• 대한기계학회논문집
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• 제7권2호
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• pp.226-232
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• 1983

회전수를 용접변수로 했을 때 이종강봉 및 이종강관의 마찰용접에 있어서 소성변형중에 발생한 AE(acoustic emission)량과 용접후의 냉각중에 발생한 AE량의 총량을 측정해석하고, 용접표면상 에 0.635mmR의 반원 노치를 가공했을 때의 용접부 인장강도를 구하여, AE총량과 용접부강도와 의 상관관계실험식 모델을 만들었고, 이들과 관계계산식과의 비교 조사와 95%신뢰성을 검증하였 고, 이종강의 마찰용접 중에 용접강도와 품질을 검토관리할 수 있는 기본자료가 되게 하였다.

• 비파괴검사학회지
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• 제15권4호
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• pp.511-519
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• 1996

Cr-Mo강인 SNCM220, SCM435, SACM645 및 SCM415 강봉을 사용하여 ${\phi}31.2$ 봉 대 봉 동종재 마찰용접의 최적 조건을 실험적으로 구하였으며, 이를 위하여 이음부의 인장강도와 마찰용접 변수와의 정량적 상관식을 실험적으로 도출하였다. 한편 마찰용접시 음향방출시험을 병행하여, AE 누적총량과 마찰용접변수, 마찰용접부의 인장강도와 AE 누적총량과의 정량적 상관성을 도출하였다. 그리고, 마찰용접부의 인장파단면을 검토함으로써 용접품질을 확인하였다.

• 한국해양공학회:학술대회논문집
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• 한국해양공학회 2001년도 춘계학술대회 논문집
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• pp.301-306
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• 2001

In this paper, friction welding optimization for 1Cr0.5Mo to STS304 and AE applications for the weld quality evaluation were investigated The important results of this study are as follows : 1. The techiques for dissimilar friction welding optimization if the elevated temperature materials 1Cr0.5Mo and STS304 and its real-time weld quality evaluation by AE were developed, considering on both strength and toughness. 2. Quantitative relationship was identified among welding condition, weld quality and cumulative AE counts.

• Journal of Welding and Joining
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• 제13권4호
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• pp.103-112
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• 1995

This study was performed to optimize friction welding conditions of Cr-Mo steel bars used for hydraulic of pneumatic valve spools and to realize the real-time evaluation of weld quality by acoustic emission method. SNCM220, SCM435, SCAM645, and SCM415 steel bars were tested to find optimum conditions of friction welding. Auantitative equations which exhibit the relations of tensile strength, elongation, reduction of area and energy absorption with friction heating time were obtained by the experiment. Acoustic emission was also performed in the friction weldig process, and the real-time evaluation was enabled to find the optimum range of weld strength. Finally, the strength and toughness of welded joints were interpreted by the sem analysis of tensile fracture surfaces.

• 동력기계공학회지
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• 제6권2호
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• pp.48-53
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• 2002

Plunger (piston rod) materials are used in high-pressure condition. So STD11 is the essential material to build this plunger. However, it costs more to make a plunger by using only STD11 than using the welding of STD11 to SCM440 and other dissimilar material. And it has been difficult to weld this sort of dissimilar materials. They could be unstable in the quality by the conventional arc welding. And also they have a lot of technical problems in manufacturing. But, by the friction welding technique, it will be able to be made without such problems. And then, on account of such reasons, we need a new approach of study on real-time quality evaluation by acoustic emission (AE) techniques as well as a domestic development of the plunger by friction welding. So that, the purpose of this study for such developments is the development of a plunger by optimizing of friction welding with more reliability and more applicability. Then, this study aimed not only to develop the optimization of friction welding of dissimilar plunger steels of STD11 to SCM440, but also to develop the application technique of the acoustic emission to accomplish an in-process real-time quality evaluation during friction welding of the plunger materials by the AE technique.

