• 한국세라믹학회지
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• 제29권7호
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• pp.511-516
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• 1992

In this study, SiC powder and Si powder were used as the raw materials. Mixture was prepared with addition of Al2O3 and Fe2O3 at 0.1~0.5wt% respectively. After this step, the mixture was pressed and nitrided for 30 hrs at 140$0^{\circ}C$ under NH3-N2 atmosphere. Mechanical properties of sintered specimens were investigated from measurement of porosity, bulk density and three point bending test. nitration reaction extent was observed at the change of mass before and after reaction, and the microstructure and the change of $\alpha$-Si3N4 and $\beta$-Si3N4 were observed by XRD and SEM. In the current work, the results are as follows 1. When Fe2O3 added, the nitridation increased with the content of Fe2O3, and the bending strength was increased from 0.1 wt% to 0.3 wt%, and decreased to 0.5 wt%. 2. When Al2O3 added, the nitridation and the bending strength increased little by little with the content of Al2O3 3. The bending strength of the specimen added with Fe2O3 were higher than that with Al2O3. Because the specimens contained Fe2O3 had much more the whisker type crystal of Si3N4 contributing to strength than contained Al2O3.

• 산업기술연구
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• 제20권A호
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• pp.169-178
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• 2000

The 4-point bending tests have been performed In order to estimate the effect of TIG-dressing on fatigue strength and fatigue characteristics quantitatively for non load-carrying fillet welded joints subjected to pure bending. As a result of fatigue tests, fatigue strengths of as-welded specimens have satisfied the grade of fatigue strength prescribed in specifications of korea, AASHTO and JSSC. Fatigue strength at 2 million cycles of TIG-dressing specimens have increased compared with as-welded specimens. As the result of beachmark tests, fatigue cracks occurred at several points, where the radius of curvature and flank angle in the weld bead toes were low, and grew as semi-elliptical cracks, then approached to fracture. As a result of finite element analysis, stress concentration factor in weld bead toes has closely related to the flank angle and radius of curvature, and between these, the radius of curvature has more largely affected in stress concentration factor than flank angle. As a result of fracture mechanics approaches, the crack correction factor of test specimens has largely affected on stress gradient correction factor in case a/t is below 0.4. From the relations between stress intensity factor range estimated from FEM analysis and fatigue crack growth rate, fatigue life has been correctly calculated.

• 열처리공학회지
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• 제7권3호
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• pp.160-168
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• 1994

This was studied about mechanical characteristic of AC4A/SiCw 10-30% reinforced composites. Tensile strength of pressed base metal(base metal) with SiCw preform was higher than without pressed base metal(AC4A). If SiCw whisker volume fraction was increased, tensile strength at room temperature was increased. And tensile strength of SiCw 30% was about $35kg/mm^2$. Tensile strength of SiCw 30 % $400^{\circ}C$ at same time aging was the most excellence, about $40kg/mm^2$. The fracture energy value of composite material at three point bending test was higher than AC4A. Dislocation at matrix of composite material was evenly distributed. But dislocation around whisker of composite material was more existed than matrix. The reasom was thought of pile-up around whisker.

• 대한토목학회논문집
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• 제32권2A호
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• pp.65-73
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• 2012

