• Title/Summary/Keyword: ASTM method

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Prediction of Upper Explosion Limits(UEL) by Measurement of Upper Flash Points for n-Alkanes and Aromatic Compounds (노말알칸류와 방향족탄화수소류의 상부인화점 측정에 의한 폭발상한계의 예측)

  • Ha, Dong-Myeong
    • Journal of the Korean Society of Safety
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    • v.26 no.4
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    • pp.59-64
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    • 2011
  • Explosion limit and flash point are the major combustion properties used to determine the fire and explosion hazards of the flammable substances. In this study, in order to predict upper explosion limits(UELs), the upper flash point of n-alkanes and aromatic compounds were measured under the VLE(vapor-liquid equilibrium) state by using Setaflash closed cup tester(ASTM D3278). The UELs calculated by Antoine equation and chemical stoichiometric coefficient tusing the experimental upper flash point were compared with the several reported UELs. From the given results, using the proposed experimental and predicted method, it is possible to research the upper explosion limits of the other flammable substances.

Synthesis and Lubrication Properties of Semi-Fluorinated Polyol Esters (불소계 폴리올에스테르의 합성과 윤활 특성)

  • 백진욱;정근우;김영운
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 2001.06a
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    • pp.149-155
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    • 2001
  • New semi-fluorinated polyol esters were synthesized by condensation reaction of polyols (NPG and TMP) and carboxylic acids such as 2-ethylhexanoic acid, stearic acid and perfluorooctanoic acid. The structures of polyol esters were confirmed by FT-IR and H-NMR etc. And, the fluorinated polyol esters were insoluble in several oils, however, the semi-fluorinated polyol esters were soluble in several oils depended on the structure of polyol esters. The physical properties such as 4-ball wear property and extreme-pressure (EP) properties were characterized by measuring wear scar diameter through ASTM D2266 and by determining the load-carrying through ASTM D2783 method, respectively. As the results, wear scar diameters of oils in which the semi-fluorinated polyol esters were added were not changed compared to those of not added oils. While extreme-pressure properties remarkably Increased with fluorine contents of the esters depended on the structure of acid moiety and polyol moiety. Also, the extreme-pressure property of semi-fluorinated NPG polyol ester in gasoline engine oil was better than that of commercial Teflon coating additive.

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Comparison of Cement Strength According to Standard Units (각국 표준 규격에 따른 시멘트 강도 비교실험)

  • 김남호;정재동;이한봉
    • Proceedings of the Korea Concrete Institute Conference
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    • 1990.04a
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    • pp.20-23
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    • 1990
  • In order to evaluate the difference of testing results in the standards on the compressive strength of various countries, we have compared the testing results of the compressive and flexural strength, one of the most important properties of cement, obtained on the various standards(KS, JIS, BS, ASTM) and the statistical method was used to evaluate the results.

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A study of asbestos containing material characteristics and grade of risk assessment in schools, Korea (일부 학교 건축물의 석면함유 건축자재(ACM) 특성과 위해등급에 관한 연구)

  • Jung, Joon-sig;Park, Hyung-kyu;Song, Hyea-suk;Lee, Won-jeong;Kim, Yoon-shin;Jeon, Hyung-jin
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.16 no.7
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    • pp.5029-5037
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    • 2015
  • The objective of this study is to investigate the distribution of asbestos containing materials and to evaluate risk assessment method in some schools, Korea. For the survey on ACM risk assessment, we used both EPA AHERA rule and ASTM rule. We investigated 100 schools between January and December in 2010. Detection rate of the ACM according to construction year showed that before 1980's, 1990's, 2000's, after 2000's buildings were 100%, 94.1%, 100% and 62.5%, respectively. Compared with school types, detection rate of the ACM in Kindergarten, Elementary, Middle, High, Special Education schools were 100%, 97.1%, 92.9%, 100%, 80%, respectively. Ceiling textiles contained chrysolite/mixed amosite(2~8 %) and wall cement flat boards contained chrysolite(6~11 %). Also, gasket contained chrysolite(16~17 %), slate roof contained chrysolite(10~13 %). In this study, risk assessment EPA AHERA rule of ACM showed that all materials were "Pool" grade. And, ASTM rule risk assessment showed that all materials were "Q&M program" grade.

Electromagnetic Shielding Effectiveness of a Soft Magnetic Film for Application of Noise Reduction In RE Range (RF대역 노이즈 저감용 연자성 필름의 전자기파 차폐효과)

  • Kim Sang-Woo;Yun Yong-Woon;Kim Gwang-Yoon;Lee Yo-Chun;Lee Kyung-Sup
    • Journal of the Microelectronics and Packaging Society
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    • v.11 no.3 s.32
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    • pp.31-36
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    • 2004
  • We charaterized electromagnetic shielding properties of a soft magnetic film using by a ASTM method and 2-port flanged coaxial line method in a RF range and quantitatively analyzed factors for the shielding effectiveness of the soft magnetic film in far field. The shielding effectiveness of the soft magnetic film was dominantly affected by absorption loss not reflection loss in high frequency range of 4-13.5 GHz.

