• Transactions of the Korean Society of Mechanical Engineers
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• v.7 no.2
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• pp.226-232
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• 1983

회전수를 용접변수로 했을 때 이종강봉 및 이종강관의 마찰용접에 있어서 소성변형중에 발생한 AE(acoustic emission)량과 용접후의 냉각중에 발생한 AE량의 총량을 측정해석하고, 용접표면상 에 0.635mmR의 반원 노치를 가공했을 때의 용접부 인장강도를 구하여, AE총량과 용접부강도와 의 상관관계실험식 모델을 만들었고, 이들과 관계계산식과의 비교 조사와 95%신뢰성을 검증하였 고, 이종강의 마찰용접 중에 용접강도와 품질을 검토관리할 수 있는 기본자료가 되게 하였다.

• Journal of the Korean Society for Nondestructive Testing
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• v.15 no.4
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• pp.511-519
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• 1996

The purposes of this study are 1) to develop optimum FRW technique of SNCM220, SCM435, SACM645 and SCM415 bar-to-bar similar friction welding, 2) to develop in-process real-time weld quality nondestructive evaluation technique by acoustic emission method, and 3) to certify of weld quality by inspection of tensile fracture surface on friction welded joints.

• Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
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• 2001.05a
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• pp.301-306
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• 2001

In this paper, friction welding optimization for 1Cr0.5Mo to STS304 and AE applications for the weld quality evaluation were investigated The important results of this study are as follows : 1. The techiques for dissimilar friction welding optimization if the elevated temperature materials 1Cr0.5Mo and STS304 and its real-time weld quality evaluation by AE were developed, considering on both strength and toughness. 2. Quantitative relationship was identified among welding condition, weld quality and cumulative AE counts.

• Journal of Welding and Joining
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• v.13 no.4
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• pp.103-112
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• 1995

This study was performed to optimize friction welding conditions of Cr-Mo steel bars used for hydraulic of pneumatic valve spools and to realize the real-time evaluation of weld quality by acoustic emission method. SNCM220, SCM435, SCAM645, and SCM415 steel bars were tested to find optimum conditions of friction welding. Auantitative equations which exhibit the relations of tensile strength, elongation, reduction of area and energy absorption with friction heating time were obtained by the experiment. Acoustic emission was also performed in the friction weldig process, and the real-time evaluation was enabled to find the optimum range of weld strength. Finally, the strength and toughness of welded joints were interpreted by the sem analysis of tensile fracture surfaces.

• Journal of Power System Engineering
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• v.6 no.2
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• pp.48-53
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• 2002

Plunger (piston rod) materials are used in high-pressure condition. So STD11 is the essential material to build this plunger. However, it costs more to make a plunger by using only STD11 than using the welding of STD11 to SCM440 and other dissimilar material. And it has been difficult to weld this sort of dissimilar materials. They could be unstable in the quality by the conventional arc welding. And also they have a lot of technical problems in manufacturing. But, by the friction welding technique, it will be able to be made without such problems. And then, on account of such reasons, we need a new approach of study on real-time quality evaluation by acoustic emission (AE) techniques as well as a domestic development of the plunger by friction welding. So that, the purpose of this study for such developments is the development of a plunger by optimizing of friction welding with more reliability and more applicability. Then, this study aimed not only to develop the optimization of friction welding of dissimilar plunger steels of STD11 to SCM440, but also to develop the application technique of the acoustic emission to accomplish an in-process real-time quality evaluation during friction welding of the plunger materials by the AE technique.

• Journal of Power System Engineering
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• v.6 no.1
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• pp.55-60
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• 2002

There has been no report on the life prediction for gas turbine materials at high temperatures based on the creep properties and their relationship with the AE(acoustic emission) properties as a means of real-time non-destructive testing. One of the important issues is thus to develop a reliable method of evaluating creep properties by the AE technique. In this paper, the real-time evaluation of high temperature creep time and AE cumulative counts for nickel-based superalloy Udimet 720 was performed on round-bar type specimens under pure load at the temperatures of 811, 922 and 977K. The total AE cumulative counts until the starting point of secondary creep($N_1$) and that of tertiary creep($N_2$) have quantitative relationship with the tertiary creep time and the rupture time. It is thus possible to construct the life prediction system based on creep and the prevention system of tertiary creep by using AE technique.

• Journal of Power System Engineering
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• v.6 no.1
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• pp.68-73
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• 2002

An opportunity to use the elevated temperature has been recently increasing in various elements of heat facilities or machines such as heat exchanger tubes, pressure vessels, engines of aircraft, boilers and turbines in power plants, and nuclear reactor components, etc. as machinery industry develops. Thus, the development of such elevated-temperature heat-resisting materials and the studies on their elevated-temperature materials friction welding, creep design and analysis have been considered as an important and needful fact. In this paper, friction welding optimization for 1Cr0.5Mo to STS304 and AE applications for the weld quality evaluation were investigated. The important results of this study are as follows : The techniques for dissimilar friction welding optimization of the elevated temperature materials 1Cr0.5Mo and STS304 and its real-time weld quality evaluation by AE were developed, considering on both strength and toughness. Quantitative relationship was identified among welding condition, weld quality and cumulative AE counts.

