• Journal of Korean Society for Atmospheric Environment
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• v.34 no.4
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• pp.616-624
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• 2018

In this study, a previous DNPH (2,4-dinitrophenylhydrazine) coupled with high performance liquid chromatography (HPLC) method to measure the concentration of formaldehyde in ambient and source environments has been improved. To improve the disadvantage of the previous HPLC method, an appropriate composition ratio of mobile phase (water: acetonitrile (ACN)) was determined and an isocratic analysis was conducted. Furthermore, limit of detection (LOD), limit of quantitation(LOQ), accuracy, and precision were investigated to verify the reliability of the analytical conditions determined. Finally, samples of exhaust gases from five different industrial facilities were applied to HPLC analytial method proposed to determine their formaldehyde concentrations. The appropriate composition ratio of the mobile phase under the isocratic condition was a mixture of water(40%) and ACN(60%). As the volume fraction of the organic solvent ACN increases, retention time of the formaldehyde peak was reduced. Detection time of formaldehyde peak determined using the proposed isocratic method was reduced from 7 minutes(previous HPLC method) to approximately 3 minutes. LOD, LOQ, accuracy, and precision of the formaldehyde determined using standard solutions were 0.787 ppm, 2.507 ppm, 93.1%, and 0.33%, respectively, all of which are within their recommended ranges. Average concentrations of the formaldehyde in five exhaust gases ranged from 0.054 ppm to 1.159 ppm. The lowest concentration (0.054 ppm) was found at samples from waste gas incinerator in a bisphenol-A manufacturing plant. The highest was observed at samples from the absorption process in manufacturing facilities of chemicals including formaldehyde and hexamine. The analytical time of the formaldehyde in ambient air can be shortened by using the isocratic analytical method under appropriate mobile phase conditions.

• Journal of Korean Medicine Rehabilitation
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• v.30 no.4
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• pp.31-39
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• 2020

Objectives Danggwisoo-san and Jakyakgamcho-tang are frequently prescribed for traffic accident patients in Korea. The aim of this study was to examine index compound analysis, antioxidant activity and amount of starch measurement by extraction method. Methods Danggwisoo-san and Jakyakgamcho-tang were extracted with water and 70% ethanol. Antioxidant activity was measured by 2,2-Diphenyl-1-picrylhydrazyl, 2,2-azino-bis(3-ethylbenzothiazoline-6-sulfonic acid) and ferric reducing antioxidant power according to the standard protocol. The contents of the indicator components nodakenin, paeoniflorin, and glycyrrhizin were measured by high-performance liquid chromatography, respectively. All starches were hydrolyzed and then total D-glucose was measured and compared. Results Antioxidant activity was excellent in 70% ethanol in all assays. The index component was jagged because its solubility was different depending on the extraction solvent. Starch content was significantly lower in 70% alcohol extract than water extract. Conclusions The results of this study showed that physiological activities and components are different according to extraction conditions. Each herbal medicine has a suitable extraction solvent. Also, the difference in starch content is an object to be considered as it may affect digestion and absorption.

• Journal of the Korea Institute of Building Construction
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• v.12 no.5
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• pp.490-502
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• 2012

The use of recycled aggregate, even for low-performance concrete, has been very limited because recycled aggregate, which contains a large amount of old mortar, is very low in quality. To produce a high-quality recycled aggregate, removing the paste that adheres to the recycled aggregate is very important. We have conducted research on a complex abrasion method, which removes the component of cement paste from recycled fine aggregate by using both a low-speed wet abrasion crusher as a mechanical process and neutralization as chemical processes, and well as research on the optimal manufacturing condition of recycled fine aggregates. Subsequently, we evaluated the quality of recycled fine aggregate manufactured using these methods, and tested the specimen made by this aggregate. As a result, it was found that recycled fine aggregates produced by considering the aforementioned optimal abrasion condition with the use of sulfuric acid as reactant showed excellent quality, recording a dry density of 2.4 and an absorption ratio of 2.94. Furthermore, it was discovered that gypsum, which is a reaction product occurring in the process, did not significantly affect the quality of aggregates. Furthermore, the test of mortar using this aggregate, when gypsum was included as a reaction product, showed no obvious retarding effect. However, the test sample containing gypsum recorded a long-term strength of 25.7MPa, whereas the test sample that did not contain gypsum posted a long-term strength of 29.4MPa. Thus, it is thought to be necessary to conduct additional research into the soundness and durability because it showed a clear reduction of strength.