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A Study on the Forging Process Development of the Commutator of an Automotive Starting Motor (자동차용 시동 모터 정류자의 단조공정 개발에 관한 연구)

  • 서명규;배원병;정호승;조종래
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2002.05a
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    • pp.905-909
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    • 2002
  • Commutators of a starting motor for automobiles has been produced through various processes such as forging, segmenting, and assembling. And the conventional method producing an automotive motor commutator is not appropriate for saving material and cost, because it makes each segment separated one by one. Therefore a new process design is required in oder to avoid the assembling process. In this study, a new process design of the commutator of an automotive starting motor has been carried out to save material and manufacturing time by FE analysis. In the FE analysis, three forging processes are proposed for producing the copper(ASTM Cl1000) commutators of a starting motor. And forging experiments are performed to make an unsegmented commutator in order to verify the theoretically proposed process. And then, in order to get the final product, the forged commutator is passed through various postprocessing such as resin terming, and machining. From the experimental result, the forging process proposed from the FE analysis is verified to be an economical method for producing the commutator of an automotive starting motor.

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Prediction of Elastic-Plastic Fracture Toughness for Metallic Material using Finite Element Method (유한요소법에 의한 금속재료의 탄소성파괴인성 예측)

  • Sun Dong-Ju;Park Myung-kyun;Bahk Sae-Man;Choi Young-Taek
    • Journal of the Korean Institute of Gas
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    • v.1 no.1
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    • pp.95-100
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    • 1997
  • In order to predict the elastic-plastic fracture toughness for metallic materials, Finite Element Method(FEM) was used for analysis of compact tension specimen. ASTM E399 test procedure was adopted for simulation of FEM. The Load-Crack Mouth Opening Displacement curve obtained from this analysis was used to detect the crack initiation point and determine the elastic-plastic fracture toughness $J_{IC}$. In order to prove the results, they were compared with the results from previous experiments and they agree with experimental results.

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Evaluation of J$_lc$ and T$_mat$ of aged 1Cr-1Mo-0.25V steel at elevated temperature (시효열화시킨 1Cr-1Mo-0.25V 강의 고온에서의 J$_lc$ 및 T$_mat$ 의 평가)

  • 윤기봉;윤석호;서창민;남승훈
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.18 no.11
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    • pp.2860-2870
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    • 1994
  • When crack are detected in aged turbine rotors of power plants, information on fracture resistance of the aged material at operating temperature is needed for determination of critical loading condition and residual life of the turbine. In this study, fracture toughness (J$_lc$) and tearing modulus(T$_mat$) of virgin and thermally degraded 1Cr-1Mo-0.25V steel, which is one of the most widely used rotor steels, were measured at 538.deg. C according to ASTM E813 and ASTM E1152, respectively. Five kinds of specimen with different degradation levels were prepared by isothermal aging heat treatment at $630^{\circ}C.$ It was observed that J$_lc$ and T$_mat$ value decreased as the degradation level increased. Analysis of microstructures using a scanning electron microscope showed that the decrement of J$_lc$ is related to segregation of impurities at grain boundaries. It was also verified that the DC electric potential drop method is accurate and reliable for crack length monitoring at elevated temperature.

Two-dimensional Coupled Moisture and Heat Flow Model and Sensitivity Analysis (이차원 복합적 습기와 열흐름의 분석모델과 민감도 분석)

  • Kim, Suk-Nam
    • Journal of the Korean Geotechnical Society
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    • v.19 no.5
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    • pp.99-107
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    • 2003
  • Moisture flow and heat flow within pavement systems have been recognized as coupled processes with complex interactions between them. The distribution of moisture and temperature within pavement due to the moisture flow and heat flow varies not only seasonally but also vertically and horizontally. This paper presents an analysis model by the finite element method for the two-dimensional coupled moisture and heat flow in unsaturated soils. To test the model the analysis result by the model is compared with the analysis result by the software, GEO-SLOPE developed by GEO-SLOPE International Ltd. in Alberta, Canada. And a sensitivity analysis using ASTM method is performed to identify how model inputs affect the modeling analysis.

A Study on Fracture Toughness Properties of $Al_{18}B_4O_{33}/AC4CH$ by Binder Additives (바인더 첨가에 따른 $Al_{18}B_4O_{33}/AC4CH$의 파괴인성에 관한 연구)

  • Shin, Dong-In;Jung, Jae-Wook;Park, Won-Jo;Huh, Sun-Chul;Kim, Hyung-Jin
    • Proceedings of the KSME Conference
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    • 2003.04a
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    • pp.61-66
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    • 2003
  • In this paper, the effect of binder additive on the fracture toughness was metal matrix composite produced by squeeze casting method. In this study using the matrix is AC4CH and reinforcement used Aluminum borate whisker. Each MMC was produced by add inanimate binder ($SiO_2,\;Al2O_3,\;TiO_2$) to whiskers for increase the binding together of whiskers. Fracture toughness test were carry out in accordance with the ASTM E-399 standard test method, W=25mm, b=12.5mm CT(half size) specimen. However Base metal AC4CH was not meet the qualification of $P_m/P_Q<1.1$, so that test were performed $J_{IC}$ test. $K_{J_{IC}}$ value was measuring by $J_{IC}$ value change into $K_{IC}$. $J_{IC}$ test was carry out in accordance with the ASTM 1820.

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