• 동력기계공학회지
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• 제6권1호
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• pp.55-60
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• 2002

There has been no report on the life prediction for gas turbine materials at high temperatures based on the creep properties and their relationship with the AE(acoustic emission) properties as a means of real-time non-destructive testing. One of the important issues is thus to develop a reliable method of evaluating creep properties by the AE technique. In this paper, the real-time evaluation of high temperature creep time and AE cumulative counts for nickel-based superalloy Udimet 720 was performed on round-bar type specimens under pure load at the temperatures of 811, 922 and 977K. The total AE cumulative counts until the starting point of secondary creep($N_1$) and that of tertiary creep($N_2$) have quantitative relationship with the tertiary creep time and the rupture time. It is thus possible to construct the life prediction system based on creep and the prevention system of tertiary creep by using AE technique.

• 동력기계공학회지
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• 제6권1호
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• pp.68-73
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• 2002

An opportunity to use the elevated temperature has been recently increasing in various elements of heat facilities or machines such as heat exchanger tubes, pressure vessels, engines of aircraft, boilers and turbines in power plants, and nuclear reactor components, etc. as machinery industry develops. Thus, the development of such elevated-temperature heat-resisting materials and the studies on their elevated-temperature materials friction welding, creep design and analysis have been considered as an important and needful fact. In this paper, friction welding optimization for 1Cr0.5Mo to STS304 and AE applications for the weld quality evaluation were investigated. The important results of this study are as follows : The techniques for dissimilar friction welding optimization of the elevated temperature materials 1Cr0.5Mo and STS304 and its real-time weld quality evaluation by AE were developed, considering on both strength and toughness. Quantitative relationship was identified among welding condition, weld quality and cumulative AE counts.

• Journal of Advanced Marine Engineering and Technology
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• 제17권4호
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• pp.38-48
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• 1993

A study on friction welding of stainless steel bar(SUS431) to chrome molybdenum steel bar(SCM21) was accomplished experimentally through analysis for relations among friction welding conditions, tension test, hardness test, microstructure test and acoustic emission test. The results obtained are summarized as follows ; 1. Through friction welding of SUS431 bar to SCM21 bar, the optimum welding condition by considering on strength and toughness was found to be the range of heating time of 3-5 sec when the number of rotating speed of 2000rpm, heating pressure of 10kg/$mm^2$, and upsetting time of 4 sec. 2. Quantitative ralationship was identified between heating time($T_1$, sec) and tensile strength (${\sigma},\;kgf/mm^2$) of the friction welded joint and the relation equation is $\sigma$=52.62$T_1{^{0.06}}$. 3. Through AE test, quantitative relationship was confirmed between heating time($T_1$, sec) and total AE(N, counts) during welding, and the relation is computed as follows ; N=30413.6$e^{0.06T1}$. 4. It was confirmed that the quantitative ralationship exists between the tensile strength of the welded joints and AE cumulative counts. And the relation is computed as the following ; ${\sigma}$=16.37(ln N)- 116.4. 5. When ONZ=36500-41500 counts by $OT_1Z$=3~5sec, it was identified by experiment that the range of welded joint tensile strength is 55.6-57.7kgf/$mm^2$/ whose joint efficiency is more than 100%, and it was experimentally confirmed that the real-time nondestructive quality(strength) evaluation for the friction welded joints could be possible by acoustic emission technique.

• 한국작물학회지
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• 제49권6호
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• pp.528-532
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• 2004

