• Title/Summary/Keyword: 6LiF

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A Study OH Mossbauer Spectra Of the $Li_{0.5}Fe_{2.5-x}Al_xO_4$ Ferrite System (Li_{0.5}Fe_{2.5-x}Al_xO_4 페라이트계의 Mossbauer 스펙트럼 연구)

  • 백승도
    • Journal of the Korean Magnetics Society
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    • v.11 no.2
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    • pp.58-62
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    • 2001
  • The L $i_{0.5}$F $e_{2.5-x}$A $l_{x}$ $O_4$ systems (x=0, 0.3, 0.6, 0.9, 1.2, 1.5) were investigated by X-ray diffraction and Mossbauer spectroscopy. The structure of all the samples is cubic spinel type and lattice constant decrease with increasing Al content x. The Moissbauer spectra reveal two sextet for 0$\leq$x$\leq$0.6, two sextet and a doublet for 0.9$\leq$x$\leq$1.2, and a doublet for x=1.5. The cation distribution of the samples is (L $i_{1-a}$$^{+}$F $e_{a}$ $^{3+}$)$^{A}$[L $i_{a-0.5}$$^{+}$A $l_{2.5-a-x}$$^{+}$F $e_{2.5-a-x}$$^{3+}$]$^{B}$ $O_4$$^{2-}$ and substituted $Al^{3+}$ ions decrease the covalency of F $e^{3+}$- $O^{2-}$ bond in B-sites and A-B super-exchange interactions.tions.s.tions.ons.s.

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Comparison of Li-heparinized Versus Na-fluorinated Plasma for Routine Blood Glucose Determination Using Hexokinase Procedure (Hexokinase 방법을 이용한 Heparin 혈장과 NaF 혈장 시료의 혈당 분석치 비교)

  • Moon, In-Kyung
    • Korean Journal of Clinical Laboratory Science
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    • v.39 no.1
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    • pp.25-30
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    • 2007
  • In this study, the two sampling methods for blood glucose measurement were evaluated in order to reduce pre-analytical error. For this purpose, glucose levels of Li-heparinized plasma (LHP) and Na-fluorinated plasma (NFP) in blood collected from healthy volunteers were determined by using routine hexokinase procedures. The percentage range of pre-analytical error was quantitated by comparing LHP glucose values with NFP glucose values according to delaying analytical time (0, 60, and 120 min). LHP glucose values were decreased by 6.6% in 60 min., 17.7% in 120 min, whereas NFP glucose values decreased by 1.1% in 60 min, 2.0% in 120 min. Therefore it may be recommended that the NFP sampling method should be used for routine blood glucose determination in diabetes mellitus diagnosis.

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Characterization of Blue Organic Light Emitting Diodes using TPM-BiP (TPM-BiP 청색 형광 재료의 전계발광특성)

  • Chang, Ji-Geun;Shin, Sang-Baie;Ahn, Jong-Myoung;Chang, Ho-Jung;Lee, Hak-Min;Gong, Myoung-Sun;Kim, Min-Young;Kim, Jun-Woo
    • Journal of the Semiconductor & Display Technology
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    • v.6 no.2 s.19
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    • pp.11-14
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    • 2007
  • For the fabrication of blue color organic light emitting diodes(OLED) with a high performance, 2-TNATA [4,4',4"-tris (2-naphthylphenyl-phenylamino)-triphenylamine] as hole injection material and NPB [N,N'-bis (1-naphthyl) -N,N'-diphenyl-1,1'-biphenyl-4,4'-diamine] as hole transport material were deposited on the ITO (indium tin oxide)/glass substrate by the vacuum thermal evaporation. After then, blue color emission layer was deposited using TPM-BiP[(4'-Benzoylferphenyl-4-yl)phenyl-methanone-Diethyl(biphenyl-4-ymethyl)phosphonate] and GDI602 as a light emitting organic material. Finally, the two kinds of OLEDs with the structure of $ITO/2-TNATA/NPB/TPM-BiP/Alq_3/LiF/Al and ITO/2-TNATA/NPB/GDI602/Alq_3/LiF/Al$ were prepared by in-situ deposition. The maximum current density and luminance were found to be about $588\;mA/cm^2\;and\;5239\;cd/m^2$ at 12V for the OLED sample with the structure of $ITO/2-TNATA/NPB/TPM-BiP/Alq_3/LiF/Al$. Color coordinate of blue OLED was x=0.18, y=0.18 (at llV) and the maximum current efficiency was 2.82 cd/A (at 6V) with the peak emission wavelength of 440 nm.

