• Transactions of Materials Processing
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• v.8 no.3
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• pp.253-253
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• 1999

Dense WC-10 vol.%Co composite was simultaneously synthesized with field-activated and pressure-assisted combustion synthesis (FAPACS) within several minutes in one step from elemental powders of W, C and Co. Combustion synthesis was carried out under the combined effect of an electric field and mechanical pressure. Under the application of 60MPa pressure and 3000A current on the reactants, the relative density of WC-10 vol.%Co composite was 98.4%. The fracture toughness and hardness of WC-10 vol.%Co were 8.6 MPa·$m^{1/2}$ and 1900 kg/mm², respectively.

• Journal of the korean academy of Pediatric Dentistry
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• v.24 no.1
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• pp.112-124
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• 1997

According to extensive use of composite resin which have superior esthetic property, every effort on improving bonding strength between a tooth and composite resin has been continued. Acid etching technique is a method that micro-etches the tooth surface which provides bonding with composite resin possible. Recently, there were several reports that mechanical treatment obtained from air-abrasion can provide similar bonding strength with acid etching technique. So, this experimental study was designed to compare the shear bonding strength between using air-abrasion technique and using acid etching technique. Initially, bovine teeth were divided into enamel and dentin experimental groups. Respectively each group was categorized into three subgroups. One subgroup was acid etched with 35% phosphoric acid, then bonded with composite resin. The other subgroup was air-abraded with $50{\mu}m$ $Al_2O_3$ particles sprayed with 160psi air pressure using air abrasion unit(KCP-1000, A.D.T., U.SA), and composite resin was bonded. In another subgroup, composite resin was bonded after acid etching following air-abrasion. So, enamel experimental groups were made of E1 (acid etched only), E2(air-abraded only), E3(acid etched following air-abraded), and dentin experimental groups were made of D1(acid etched only), D2(air-abraded only), D3(acid etched following air-abraded). Each subgroup had 10 specimens. Dentin bonding system(Scotchbond Multi-purpose, 3M Co., U.S.A.) and composite resin(Z-100, 3M Co., U.S.A.) were applied on treated surface using 5mm diameter gelatin capsule as manufacturer's direction. After 1200 times thermocycling between $5^{\circ}C$ and $55^{\circ}C$, shear bond strength was measured in 5mm/min crosshead speed with Instron(Instron Co., U.S.A.), and also treated enamel and dentin were observed with SEM(JEOL Co., Japan). The following results were obtained: 1. In the enamel experimental groups, acid etched following air-abraded group had highest shear bond strength, but there was no significant difference compared to acid etched group. Air-abraded only group had lowest shear bond strength, and there was significant difference compared to the rest of groups. 2. In the dentin experimental groups, acid etched following air-abraded group had highest shear bond strength, but there was no significant difference compared to acid etched group. Air-abraded only group had lowest shear bond strength, and there was significant difference compared to the rest of groups. 3. In the SEM study, air-abraded enamel and dentin had irregular and rough surfaces.

• Proceedings of the KIEE Conference
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• 1989.11a
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• pp.72-74
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• 1989

A composite with 1-3 connectivity was fabricated by filling spurrs epoxy in arried PZT bars. The composite bad lower density(2220 Kg/$m^3$), lower dielectric constant, lower piezoelectric coefficient d33(260*$10^{12}$ C/N), and higher voltage coefficient(110.1*$10^{-3}$ Vm/N) than that of solid PZT. The probe was fabricated by using composite transducer that was made above. The underwater testing of the composite transducer was performed with water backing.

• Proceedings of the Korean Magnestics Society Conference
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• 2009.12a
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• pp.192-192
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• 2009

Magnetic and magnetotransport properties of (1-x) $La_{0.7}Sr_{0.3}MnO_3-xRE_2O_3$ (RE=La, Nd) (x = 0.025, 0.05, 0.075, 0.1, 0.2, 0.3) composite polycrystalline samples were systematically studied. Samples were prepared using conventional solid-state reaction. LSMO and $RE_2O_3$ react at high temperature and become chemically compatible. The ferromagnetic-paramagnetic transition temperatures ($T_c$) of the LSMO-$Nd_2O_3$ composite samples were decreased 313K~349K with increasing x, while the $T_c$ values of the LSMO-$La_2O_3$ composite samples were almost unaltered in the range of 355K~358K, representing that the ferromagnetism of LSMO might be more seriously degraded by Nd substitution on the ($La_{0.7}Sr_{0.3}$) site. However, LSMO-$RE_2O_3$ composite samples exhibit greatly enhanced low field magnetoresistance (LFMR) and dMR/dH value without an appreciable increase in its resistivity. Remarkably improved LFMR properties are attributed to LSMO grain boundaries acting as effective spin-dependent scattering centers. The relationship among the $RE_2O_3$ addition, microstructure, magnetic and magnetotransport properties will be discussed in this paper.