본 연구에서는 PSC 거더교의 장경간 적용을 위해 개발된 Half-Decked PSC 거더의 구조적 성능을 실험하였다. 이를 위해 힌지-롤러의 지점 조건의 단순교로 설계된 60 m 경간의 실물 크기 거더를 제작하여 4점 재하실험을 수행하였다. 거더의 중앙을 기준으로 양쪽으로 5.5 m 씩 떨어진 위치에 가력장치를 설치 후 1 kN/sec의 속도로 하중을 재하하여 총 4단계에 걸쳐 반복하중을 가하였다. 1단계부터 4단계까지 1,000 kN, 1,200 kN, 1,500 kN, 2,000 kN의 하중을 재하하고 제거하기를 반복하며 거더의 변위, 콘크리트와 철근의 변형률, 균열 등을 확인하였다. 이를 분석하여 거더의 내하력을 평가하고 하중 제거 시 나타나는 복원력 등을 살펴보았다. 1,400 kN 인근에서 초기 휨균열이 발생하여, 이 시점부터 하중 재하 시 비선형 성이 나타나며 뚜렷한 잔류변형이 계측되었다. 초기 균열이 1등교 기준의 사용하중보다 2배 이상 큰 하중에서 계측되어 충분한 내하력을 갖고 있는 것으로 나타났다. 실험 결과의 검증을 위해 수치해석을 수행하여 결과 값을 비교하였고 그 결과 실험 결과와 해석 결과의 유사한 거동을 확인하였다. 본 연구에서 개발된 거더의 정적재하실험을 통하여 그 구조적 성능을 입증하였으며, 이를 바탕으로 Half-Decked PSC 거더 형식의 60 m 경간 실교량 설계 적용 가능성을 확인하였다.

• 한국안전학회지
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• 제11권3호
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• pp.20-24
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• 1996

Indentation fracture method and 4-point bending test are carried out to measure the residual stresses and the bending strength, and to investigate the mechanism of fracture mechanics in the bonded interface of ceramic and metal. The results obtained are as follows ; 1) The fracture patterns of bonded materials shows that the delamlnatlon fracture of Interfaces is stablely developed from the interfaces of ceramic/active metallic bonded materials at the specimen center, and the fracture is unstablely generated through a refraction on the middle ceramic. 2) Distribution of residual stresses is quantitatively investigated on the ceramic side of bonded materials. 3) It Is found that the residual stresses of interface vertical direction are concentrated on the bonded interface at the ceramic side.

• The Journal of Advanced Prosthodontics
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• 제10권1호
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• pp.43-49
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• 2018

PURPOSE. The purpose of this in vitro study is to examine the effects of a nano-structured alumina coating on the adhesion between resin cements and zirconia ceramics using a four-point bending test. MATERIALS AND METHODS. 100 pairs of zirconium bar specimens were prepared with dimensions of $25mm{\times}2mm{\times}5mm$ and cementation surfaces of $5mm{\times}2mm$. The samples were divided into 5 groups of 20 pairs each. The groups are as follows: Group I (C) - Control with no surface modification, Group II (APA) - airborne-particle-abrasion with $110{\mu}m$ high-purity aluminum oxide ($Al_2O_3$) particles, Group III (ROC) - airborne-particle-abrasion with $110{\mu}m$ silica modified aluminum oxide ($Al_2O_3+SiO_2$) particles, Group IV (TCS) - tribochemical silica coated with $Al_2O_3$ particles, and Group V (AlC) - nano alumina coating. The surface modifications were assessed on two samples selected from each group by atomic force microscopy and scanning electron microscopy. The samples were cemented with two different self-adhesive resin cements. The bending bond strength was evaluated by mechanical testing. RESULTS. According to the ANOVA results, surface treatments, different cement types, and their interactions were statistically significant (P<.05). The highest flexural bond strengths were obtained in nano-structured alumina coated zirconia surfaces (50.4 MPa) and the lowest values were obtained in the control group (12.00 MPa), both of which were cemented using a self-adhesive resin cement. CONCLUSION. The surface modifications tested in the current study affected the surface roughness and flexural bond strength of zirconia. The nano alumina coating method significantly increased the flexural bond strength of zirconia ceramics.

• 대한기계학회논문집A
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• 제26권5호
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• pp.835-842
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• 2002

In this paper, static and fatigue bending strengths and failure mechanisms of CFRP (carbon fiber reinforced plastics) laminates having impact damages have been evaluated. Composite laminates used for this experiment are CF/EPOXY orthotropy laminated plates, which have two-interfaces $[0^0_ 4/90^0_4]_{ sym}$. A steel ball launched by the air gun collides against CFRP laminates to generate impact damages. The damage growth during bending fatigue test is observed by the scanning acoustic microscope (SAM) and also, the fracture surfaces were observed by using the SEM (scanning electron microscope). In the case of impacted-side compression, fracture is propagated from the transverse crack generated near impact point. On the other hand, fracture is developed toward the impact point from the edge of interface-B delamination in the case of impacted-side tension. Eventually, failure mechanisms have been confirmed based on the observed delamination areas and fracture surfaces.

