• Title/Summary/Keyword: After-Curing

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Effects of 3 different light-curing units on the physico-mechanical properties of bleach-shade resin composites

  • Azin Farzad;Shahin Kasraei;Sahebeh Haghi;Mahboubeh Masoumbeigi;Hassan Torabzadeh;Narges Panahandeh
    • Restorative Dentistry and Endodontics
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    • v.47 no.1
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    • pp.9.1-9.11
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    • 2022
  • Objectives: This study investigated the microhardness, flexural strength, and color stability of bleach-shade resin composites cured with 3 different light-curing units. Materials and Methods: In this in vitro experimental study, 270 samples were fabricated of bleach and A2 shades of 3 commercial resin composites (Point 4, G-aenial Anterior, and Estelite Sigma Quick). Samples (n = 5 for each trial) were cured with Bluephase N, Woodpecker LED.D, and Optilux 501 units and underwent Vickers microhardness and flexural strength tests. The samples were tested after 24 hours of storage in distilled water. Color was assessed using a spectrophotometer immediately after preparation and 24 hours after curing. Data were analyzed using 3-way analysis of variance and the Tukey test (p ≤ 0.001). Results: Samples cured with Optilux exhibited the highest and those cured with LED.D exhibited the lowest microhardness (p = 0.023). The bleach shade of Point 4 composite cured with Optilux displayed the highest flexural strength, while the same composite and shade cured with Sigma Quick exhibited the lowest (p ≤ 0.001). The color change after 24 hours was greatest for the bleach shade of G-aenial cured with Bluephase N and least for the A2 shade of Sigma Quick cured with Optilux (p ≤ 0.001). Conclusions: Light curing with polywave light-emitting diode (LED) yielded results between or statistically similar to those of quartz-tungsten-halogen and monowave LED in the microhardness and flexural strength of both A2 and bleach shades of resin composites. However, the brands of light-curing devices showed significant differences in color stability.

New curing method using gaseous oxidant on sweet potato (Ipomoea batatas)

  • Jin, Hyunjung;Kim, Wook
    • Proceedings of the Korean Society of Crop Science Conference
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    • 2017.06a
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    • pp.39-39
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    • 2017
  • In Asia, sweet potato (Ipomoea batatas) is a very important crop for starch production. Approximately 74.3% of the total sweet potato production quantity is produced in Asia (FAO, 2014) and China is the largest producer of sweet potato. Post-harvest management is particularly important because it is difficult to maintain the quality as well as quantity of sweet potatoes. Despite the importance of post-harvest management, researches on sweet potato have been focused on production-related study such as breeding of new variety, improved techniques of cultivation, so there is limited research on storage after harvest. Curing is a normal practice after sweet potato harvest to promote wound healing and extend postharvest storage life. In Korea, harvested sweet potatoes are usually cured for 4 to 7 days at $30-33^{\circ}C$ and 80-95% relative humidity within one week. Since the optimum storage temperature of sweet potato is regarded as $15-20^{\circ}C$, additional facilities and costs are required to raise the temperature for curing. However, the majority of small farmers do not have the capacity to provide additional facilities and costs. This study was initiated to suggest a new curing method to accelerate the wound healing by applying chemical oxidation to the wound surface of sweet potato. Oxidative stress is known to play an important role in the synthesis of secondary metabolites including lignin. In addition, chemical oxidation can be applied to prevent spoilage caused by microorganisms. Powerful gaseous oxidant with excellent penetration ability and superior sterilization effect was selected for this study. Lignification, weight loss, and spoilage rate of artificially wounded sweet potatoes were investigated after oxidant fumigation. There were clear differences in morphological analysis such as lignification pattern, lignin deposition color, and continuity of lignified cell layers between oxidant-fumigated sweet potatoes and control. These results show that gaseous oxidant can be used to supplement or replace the curing practice, to improve shelf-life as well as curing cost reduction.

