• Tribology and Lubricants
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• v.32 no.1
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• pp.32-37
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• 2016

The wear characteristics of metal ball and seat in a metal-seated ball valve significantly affect the performances such as leakage and valve torque. In this work, the wear characteristics of metal ball and seat are experimentally investigated. A stainless steel ball and seat with a high corrosion-resistant coating are prepared and a component level test was performed. The hardness and surface roughness of specimens cut from the metal ball and seat are measured before and after the test using a micro-Vickers hardness tester and confocal microscopy, respectively. In order to assess the wear characteristics, the surfaces of the specimens are carefully examined after the test. The confocal microscope data show that the surface roughness values of both the ball and seat increase by a factor of 3-4, which may lead to an increase in valve torque. However, the wear of the seat is found to be more significant than that of the ball. In addition, a comparison of the surfaces of the ball and seat before and after testing revealed that adhesive and abrasive wear are the major wear mechanisms. The results of this study may aid in the design of metal-seated ball valves from the tribological point of view.

• Tribology and Lubricants
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• v.16 no.6
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• pp.477-483
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• 2000

Rolling contact fatigue (RCF) tests were performed for two kinds of commercial silicon nitride balls using 4-Ball rolling contact fatigue life tester under EHL condition (Λ=8.9) and boundary lubrication condition (Λ=0.2). All the test balls were finished up to the dimensional accuracy of Grade 5 defined in KS B 2001 (Steel Balls for Ball Bearings) with a size of 8.731 mm. RCF tests were then conducted under the initial theoretical maximum contact stress 6.63 GPa and the spindle speed 10,000 rpm. All the test balls were not failed until 3.75 $\times$ 107 contact cycles and wear tracks of test balls were not conspicuous under EHL condition (Λ= 8.9). In the operations of low lambda regime (Λ= 0.2), all the test balls were surface damaged and high rolling wear resistance was achievable in fully densified using MgO 1 wt% and HIPed balls. Rolling wear of silicon nitride balls under boundary lubrication condition depend mainly on grain size and intergranular phase content of silicon nitride balls.

• Tribology and Lubricants
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• v.11 no.5
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• pp.184-189
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• 1995

The antiwear performance of dialkyl 3, 5-di-t-butyl 4-hydroxy benzyl phosphonates was investigated using a four ball wear test machine. Diethyl 3, 5-di-t-butyl 4-hydroxy benzyl phosphonate (DEP) and dibutyl 3,5-di-t-butyl 4-hydroxy benzyl phosponate (DBP) among them showed excellent antiwear performances compared with conventional additives, ZDDP and TCP as the bulk oil temperature and the sliding velocity increased. The surface analysis through an optical microscopy was conducted for tribological studies.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 2002.10b
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• pp.155-156
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• 2002

During the sliding between a-CNx and $Si_3N_4$, applying nitrogen as environmental gas provided very low friction as the level of 0.01 in friction coefficient. In order to know the effect of the running-in process on the reduction of the friction, the effect of surface roughness of mating surface on friction was investigated. It was shown that smooth surface in wear scar of ball provided low friction coefficient. Friction coefficient after running-in was proportional to the Ry value of wear scar of ball. Also smooth thin transferred layer was observed on the wear scar of balls with an AFM after sliding test. Those results showed the smoothing of wear scar of ball, the generating of the transferred layer from CNx was necessary for low friction.

• Tribology and Lubricants
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• v.19 no.3
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• pp.159-166
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• 2003

This research for replacement of chlorine or sulfur based EP(extreme pressure) -additives which is restricted materials by environmental regulation. The subject of this study is as follows, 4-ball test and friction coefficient test were experimented in accordance with temperature and velocity, compounding with several organic or inorganic metallic elements. After 4-ball test, wear area of steel ball was analysed by SEM-EDX. As the analysis, organic and inorganic elements make a effect for extreme pressure lubricity. It is shown that the friction coefficient of lubricant which includes chlorine or sulfur additives, the scoring phenomenon is found accord-ing to temperature and the scuffing phenomenon at 200$^{\circ}C$. Applying to Na, P, S, Zn, Ca based on inorganic and organic elements, the result showed that friction coefficient is decreased more and more, as increasing temperature of lubricant. The additive based on S, Cl, P elements is effect far extreme pressure in the sample#1 and Na, P, S, Zn, Ca in sample #2. These elements are environmental contaminants and S, Cl based on EP additives which are very popular in domestic industry, when they are properly composed with non-chlorine based on additives and Na, P, S, Zn, Ca organic or inorganic elements. It is showed that lubricity and excellent anti-wear properties.