• Journal of Advanced Marine Engineering and Technology
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• v.17 no.4
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• pp.38-48
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• 1993

A study on friction welding of stainless steel bar(SUS431) to chrome molybdenum steel bar(SCM21) was accomplished experimentally through analysis for relations among friction welding conditions, tension test, hardness test, microstructure test and acoustic emission test. The results obtained are summarized as follows ; 1. Through friction welding of SUS431 bar to SCM21 bar, the optimum welding condition by considering on strength and toughness was found to be the range of heating time of 3-5 sec when the number of rotating speed of 2000rpm, heating pressure of 10kg/$mm^2$, and upsetting time of 4 sec. 2. Quantitative ralationship was identified between heating time($T_1$, sec) and tensile strength (${\sigma},\;kgf/mm^2$) of the friction welded joint and the relation equation is $\sigma$=52.62$T_1{^{0.06}}$. 3. Through AE test, quantitative relationship was confirmed between heating time($T_1$, sec) and total AE(N, counts) during welding, and the relation is computed as follows ; N=30413.6$e^{0.06T1}$. 4. It was confirmed that the quantitative ralationship exists between the tensile strength of the welded joints and AE cumulative counts. And the relation is computed as the following ; ${\sigma}$=16.37(ln N)- 116.4. 5. When ONZ=36500-41500 counts by $OT_1Z$=3~5sec, it was identified by experiment that the range of welded joint tensile strength is 55.6-57.7kgf/$mm^2$/ whose joint efficiency is more than 100%, and it was experimentally confirmed that the real-time nondestructive quality(strength) evaluation for the friction welded joints could be possible by acoustic emission technique.

• KOREAN JOURNAL OF CROP SCIENCE
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• v.49 no.6
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• pp.528-532
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• 2004

We have studied physiological responses of mung bean sprout to the treatment of elicitors. Chemicals such as salicylic acid and methyl jasmonic acid are not only the intermediates found in plant defense system but also could affect plant secondary metabolism. We found that mild treatment of salicylic acid and acetyl salicylic acid (aspirin) increase isoflavone production dramatically in mung bean sprout which has very low level of isoflavones compared with soybean sprout. The isoflavone content in salicylic acid treated- and acetyl salicylic acid treated-mung bean sprout was about 2.3 and 2.2 times higher than that of control, respectively. However, the increasing patterns of isoflavone in cotyledon and hypocotyl and root were not identical. The major increase among isoflavone fractions in cotyledon was led by the increase in malonylglycitin and malonyldaidzin level. Whereas, the increase in hypocotyl and root was led by malonyldaidzin. Methyl jasmonic acid did not show statistically significant increase in mung bean sprout. With this result, we were able to propose the non-transgenic method, which can control the isoflavone production in germinating mung bean.

• Analytical Science and Technology
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• v.27 no.2
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• pp.92-99
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• 2014

Interferences were removed using anion exchange solid phase extraction (AE SPE) in quantification of selenoproteins in Korean human blood serum with affinity high performance liquid chromatography (AF HPLC)-inductively coupled plasma/mass spectrometry (ICP/MS). The average selenium level obtained for healthy Koreans was $94.3{\pm}2.3ngg^{-1}$ using isotope dilution method. AE SPE was coupled to AF column to separate 3 selenoproteins, glutathione peroxidase GPx, selenoprotein SelP, and selenoalbumin SeAlb. Post column isotope dilution was employed to quantify the proteins. The certified reference material of human blood serum BCR-637 was analyzed to give total selenoprotein concentration of $85.4{\pm}3.4ngg^{-1}$, which agreed well with the reference value of $81{\pm}7ngg^{-1}$. The pooled concentration of GPx, SelP, and SeAlb from healthy Koreans (n=20) was $12.1{\pm}1.4ngg^{-1}$, $57.2{\pm}2.0ngg^{-1}$, and $20.0{\pm}1.9ngg^{-1}$, respectively. The sum of selenoproteins is $89.3ngg^{-1}$, which is about the same as the total selenium concentration of $94.3ngg^{-1}$. The fact suggests that selenium in blood serum is mostly consisted of selenoproteins. After the removal of interference, GPx showed a significant decrease (more than 50%) from $25.0ngg^{-1}$ to $12.1ngg^{-1}$. It was identified that the interference in blood serum was mostly from GPx and the use of AE SPE was proven to be efficient in eliminating Cl and Br that cause interference to GPx.