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Errors in light-emitting diodes positioning when curing bulk fill and incremental composites: impact on properties after aging

  • Abdulrahman A. Balhaddad;Isadora M. Garcia;Haifa Maktabi;Maria Salem Ibrahim;Qoot Alkhubaizi;Howard Strassler;Fabricio M. Collares;Mary Anne S. Melo
    • Restorative Dentistry and Endodontics
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    • v.46 no.4
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    • pp.51.1-51.13
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    • 2021
  • Objectives: This study aimed to evaluate the effect of improper positioning single-peak and multi-peak lights on color change, microhardness of bottom and top, and surface topography of bulk fill and incremental composites after artificial aging for 1 year. Materials and Methods: Bulk fill and incremental composites were cured using multi-peak and single-peak light-emitting diode (LED) following 4 clinical conditions: (1) optimal condition (no angulation or tip displacement), (2) tip-displacement (2 mm), (3) slight tip angulation (α = 20°) and (4) moderate tip angulation (α = 35°). After 1-year of water aging, the specimens were analyzed for color changes (ΔE), Vickers hardness, surface topography (Ra, Rt, and Rv), and scanning electron microscopy. Results: For samples cured by single-peak LED, the improper positioning significantly increases the color change compared to the optimal position regardless of the type of composite (p < 0.001). For multi-peak LED, the type of resin composite and the curing condition displayed a significant effect on ΔE (p < 0.001). For both LEDs, the Vickers hardness and bottom/top ratio of Vickers hardness were affected by the type of composite and the curing condition (p < 0.01). Conclusions: The bulk fill composite presented greater resistance to wear, higher color stability, and better microhardness than the incremental composite when subjected to improper curing. The multi-peak LED improves curing under improper conditions compared to single-peak LED. Prevention of errors when curing composites requires the attention of all personnel involved in the patient's care once the clinical relevance of the appropriate polymerization reflects on reliable long-term outcomes.

The Effect of Heat Curing Methods on the Protection against Frost Damage at Early Age of the Concrete Under Extremely Cold Climate

  • Jung, Eun-Bong;Shin, Hyun-Sup;Han, Min-Cheol
    • Journal of the Korea Institute of Building Construction
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    • v.13 no.6
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    • pp.513-521
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    • 2013
  • This study aimed to examine whether heat curing methods of concrete subjected to $-10^{\circ}C$ could be effective by varying the combination of heating cable and surface heat insulations. Three different concrete specimens incorporating 30% fly ash with 50% W/B were fabricated to simulate wall, column and slab members with dimensions of $1600{\times}800{\times}200$ mm for slab, $800{\times}600{\times}200$ mm for wall and $800{\times}800{\times}800$ mm for column. For heat curing combinations, Type-1 specimens applied PE film for slab, plywood for wall and column curing. Type-2 specimens applied double layer bubble sheet (2LB) and heating coil for slab, and 50 mm styrofoam for wall and column curing. Type-3 specimen applied 2LB for slab, electrical heating mat for wall and column inside heating enclosure. The test results revealed that the temperature of Type 1 specimen dropped below $0^{\circ}C$ beginning at 48 hours after placement due to its poor heat insulating capability. Type 2 and 3 specimens maintained a temperature of around $5{\sim}10^{\circ}C$ after placement due to favorable heat insulating and thermal resistance.

MLR & ANN approaches for prediction of compressive strength of alkali activated EAFS

  • Ozturk, Murat;Cansiz, Omer F.;Sevim, Umur K.;Bankir, Muzeyyen Balcikanli
    • Computers and Concrete
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    • v.21 no.5
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    • pp.559-567
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    • 2018
  • In this study alkali activation of Electric Arc Furnace Slag (EAFS) is studied with a comprehensive test program. Three different silicate moduli (1-1,5-2), three different sodium concentrations (4%-6%-8%) for each silicate module, two different curing conditions (45%-98% relative humidity) for each sodium concentration, two different curing temperatures ($400^{\circ}C-800^{\circ}C$) for each relative humidity condition and two different curing time (6h-12h) for each curing temperature variables are selected and their effects on compressive strength was evaluated then regression equations using multiple linear regressions methods are fitted. And then to select the best regression models confirm with using the variables, the regression models compared between itself. An Artificial Neural Network (ANN) models that use silicate moduli, sodium concentration, relative humidity, curing temperature and curing time variables, are formed. After the investigation of these ANN models' results, ANN and multiple linear regressions based models are compared with each other. After that, an explicit formula is developed with values of the ANN model. As a result of this study, the fluctuations of data set of the compressive strength were very well reflected using both of the methods, multiple linear regression with quadratic terms and ANN.

Mechanical Property of Fiber Reinforced Concrete according to the Change of Curing Method (양생방법 변화에 따른 섬유보강콘크리트의 역학적 특성)

  • Kim, Chun-Ho;Kim, Nam-Wook
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.20 no.2
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    • pp.67-73
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    • 2016
  • When assessing crack initiation of fiber reinforced concrete, usually tensile strength or flexural strength is becomes indicator, but also depend on the curing effect take place during the production of specimen. In general, after conducting concrete specimen is cured by water at temperature $20{\pm}3^{\circ}C$ in laboratory, and accomplished the assessment of strength, but most of concrete structure is kept in drying condition after moist curing through the prescribed period. However, unlike these trends that technological advances have been made, influence of the difference of curing method on crack strength is not yet clear. Therefore, in this study, it is examined on the effect of curing methods affecting the mechanical property of fiber reinforced concrete, especially crack strength.