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DNA Fingerprint Bands Correlated with the Egg Weight Performance of Hens

  • Huang, Haigen;Meng, Anming;Qi, Shunzhang;Gong, Guifen;Li, Junying;Wang, Hongwei;Chou, Baoqin
    • Asian-Australasian Journal of Animal Sciences
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    • v.12 no.1
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    • pp.1-4
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    • 1999
  • Beijing White Chickens laying larger eggs and smaller eggs were respectively used as parental individuals for mating to produce the F1 progeny and then the F1 progeny individuals mated to produce 125 individuals of the F2 progeny. Three bands associated with the egg weight performance were identified from DNA fingerprints of the 125 individuals generated with a bovine minisatellite probe BM6.5B. The simple linear correlation analysis showed that the coefficients of correlation between frequencies of the three bands (DB1, DB2 and DB3) and egg weights were -0.6, -0.6 and 0.9, respectively.

Electrical and Optical Properties of Phosphorescent Organic Light-Emitting Devices with a TAPC Host

  • Kim, Tae-Yong;Moon, Dae-Gyu
    • Transactions on Electrical and Electronic Materials
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    • v.12 no.2
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    • pp.84-87
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    • 2011
  • We fabricated phosphorescent organic light-emitting devices with a 1,1-bis[(di-4-tolylamino)phenyl]cyclohexane (TAPC) host layer. Two kinds of devices, one of ITO/TAPC/TAPC:FIrpic/TAZ/LiF/Al (device A) and one of ITO/TAPC:FIrpic/TAPC/TAZ/LiF/Al (device B), were prepared to investigate electrical and optical properties. Iridium(III) bis[(4,6-difluorophenyl)-pyridinato-N,$C^{2'}$]picolinate (FIrpic) and 3-(4-biphenylyl)-4-phenyl-5-(4-tert-butylphenyl)-1,2,4-triazole (TAZ) were used as a blue phosphorescent guest material and an electron transport layer, respectively. The TAPC layer in device B strongly contributes to whitish emission, higher driving voltage, and lower current efficiency characteristics compared with device A. The mechanisms of these electrical and optical characteristics of the devices were investigated.

Synthesis and Electroluminescent Properties of Cabazolyl Vinylene Derivatives

  • Seo, H.J.;Park, H.C.;Lee, S.E.;Park, J.W.
    • 한국정보디스플레이학회:학술대회논문집
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    • 2003.07a
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    • pp.952-954
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    • 2003
  • We report the photo-(PL) and electroluminescence (EL) properties of new conjugated compounds based on carbazolyl vinylene moiety, 3,3'-(1,4-phenylene di-2,1-ethenediyl) bis[9-ethyl-(E,E)-9H-carbazole](PEEC) and 3,3'-([1,1'-biphenyl]-4,4'-diyldi-2,1-ethenediyl)bis[9-ethyl-9H-carbazole](BPEEC), as emitting materials. The ITO/m-MTDATA/NPB/BPEEC/Alq3/LiF/Al device shows bluish-green EL spectrum at 490nm and turn-on voltage at 8V. PEEC shows bluish-green EL around ${\lambda}$ max=496nm and turn-on voltage at 6V and 2.4 Cd/A efficiency in ITO/m-MTDATA/NPB/PEEC/Alq3/LiF/Al device.