• Korean Journal of Agricultural Science
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• v.39 no.4
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• pp.603-612
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• 2012

In this research, the feasibility of non-destructive measurement technique of pungency measurement was investigated for the red-pepper powders produced in different domestic areas in South Korea. The near-infrared absorption spectra in the range of 1100 nm~2300 nm was used to measure capsaicinoids content in red-pepper powders by using a NIR spectroscopy equipped with Acousto-optic tunable filters (AOTF). Fourth three different red-pepper powders from 14 different locations were collected and separated in three different particle size (below 0.425 mm, 0.425~0.71 mm, 0.71~1.4 mm) for the spectral measurements. The partial least square regression (PLSR) models to predict the capsaicinoids content depends on particle size were developed with the measured spectra. The determinant coefficients and standard errors of the developed models for the red-pepper powders of below 0.425 mm, 0.425~0.71 mm, and 0.71~1.4 mm were in the range of 0.859~0.887 and 12.90~12.99 mg/100 g, respectively. The PLS model with the pretreatment of Standard Normal Variate (SNV) for the red-pepper powders below 1.4 mm particle size showed the best performance with the determinant coefficient of 0.844 and the standard error of 14.63 mg/100 g.

• Journal of the Korean Society of Costume
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• v.57 no.8
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• pp.14-23
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• 2007

The purpose of this study was to investigate the present condition of cold protective clothing for mailman, to improve its design in movement, fitness, and other functions, and supply basic data for its performance evaluation. The results are as follows : The 46.60% of those questioned did not satisfy current clod protective clothing fer mailman. Especially, they considered dissatisfactory in properties such as waterproof, comfort, activity, and sweat absorption. The newly developed cold protective clothing is two-piece style composed of jacket and pants. Both jacket and pants are composed of inner and outer clothing individually. In both jacket and pants, their outer clothing's material was waterproof, windproof, and breathable shell fabric on which PTFE film laminated and their inner clothing's material was 100% polyester Polar polis to have better insulation property. The jacket has attachable cap which can be used as rain gear and set-in sleeve with stand collar. It also had big outside patch pockets and side seam pockets to ensure enough storage space. The pants have knee pads to give free movement to knees and slant side pockets. Inner clothing of both jacket and pants can be worn during working inside without out clothing. Insulation of the newly developed cold protective clothing was not better than current one except right hand, left hand and left foo. It is considered that is because thickness of material is the most important factor to influence insulation.

• Smart Structures and Systems
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• v.17 no.6
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• pp.957-980
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• 2016

Structural damage detection (SDD) is a challenging task in the field of structural health monitoring (SHM). As an exploring attempt to the SDD problem, a hybrid self-adaptive Firefly-Nelder-Mead (SA-FNM) algorithm is proposed for the SDD problem in this study. First of all, the basic principle of firefly algorithm (FA) is introduced. The Nelder-Mead (NM) algorithm is incorporated into FA for improving the local searching ability. A new strategy for exchanging the information in the firefly group is introduced into the SA-FNM for reducing the computation cost. A random walk strategy for the best firefly and a self-adaptive control strategy of three key parameters, such as light absorption, randomization parameter and critical distance, are proposed for preferably balancing the exploitation and exploration ability of the SA-FNM. The computing performance of the SA-FNM is evaluated and compared with the basic FA by three benchmark functions. Secondly, the SDD problem is mathematically converted into a constrained optimization problem, which is then hopefully solved by the SA-FNM algorithm. A multi-step method is proposed for finding the minimum fitness with a big probability. In order to assess the accuracy and the feasibility of the proposed method, a two-storey rigid frame structure without considering the finite element model (FEM) error and a steel beam with considering the model error are taken examples for numerical simulations. Finally, a series of experimental studies on damage detection of a steel beam with four damage patterns are performed in laboratory. The illustrated results show that the proposed method can accurately identify the structural damage. Some valuable conclusions are made and related issues are discussed as well.