Experimental and analytical study on flexural behaviour of fly ash and paper sludge ash based geopolymer concrete

  • Senthamilselvi, P.;Palanisamy, T.
    • Computers and Concrete
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    • v.21 no.2
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    • pp.157-166
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    • 2018
  • This article presents the flexural behaviour of reinforced fly ash (FA)-based geopolymer concrete (GPC) beams with partial replacement of FA for about 10% by weight with paper sludge ash (PSA). The beams were made of M35 grade concrete and cured under three curing conditions for comparison viz., ambient curing, external exposure curing, and oven curing at $60^{\circ}C$. The beams were experimentally tested at the 28th day of casting after curing by conducting two-point loading flexural test. Performance aspects such as load carrying capacity, first crack load, load-deflection and moment-curvature behaviours of both types of beams were experimentally studied and their results were compared under different curing conditions. To verify the response of reinforced GPC beams numerically, an ANSYS 13.0 finite element program was also used. The result shows that there is a good agreement between computer model failure behaviour with the experimental failure behaviour.

Curing Characteristics of Low Molar Ratio Urea-Formaldehyde Resins

  • Fan, Dongbin;Li, Jianzhang;Mao, An
    • Journal of Adhesion and Interface
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    • v.7 no.4
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    • pp.45-52
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    • 2006
  • Five low molar ratio urea-formaldehyde (LUF) resins were synthesized in this study. The effects of molar ratio, free formaldehyde content, and catalysts on the curing characteristics of LUF resins were studied by measuring its free formaldehyde content, pH value change after catalysts added, curing rate, and pot life, observing its cured appearance, and analyzing its thermal behavior. The results indicate that: 1) The LUF resin with lower molar ratio than 1.0 can still cure; 2) Free formaldehyde content is not the main factor in affecting curing rate of LUF resin; 3) Compared with ammonium chloride as a traditional catalyst, persulfate salts markedly accelerate the curing rate of LUF resin, and result in the different appearance; 4) the addition of sodium chloride to catalysts can accelerate the curing rate of LUF resin, but the effect is moderate.

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A Fundamental Study on the Strength Development in Cement Mortar under Initial Curing Temperature (초기양생온도에 따른 시멘트 모르터의 강도발현에 관한 기초적 연구)

  • 백민수;이영도;임남기;김성식;이종균;최문식;정상진
    • Proceedings of the Korea Concrete Institute Conference
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    • 1997.10a
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    • pp.157-165
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    • 1997
  • In this experiment, there is a purpose to analysis the relationship of feature of compressive strength after fixing of remarkable element under the condition of initial curing temperature. According to this experiment, we get to the fallow result. In case of highest curing temperature, 3-day-strength become high but last revelation of strength become low among the condition of initial curing temperature, the highest curing temperature have an effect on revelation of strength by the application of cumulative temperature, we can get the shape of revelation of strength.

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Characteristics of polymerization in nanofiller-containing composite resins (나노필러를 포함하고 있는 복합레진의 중합특성)

  • Lee, Hee-Kyung
    • Journal of Technologic Dentistry
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    • v.29 no.2
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    • pp.9-15
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    • 2007
  • As the development of nanotechnology, the use of composite resins which containing nanofillers becomes popular. The purpose of this study was to test the degree of polymerization of nanofillercontaining composite resins. For the study, three different nanofiller-containing composite resins and two different light-curing units were used. To evaluate the degree of polymerization, the maximum polymerization shrinkage taking place during the light curing, and the microhardness, after the light curing, were measured. As results, two light-curing units exhibited a similar emission spectrum to that of the included photoinitiator, camphorquinone. The only difference between the light-curing units were the width of the emission spectrum. Three different composite resins showed different microhardness values. Among them, Grandio showed the greatest microhardness value. However, there was less microhardness difference on the top and bottom surfaces due to the difference of the light-curing units. The maximum polymerization shrinkage values were also similar in the tested specimens regardless of the difference of the light-curing units. However, Grandio showed the least polymerization shrinkage. According to the manufacturers' data, Grandio showed the highest filler content(vol%).

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