• Tribology and Lubricants
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• 제30권5호
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• pp.295-302
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• 2014

The tribological behavior of an Fe-based bulk amorphous alloy while sliding against a AISI 304 disc is investigated using a unidirectional pin-on-disc type tribometer in dry and distilled water environments. The rod-shaped bulk pins are fabricated by suction casting. The crystallinities of the bulk amorphous alloys before and after the friction tests are determined by X-ray diffraction. The friction coefficient and specific wear rate of the amorphous pin in the water environment are found to be twice and thrice as much as in the dry environment at a low applied pressure, respectively. However, at a higher pressure, the friction coefficient and specific wear rate are 0.4 and 1.02 mg/(Nm/s), respectively, in the water environment. A microstructure analysis shows that the worn surface of the alloy is characterized by delamination from the smooth friction surface, and thus delamination is the main wear mechanism during the friction test in dry sliding environment. In contrast, brittle fracture morphologies are apparent on the friction surface formed in distilled water environment. For the sample tested at a lower sliding speed, the XPS data from the oxide layer are similar to those of the pure element with weak suboxide peaks. For higher sliding speeds, all the main sharp peaks representing the core level binding energies are shifted to the oxide region.

• 한국세라믹학회지
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• 제43권6호
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• pp.358-361
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• 2006

A two-step plasma-assisted boronizing process was carried out on the AISI 1045 steel substrate to reduce the pore density introduced by a conventional single plasma boronizing process. The specimens were plasma boronized for 1 h at $650^{\circ}C$ and subsequently far 7 h at $800^{\circ}C$ in an atmosphere of $BCl_3-H_2-Ar$. The boride layer thickness was parabolic in boronizing time, a high HV reading of 1540 was found up to the boride layer thickness of $25{\mu}m$. It was found that the morphology of the boride layer prepared by the two-step boronizing process was changed from a columnar to a tooth-like structure and the pores in the borided steel were eliminated completely in comparison to those synthesized by the conventional single boronizing process, implying that it is highly applicable for enhancing the dense and compact coating properties of the low-alloy steel.

• Structural Engineering and Mechanics
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• 제64권5호
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• pp.621-640
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• 2017

This paper reports the numerical investigation conducted to study the influence of Local-Distortional (L-D) interaction mode buckling on post buckling strength erosion in fixed ended lipped channel cold formed steel columns. This investigation comprises of 81 column sections with various geometries and yield stresses that are carefully chosen to cover wide range of strength related parametric ratios like (i) distortional to local critical buckling stress ratio ($0.91{\leq}F_{CRD}/F_{CRL}{\leq}4.05$) (ii) non dimensional local slenderness ratio ($0.88{\leq}{\lambda}_L{\leq}3.54$) (iii) non-dimensional distortional slenderness ratio ($0.68{\leq}{\lambda}_D{\leq}3.23$) and (iv) yield to non-critical buckling stress ratio (0.45 to 10.4). The numerical investigation is carried out by conducting linear and non-linear shell finite element analysis (SFEA) using ABAQUS software. The non-linear SFEA includes both geometry and material non-linearity. The numerical results obtained are deeply analysed to understand the post buckling mechanics, failure modes and ultimate strength that are influenced by L-D interaction with respect to strength related parametric ratios. The ultimate strength data obtained from numerical analysis are compared with (i) the experimental tests data concerning L-D interaction mode buckling reported by other researchers (ii) column strength predicted by Direct Strength Method (DSM) column strength curves for local and distortional buckling specified in AISI S-100 (iii) strength predicted by available DSM based approaches that includes L-D interaction mode failure. The role of flange width to web depth ratio on post buckling strength erosion is reported. Then the paper concludes with merits and limitations of codified DSM and available DSM based approaches on accurate failure strength prediction.