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Characteristics of Organic Light Emitting diodes with DCM derivatives (DCM-A 유도체를 이용한 유기 광전 변환 소자의 특성)

  • Mun, Soo-San;Lee, An-Sung;Han, Mi-Eun
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2010.06a
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    • pp.168-168
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    • 2010
  • DCM derivatives were newly synthesized. The OLEDs with a DCM-A as an emitting layer was fabricated and analyzed their opto-electrical properties. The structures of OLEDs were I) ITO/DCM-A/Al, II) ITO/-NPD/DCM-A/LiF/Al, and III) ITO/-NPD/DCM-A/Alq3/LiF/Al. The EL peak of the DCM-A shows the red emission in the range of 700 nm. The structure I) shows that 1050 nW/cm2 at 510 mA/cm2. The structure II) shows that takes the most excellent luminance about 39,000 nW/cm2 at 290 mA/cm2. The EL structure ill shows luminance about 13,000 nW/cm2 at 6 mA/cm2.

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ANSI 13.32 말단부 팬템에 의한 열형광말단선량계의 방향의존성 연구

  • 김종수;윤석철;윤여창
    • Proceedings of the Korean Nuclear Society Conference
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    • 1995.05b
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    • pp.889-894
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    • 1995
  • 본 연구에서는 ANSI N13.32(1995)에서 제시한 손가락, 손목/발목 기준 팬텀(1)을 설계 제작하여 Teledye사의 말단선량계(finger와 wrist dosimeter)에 대한 방향의존성 실험을 수행하였다. 방사선원으로는 PTB 2차 베타표준선원 $^{204}$Tl(0.24 MeV), $^{90}$ sr/Y(0.8 MeV) 그리고 $^{l37}$ Cs(0.66 MeV) 표준 감마선원을 사용하였으며, 말단선량계로는 LiF Teflon(D-LiF-7-0.13)을 사용하였다. 90$^{\circ}$ 에서 $10^{\circ}$ 까지 20$^{\circ}$ 씩 수직과 수평으로 팬텀을 회전하여 정상각과 비정상각에 대한 상대응답을 제시하였다. 실험결과 90$^{\circ}$에서 모든 선량계는 잘 일치하였다. $^{90}$ Sr/Y은 50$^{\circ}$ 정도에서 다소 방향의존성이 적은 결과를 보였으며, $^{204}$ TI는 20$^{\circ}$에서 최소 13% 정도의 심한 방향의존성이 나타났다. 또한 $^{137}$Cs은 $10^{\circ}$에서도 최대 10.6% 정도의 적은 방향의존성을 나타냈다. 본 실험의 결과로부터 말단선량계는 저에너지와 낮은 투과 방사선[2]에서 심하게 방향의존성이 나타남을 알 수 있었다.

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Determination of Microamounts of Copper by Fluorescence X-Ray Analysis (형광 X-선 분석에 의한 미량 구리의 정량)

  • Choi Won-hyung;Kim Chan-ho
    • Journal of the Korean Chemical Society
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    • v.16 no.6
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    • pp.373-377
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    • 1972
  • The analytical conditions for the fluorescence X-ray determination of small amount of cupper in solution were established. Copper in solution was extracted by diethyldithiocarbamate ethyl acetate and adsorbed by zinc powder. After drying, it was pressed to tablet under the pressure of $250Kg/cm^2.$$K_{\alpha}2(2{\theta}_{LiF} = 45.08^{\circ})$. The limit of detection was estimated to be about $10{\mu}g$ by the method of standard addition with an error of 10 %.

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The Fabrication of Low Temperature Firing Substrate of $Li_2O-MgO-MgF_2-SiO_2-B_2O_3$ system

  • Park, Jung-Houn;Park, Dae-Hyun;Kang, Won-Ho
    • Journal of the Microelectronics and Packaging Society
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    • v.6 no.4
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    • pp.35-39
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    • 1999
  • The $Li_2O-MgO-MgF_2-SiO_2$glasses with addition of $B_2O_3$ were investigated in order to make glass-ceramics for low temperature firing substrate. Glasses were made by melting at $1450^{\circ}C$ in the electronic furnace and crystallized at $750^{\circ}C$. The crystal phases were polycrystalline of lithium boron fluorphlogopite and lithium fluorhectorite. The crystal shape was chanced to granule type from needle type with increasing $B_2O_3$ content. Average particle size of the glass-ceramics after water swelling was 3.77$\mu\textrm{m}$. The optimum sintering temperature and sintering shrinkage of the substrate were $900^{\circ}C$ and 13.4%, respectively.

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