• Journal of the Korean Solar Energy Society
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• v.33 no.5
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• pp.9-17
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• 2013

Hourly horizontal global solar radiation has been used as one of significant parameters in a weather file for building energy simulations, which determines the quality of building thermal performance. However, as about twenty two weather stations in Korea have actually measured the horizontal global sola radiation, the weather files collected in other stations requires solar data simulation from the other meteorological parameters. Thus, finding the reliable complicated method that can be used in various weather conditions in Korea is critically important. In this paper, three solar simulation models were selected and evaluated through the reliability test with the simulated hourly horizontal global solar radiation against the actually measured solar data to find the most suitable model for the south east area of Korea. Three selected simulation models were CRM, ZHM, and MRM. The first two models are regression type models using site-fitted coefficients which are derived from the correlation between measured solar data and local meteorological parameters from the previous years, and the last model is a mechanistic type model using the meteorological data to calculate conditions of atmospheric constituents that cause absorption and scattering of the extraterrestrial radiation on the way to the surface on the Earth. The evaluation results show that ZHM is the most reliable model in this area, yet a complicated hybrid simulation methods applying the advantages of each simulation method with the monthly-based weather data is needed.

• The Journal of Korean Institute of Electromagnetic Engineering and Science
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• v.25 no.6
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• pp.679-689
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• 2014

In this paper, an analysis of the effect of time-variant reflected impedance and its detection method on wireless power transfer(WPT) systems are presented. The reflected resistance at WPT systems is very important parameter as it indicates how well matched antenna is and will exhibit high efficiency. Proposed detection method is based on transmitter current variation analysis with respect to frequency sweep. Using the proposed design method, a wireless power transfer system operating at the frequency of 125 kHz, is design and detect reflected impedance variation. The proposed design method provides good agreements between measured and simulated results. Therefore, The proposed detecting method provides a nonintrusive method to detect harmful object in WPT system.

• Journal of Korean Society for Atmospheric Environment
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• v.24 no.1
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• pp.43-54
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• 2008

Management and control of ammonia at the sources and ambient largely depend on sampling and measurement techniques. Good sampling and measurement techniques provide high quality data. The main purpose of the study is compare the analytical characteristics of the Indolphenol method which is one of the standard method in Korea with automatic analyzers for continued measuring gaseous ammonia. For comparison with other analytical methods, the verification test was designed to evaluate performance parameters; linearity, absorption efficiency, reproducibility and repeatability test, accuracy, and response time test. $R^2$ of calibration curve using IPM and CLM was very high (value is 1.000), but for EcSM $R^2$ value was estimated to be lower than IPM and CLM (as 0.991). The RSD of the CLM ranged from 0.1 to 2.3% over the nine concentration levels measured, %Ds was 0.1 to 10.7%, and average RA over all the measurements was 3.3%. The RSD of IPM and EcSM was ranged from 1.0 to 8.1, 3.9 to 14.0 respectively, and average RA were 8.71, 4.9% respectively. Rise in response times of EcSM was estimated to be 1 minute. It is found to be more sensitive than response time (which ranged from 2 to 9 minute) of CLM. For ammonia concentration measured using the IPM and the CLM from the same ammonia source, linear regression of IPM versus CLM show a slope of 0.805, an intercept of 637 ppb, and $R^2$ of 0.868.

• Journal of the Microelectronics and Packaging Society
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• v.16 no.3
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• pp.25-29
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• 2009

High temperature high humidity and thermal shock reliability tests were performed for the board level COB(chip-on-board) flip chip packages using self-formulated and commercial NCPs(non-conductive pastes) to ensure the performance of NCP flip chip packages. It was considered that the more smaller fused silica filler in prototype NCPs is more favorable for high temperature high humidity reliability. The failure of NCP interconnection was affected by the expansion of epoxy due to moisture absorption rather than the fatigue due to thermal stress. It was considered that the NCP having more higher adhesive strength seems to be more favorable to increase the thermal shock reliability.