• 한국윤활학회:학술대회논문집
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• 한국윤활학회 2001년도 제34회 추계학술대회 개최
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• pp.109-116
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• 2001

In this study, the effects of oxide layer formed on the contact parts of TiN coated ball and steel disk in sliding are investigated. Also wear mechanism to form the oxide layer and the characteristics of the oxide layer formation are investigated. AIS152100 steel ball is used for the substrate of coated ball specimens. Two types of coated ball specimens were prepared by depositing TiN coating with 1 and 4um in coating thickness. AISI1045 steel is used for the disk type counter-body. To investigate the effect of oxide layer on the contact parts of the two materials, the tests were performed both in ambient for forming oxide layer on the contact parts and in nitride environment to avoid oxidation. And to study the effects of surface roughness of counter-body, TiN coating thickness and contact load of sliding test on the characteristics of oxide layer formation on counter-body, various tests were carried out. From the results, the friction characteristics between the two materials was predominated by iron oxide layer that formed on wear track on counter-body and this layer caused the high friction. And the formation rate of the oxide layer on wear track increased as the real contact area between the two materials increased as the contact load increased, the TiN coating thickness decreased and the surface of counter-body smoothened.

• 한국재료학회지
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• 제7권1호
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• pp.76-80
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• 1997

용융탄산염 연료전지 분리판의 wet-seal부의 내식성 향상을 위한 NiAl 피복공정이 조사되었다. AlSl 316 스테인레스강위에 Ni과 Al를 순차적으로 피복한 후, $800^{\circ}C$에서 3시간 열처리하여 NiAl상이 형성됨을 확인할 수 있었다. NiAl상이 피복된 스테인레스강은 $650^{\circ}C$, 용융탄산염($62^{m}/_{o}Li_2CO_3-38^{m}/_{o}/K_{2}CO_{3}$)내에서 침지시험을 통해 내식성이 평가되었는데, AISI 316 스테인레스강에 비해 우수한 내식성을 보였다. 이는 표면에 치밀하게 형성된 AI 산화물층에 의한 것으로 판단되었다.

• 한국표면공학회지
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• 제43권5호
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• pp.238-242
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• 2010

In the present work, the influence of oxide on the Cr-Si-N coatings was investigated for the Cr-Si-O-N coatings on AISI 304 and Si wafer deposited by hybrid system, which combines the DC magnetron sputtering technique and arc ion plating (AIP) using Cr and Si target in an $Ar/N_2/O_2$ gaseous mixture. As the O content in the Cr-Si-N coatings increased, the diffraction patterns of the Cr-Si-O-N coatings showed CrN and $Cr_2O_3$ phases. However, as the O content increased to 28.8 at.%, diffraction peak of $Cr_2O_3$ was disappeared in the Cr-Si-O-N coating. The $d_{200}$ value was decreased with increasing of O content. The average grain size increased from about 40 nm to 65 nm as the O content increased. The maximum micro-hardness of the Cr-Si-O-N coating was obtained 4507 Hk at the O content of 24.8 at.%. The average friction coefficient of the Cr-Si-O-N coatings was gradually decreased by increasing the O content and the average friction coefficient decreased from 0.37 to 0.25 by increasing the O content. These results indicated that amorphous phase was increased in the Cr-Si-O-N coatings by increasing of O content.

• 열처리공학회지
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• 제11권4호
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• pp.305-314
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• 1998

This study has been performed to investigate into some effects of various amounts of $CO_2$ and CO gas added to the $50%NH_3-N_2$ based gas atmosphere on microstructure, hardness, chemical analysis and residual stress in the compound and diffusion layer of AISI H13 treated by gaseous nitrocarburising process. The compound layer formed in the surface is composed of mainly ${\varepsilon}-Fe_3$(N,C) and small amount of ${\gamma}^{\prime}-Fe_4N$ and cementite. The maximum hardness value obtainable from H13 steel is shown to be 1200 Hv and the effecvtive hardening depth increases with increasing CO content from 1% to 4%. In the case of CO content over 4%, however, it decreases with increasing CO content. The composition profiles of nitrogen and carbon are found to be within the ${\varepsilon}$-phase field located above the ${\varepsilon}+{\gamma}^{\prime}$ phase field in the Fe-N-C diagram. It is shown that the maximum value of compressive residual stress of H13 steel treated in atmospheres of $50%NH_3-(2,4)%CO_2-N_2-CO$ gas mixture is $48kg/mm^2$ and the depth to which residual stress is in Compressive state is $90{\mu}m$ for the atmosphere $50%NH_3-45%N_2-4%CO_2-1%CO$ gas mixture. It is consequently important to control the maximum value and size of compressive residual stress region in order to obtain desirable mechanical properties.