발아 녹두에 세 가지 스트레스 관련 화합물 salicylic acid, methyl jasmonic acid, acetyl salicylic acid를 처리하여 isoflavone의 생합성양상을 관찰한 결과를 요약하면 다음과 같다. 1. 숙주나물의 자엽에서는 isoflavone총량이 건조중 1g당 $832.5{\mu}g$인 무처리구와 비교하여 10mM salicylic acid를 처리한 경우 $169\%$, 12mM acetyl salicylic acid로 처리한 경우 $165\%$의 isoflavone 총량이 증가한 반면 $0.5\%$ methyl jasmonic acid를 처리한 경우는 오히려 무처리구보다 $47\%$ 수준으로 감소하였다. 2. 숙주나물의 자엽하부(hypocotyl and root)의 isoflavone 생성량에서는 1g당 284.8${\mu}g$이 생성된 무처리구와 비교하여 세 가지 처리 모두에서 유의성이 있는 차이를 보였다. 10mM salicylic acid 처리구의 경우 $419\%$, 12mM acetyl salicylic acid 처리구의 경우 $401\%$의 isoflavone 총량의 증가를 보였고, $0.5\%$ methyl jasmonic acid처리구의 경우에는 $121\%$증가하였다. 3.숙주나물의 자엽부위와 자엽하부에서 검출된 isoflavone의 합을 각 처리별 isoflavone생산총량으로 하여 무처리구의 건조중 1g당 1117.3${\mu}g$을 기준으로 비교하여보면 건조중 1g당 10mM salicylic acid 처리구에서는 2601.02${\mu}g$으로 $233\%$ 증가하였고, 12mM acetyl salicylic acid 2514.4${\mu}g$으로 $225\%$ 증가한 반면, $0.5\%$ methyl jasmonic acid 처리구에서는 738.8${\mu}g$으로 $66\%$ 수준으로 감소하였다. 4. 숙주나물 자엽부위의 경우 무처리구와 비교하여 증가를 보였던 10mM salicylic acid처리구와 12mM acetyl salicylic acid 처리구에서는 malonyldaidzine과 malonylglycitin이 증가가 두드러지게 나타났다. 5. 숙주나물 자엽하부의 경우 무처리구와 비교하여 증가를 보였던 10mM salicylic acid 처리구와 12mM acetyl salicylic acid 처리구에서는 malonylglycitin의 증가가 두드러지게 나타났다

• 분석과학
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• 제27권2호
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• pp.92-99
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• 2014

본 연구에서는 음이온 고체상 추출법 (AE SPE; anion exchange solid phase extraction)을 사용하여 간섭요인을 제거한 후, 친화 크로마토그래피 AF HPLC; affinity high performance liquid chromatography)와 유도결합 플라스마 질량분석법 (ICP/MS; inductively coupled plasma/mass spectrometry)을 사용하여 한국인의 혈청에서의 셀레노 단백질을 분리하고 정량하였다. 먼저 동위원소 희석법으로 셀레늄 총량을 분석한 결과, 건강한 한국 사람의 혈청내 평균농도는 $94.3{\pm}2.3ngg^{-1}$ 이었다. AE SPE와 AF 컬럼을 online으로 연결하여 셀레노단백질인 glutathione peroxidase (GPx), selenoprotein P (SelP), selenoalbumin (SeAlb)을 분리하고, 후 컬럼 동위원소 희석법 (PC ID; post column isotope dilution)으로 정량하였다. 혈청 인증표준물인 BCR-637을 분석한 결과 전체 셀레노 단백질의 합은 $85.4{\pm}3.4ngg^{-1}$으로 문헌값인 $81{\pm}7ngg^{-1}$과 일치하는 결과를 얻을 수 있었다. 20 명의 건강한 한국인의 혈청에서 얻은 셀레노 단백질 GPx, SelP 및 SeAlb 의 농도는 각각 $12.1{\pm}1.4ngg^{-1}$, $57.2{\pm}2.0ngg^{-1}$, 그리고 $20.0{\pm}1.9ngg^{-1}$ 이었으며 이들의 합인 $89.3ngg^{-1}$은 셀레늄의 총량값인 $94.3ngg^{-1}$과 거의 같은 값으로 혈청에서의 셀레늄은 주로 셀레노 단백질로 구성되어 있음을 알았다. 이 중 GPx의 농도는 간섭을 제거하기 전인 $25.0ngg^{-1}$에 비해 50% 이상 크게 감소하였는데 이로서 간섭은 주로 GPx에 포함되어 있음을 확인할 수 있었다. AE SPE는 간섭요인인 Cl과 Br을 제거 하는데 매우 효과적임을 보여주었다.