• 복합신소재구조학회 논문집
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• 제6권2호
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• pp.8-16
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• 2015

Prestressed concrete (PSC) is a method in which prestressed tendon is placed inside and/or outside the reinforced concrete member and the compressive force applied to the concrete in advance to enhance the engineering properties of concrete member which is weak under tension. In this paper we suggested the precast PSC girder assembled with segments of portable size and weight at the factory. The segments of precast PSC girder will be delivered and assembled as a unit of PSC girder at the site. Consequently, we suggested new-type of precast segmented PSC girder with different shapes of segment cross-section (i.e., I-shape, Box-shape). To mitigate the problems associated with the field splice between the segments of precast PSC girder anchor system is attached near the neutral axis of the girder and relatively uniform compression throughout the girder cross-section is applied. Prior to the experimental investigation, analytical investigation on the structural behavior of precast PSC girder was performed and the serviceability (deflection) and safety (strength) of the girder were confirmed. In addition, 4-point bending test on the girder was conducted to investigate the structural performance under bending. From the experimental investigation, it was found that the precast PSC girder spliced with 3 and 5 segments has sufficient in serviceability and safety conditions and it was also observed that the point where the segments spliced has no defects and the girder behaves as a unit.

• 대한치과기공학회지
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• 제33권4호
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• pp.283-289
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• 2011

Purpose: The purpose of this study was to evaluate flexural strength of full zirconia crown using block after clinical work. Methods: The three point bending test was used to measure the flexural strength of zirconia block. Statistical analysis was done using the Statistical Package for Social Sciences version 19.0 for Windows. As for the analysis methods, the study used analysis of variance, Tukey's test. Results: The ave Rage value of flexural strengths of WIELAND, Zirkonzahn, Hass, D-MAX were 516.2 MPa, 612.6MPa, 566.2MPa, 744.6MPa. The ave Rage value of Surface Roughness of WIELAND, Zirkonzahn, Hass, D-MAX were 0.39Ra, 0.33Ra, 0.33Ra, 0.47Ra. Conclusion: Flexural strength of zirconia block decreased after clinical work. Flexural strength of zirconia block is equal to or higher than flexural strength of dental metal, so zirconia block can be used as dental material.

• Restorative Dentistry and Endodontics
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• 제44권4호
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• pp.45.1-45.10
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• 2019

Objectives: Self-adhesive resin cements contain functional monomers that enable them to adhere to the tooth structure without a separate adhesive or etchant. One of the most stable functional monomers used for chemical bonding to calcium in hydroxyapatite is 10-methacryloyloxydecyl dihydrogen phosphate (10-MDP). The aim of this study was to evaluate the influence of the10-MDP concentration on the bond strength and physical properties of self-adhesive resin cements. Materials and Methods: We used experimental resin cements containing 3 different concentrations of 10-MDP: 3.3 wt% (RC1), 6.6 wt% (RC2), or 9.9 wt% (RC3). The micro-tensile bond strength of each resin cement to dentin and a hybrid resin block (Estenia C&B, Kuraray Noritake Dental) was measured, and the fractured surface morphology was analyzed. Further, the flexural strength of the resin cements was measured using the three-point bending test. The water sorption and solubility of the cements following 30 days of immersion in water were measured. Results: The bond strength of RC2 was significantly higher than that of RC1. There was no significant difference between the bond strength of RC2 and that of RC3. The water sorption of RC3 was higher than that of any other cement. There were no significant differences in the three-point bending strength or water solubility among all three types of cements. Conclusions: Within the limitations of this study, it is suggested that 6.6 wt% 10-MDP showed superior properties than 3.3 wt% or 9.9 wt% 10-MDP in self-adhesive resin cement.