• Journal of Surface Science and Engineering
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• v.47 no.1
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• pp.13-19
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• 2014

The various surface treated conditions of Fe-3.0%Ni-0.7%Cr-1.4%Mn-X steel such as as-received, ion nitriding, DLC coated, DLC coated after nitriding for 3 hrs and 6 hrs were investigated to evaluate the beneficial effect for plastic mold steel. Micro Vickers hardness tester was used to estimate nitriding depth from the hardness profile and to measure hardness on the surface. Elastic modulus and residual stress were measured by a nanoindentator. Scratch test and SP (small ball punch test) were utilized to assess the adhesive strength of DLC coating. The depth of nitriding layer was measured as $50{\mu}m$ for the condition of 3 hrs nitriding and $90{\mu}m$ for that of 6 hrs nitriding. Hardness, elastic modulus, residual stress of DLC coating were 20.37 GPa, 162.78 GPa and -1456 MPa respectively. Residual stress on the surface of DLC coating after nitriding could increase to -3914 MPa by introducing nitriding before DLC coating. During the 'Ball-On-Disc' test ${\gamma}^{\prime}$ particles pulled out from the surface of nitrized layer tend to enhance abrasive wear mode since the fraction of ${\gamma}^{\prime}$ (Fe4N) in ion-nitrized layer is known to increases with nitriding time. Thus the specific wear rate of the nitriding layer increased. Comparing with nitriding the specific wear rate in work piece disc as well as ball decreased prominently in DLC coating due to the remarkable reduction in friction coefficient.

• Tribology and Lubricants
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• v.33 no.4
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• pp.141-147
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• 2017

The vibration data of bearings are very useful for monitoring and determining the condition of the bearings. The defect frequencies of ball bearings have been used for monitoring there condition. However, it is not easy to verify the defect frequencies as the wear progress. Therefore there is a need for an easy method to monitor the damages of bearings in real-time and to observe the variations in vibration characteristics as the wear progress. In this study, a bearing test equipment is constructed to diagnose the damage of bearings. The friction coefficient and vibration data are measured by using a torque sensor and an acceleration sensor, and the correlation between the measured data is analyzed to diagnose the condition of the bearing. We reached the following conclusions from the results. When the ball surface, inner and outer rings of a ball bearing are damaged, the friction coefficient increases to over 0.02 with an adhesion on the surface. Moreover this damage occurs more quickly with an increase in the number of revolutions. In the vibration characteristics, the amplitude of vibration wave appears high with an increase in the friction coefficient. In the high frequency range between 1000 and 2000 Hz, a wide range of frequency components with high amplitude occurs continuously irrespective of the number of revolutions.

• Tribology and Lubricants
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• v.7 no.1
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• pp.40-45
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• 1991

Wear performances for dibutyl 3,5-di-t-butyl 4-hydroxy benzyl phosphonate (DBP) were invesitigated using the four ball test machine under sliding and also rolling contact conditions, and compared with ZDDP. DBP showed excellent antiwear performace compared with ZDDP under severe sliding contact. Also, DBP achieved a longer fatigue life than ZDDP under rolling contact conditions. The surface of the worn balls was observed using an optical microscope, and the wear derbis generated was measured using the Particle Quantifier (PQ).

• Tribology and Lubricants
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• v.6 no.2
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• pp.68-75
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• 1990

The metal-dithiophosphates as lubricant additives for reducing friction and wear, increasing load-carrying capacity and a antioxidant are very important as new additives developed in these day. The synthetic results of Metal-DTPs were described. The wear test was conducted with 4-Ball machine and wear debris were analyzed by ferrography. The tribological performances of Metal-DTPs were compared with Zn-DTP.

• Journal of the Korean Ceramic Society
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• v.33 no.2
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• pp.192-202
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• 1996

In Li0.4Ca0.05AlP0.5Si0.75O4.5 composition glass, glass-ceramic having a near 100% crystallinity after nucleation heat treatment of 74$0^{\circ}C$/2 h and crystallization heat treatment of 90$0^{\circ}C$/2 h and in-situ TiO2 whisker reinforced glass-ceramic after heat treatment of 105$0^{\circ}C$ for 20 h were fabricated with the addition of 4% TiO2 as a nucleating agent. With these materials a ball-on-disc type wear test was conducted in order to examine the effect of TiO2 whisker prepcipitation on ambient and high temperature wear properties of the glass-ceramic. Wear test results indicated that all specimens exhibited micro-fracture wear mechanism in ambient temperature. As temperature increased the wear rates of the materials were increased. However the in-situ TiO2 whisker reinforced glass-ceramic exhibited the lowest wear rate over the test temperature range. This resulted from the improvement of harness and fracture toughness of the material as the glass converted into the glass-ceramic followed by precipitation of TiO2 whiskers throughout the glass-ceramic matrix.