-negative (Escherichia coli) and gram-positive bacteria (Staphylococcus aureus). When 0.6 g of $AgNO_3$ was used for coating the Ag-coated scaffold, it showed higher antibacterial activities than that of the Ag-coated scaffold using 0.8 g of $AgNO_3$.

Production of Nano Powder by Using Transferred Thermal Plasma (이송식 열 플라즈마를 이용한 나노입자 제조)

  • Jo, Tae-Jin;Kim, Heon-Chang;Han, Chang-Suk;Kim, Jwa-Yeon;Kim, Young-Suk
    • Journal of Powder Materials
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    • v.14 no.2 s.61
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    • pp.116-122
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    • 2007
  • It is well known that thermal plasma process has lots of advantages such as high temperature and good quality for synthesis of nano particles. In this research, we attempt the synthesis of nano unitary and composite powder (Ag, Mg-Al, Zr-V-Fe) using transferred thermal plasma. Nano particles of metal alloy, ranging from 20 nm to 150 nm, have been synthesized by this process.

Determination of Fractal Dimension and Surface Characterization of Metal Nano-powder Using Nitrogen Gas Adsorption Method (질소가스흡착법을 이용한 금속 나노분말의 프랙탈 차원 결정 및 표면 특성 평가)

  • Lee, Gyoung-Ja;Uhm, Young-Rang;Rhee, Chang-Kyu
    • Journal of Powder Materials
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    • v.14 no.6
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    • pp.391-398
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    • 2007
  • The surface roughness of Al, Ag and Ni nano-powders which were prepared by pulsed wire evaporation method was quantified based upon the fractal theory. The surface fractal dimensions of metal nano-powders were determined from the linear relationship between In $V/V_{mono}$ and Inln ($P^o/P$) using multi-layer gas adsorption theory. Moreover, the fractal surface image was realized by computer simulation. The relationship between preparation condition and surface characteristics of metal nano-powders was discussed in detail.