• 한국구조물진단유지관리공학회 논문집
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• 제7권1호
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• pp.147-156
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• 2003

In this research, multiple corrosion factors of buried environments were measured in order to establish a formula for the corrosion character of corrugated steel structures in domestic environments. By substituting corrosion factors for each predicting formula, the durable lifetime was measured, and the measured lifetime was compared with the estimated lifetime by applying existing thickness-measuring techniques. A new usage standard was proposed with these results, in order to create the conclusion below. There are known differences in the soil factors used as variables in estimating the duration caused by the seasonal effects of rainfall and temperature. Comparing the durable lifetime estimated by each predicting formula, the findings show that the California technique is conservative. This study demonstrates that the error range of the AISI technique, which is mostly used as a duration technique, is a very narrow predicting technique as compared with many other countries. Considering that there is on average, a 13% error margin in this study, a proposed safety factor of 0.87 could be used to more accurately predict the duration. The laying time in the California technique is not longer than the whole durability, and as a result, this error margin exists. It is concluded that this study on the open area has been overdue. Based on these findings, it's proposed that this error margin should be applied to the domestic environment through periodic observation, in order to establish the predicting techniques of durable lifetime.

• Steel and Composite Structures
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• 제1권1호
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• pp.17-32
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• 2001

The Rosette-joining system is a completely new press-joining method for cold-formed steel structures. One Rosette-joint has a shear capacity equal to that of approximately four screws or rivets. The Rosette thin-walled steel truss system presents a new fully integrated prefabricated alternative to light-weight roof truss structures. The trusses are built up on special industrial production lines from modified top hat sections used as top and bottom chords and channel sections used as webs which are joined together with the Rosette press-joining technique to form a completed structure easy to transport and install. A single web section is used when sufficient but can be strengthened by double-nesting two separate sections or by using two lateral profiles where greater compressive axial forces are met. An individual joint in the truss can be strengthened by introducing a hollow bolt into the joint hole. The bolt gives the connection capacity a boost of approximately 20%. A series of laboratory tests have been carried out in order to verify the Rosette truss system in practice. In addition to compression tests on individual sections of different lengths, tests have also been done on small structural assemblies and on actual full-scale trusses of a span of 10 metres. Design calculations have been performed on selected roof truss geometries based on the test results, FE-analysis and on the Eurocode 3 and U.S.(AISI) design codes.

• Corrosion Science and Technology
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• 제2권3호
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• pp.117-126
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• 2003

Due to excellent corrosion resistance and mechanical properties, austenitic stainless steel is widely used as the material for chemical plants. nuclear power plants, and food processing facilities. But, the zone affected by heat in the range of 400 to $800^{\circ}C$ during welding loses corrosion resistance and tensile strength since Cr-carbide precipitation like $Cr_{23}C_6$ forms at the grain boundary and thereby takes place the intergranular corrosion. In this study, AISI 304 stainless steel with the added Nb of 0.3 to 0.7 wt% was solutionized at $1050^{\circ}C$ and sensitized at $650^{\circ}C$. Specimen was welded by MIG. The phase and the microstructure of the specimens were examined by an optical microscope, a scanning electron microscope, and a x-ray diffractometer. The corrosion characteristics of specimens were tested by electrolytic etching and by double loop electrochemical potentiokinetic reactivation method(EPR) in the mixed solution of 0.5M $H_2SO_4$ + 0.01M KSCN. The melting zone had dendritic structure constituted of austenitic phase and $\delta$-ferrite phase. Cr carbide at the matrix did not appear, as Nb content increased. At the grain boundaries of the heat affected zone, the precipitates decreased and the twins appeared. The hardness increased, as Nb content increased. The hardness was highest in the order of the heat affected zone>melted zone>matrix. According to EPR curve, as the Nb content decreased, the reactivation current density(Ir) and the activation current density(la) were highest in the order of the melted zone