• Polymer(Korea)
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• v.25 no.6
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• pp.866-875
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• 2001

In this work, thermal decomposition mechanism based on kinetic parameters and thermal stability of carbon fiber-reinforced carbon matrix composites (C/C composites), have been studied under high temperature oxidative conditions with addition of tetra-ethylorthosilicate (TEOS) as an oxidation inhibitor. Thermogravimetric analysis (TGA) was executed to evaluate the thermal decomposition mechanism and thermal stability of C/C composites in the temperature range of 30 ～ $850^{\circ}C$. As a result, the kinetic parameters of the composites impregnated with TEOS, i.e., activation energy for thermal decomposition ($E_d$), order of reaction (n) , and pre-exponential factor (A) were evaluated as 136 kJ/mol, 0, and 2.3$\times$$10^9s^{-1}$, respectively. Especially, the IPDT and $E_d$ of C/C composites impregnated with TEOS were improved largely compared with the composites impregnated without TEOS, due to the formation of $SiO_2$ on composite surfaces, resulting in interrupting the oxygen attack to carbon active site in the composites.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2003.04a
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• pp.113-116
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• 2003

The investigation of delamination growth behavior in hybrid composite material such as FRMLs should be considered delamination growth rate, dA_D/da$ using the delamination shape factor, $f_S$ instead of traditional fracture mechanics parameters. The main objective of this study is to evaluate the relationship between delamination element (i. e. delamination width, b, delamination contour, c, delamination shape factor, $f_S$ and delamination growth rate, dA_D/da$) and delamination growth in FRMLs under cyclic bending moment. The delamination shape formed along the fatigue crack between aluminum layer and glass fiber/epoxy layer are measured by scanning method. The details of study are as follow : ⅰ) Relationship between crack length, a and delamination width, b. ⅱ) Variation of delamination growth rate, dA_D/da$ was attendant on delamination shape factors, $f_{S1}$, $f_{S2}$, $f_{S3}$. The test result indicated the delamination growth behavior depends in delamination element such as delamination width, b, delamination shape factors, $f_{S1}$, $f_{S2}$, $f_{S3}$.

• Environmental Engineering Research
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• v.21 no.3
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• pp.311-317
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• 2016

A new type of biofilter packed with composite carriers was designed for tertiary denitrification of the secondary effluent with removal of both oxidized nitrogen and suspended solids (SS). At the empty bed residence time of 15 min and organic carbon to nitrate nitrogen ($C/NO_3-N$) ratios of 2, 1.5 and 1 g/g, the removal percentage of $NO_3-N$ was 67%, 58% and 36% in the ethanol biofilter, and was 61%, 43% and 26% in the acetate biofilter, respectively. The biofilters packed with composite carriers removed SS effectively, with the effluent turbidity in both biofilters of less than 3 NTU. During the operating cycle between the biofilter backwashings, the $NO_3-N$ removal percentage decreased initially after backwashing, and then gradually increased. Under $C/NO_3-N$ ratios of 2, 1.5 and 1 g/g, the $NO_3-N$ reduction rate was 1.75, 1.04 and $0.68g/m^2/d$ in the ethanol biofilter, and was 1.56, 1.07 and $0.76g/m^2/d$ in the acetate biofilter, respectively. In addition, during denitrification, the ratio of the consumed chemical oxygen demand to the removed $NO_3-N$ was 5.06-8.23 g/g in the ethanol biofilter, and was 4.26-8.6 g/g in the acetate biofilter.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2002.05a
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• pp.188-191
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• 2002

3-D orthogonal woven carbon/Al composites were fabricated using a pressure infiltration casting method. Especially, to minimize geometrical deformation of fiber pattern and $Al_4C_3$ formation, the process parameters of the minimum pressurizing force, melting temperature, delay and holding time of molten aluminum pressurizing was optimized through the PC-controlled monitoring system. Resonant ultrasound spectroscopy (RUS) was utilized to measure the effective elastic constants of 3-D orthogonal woven carbon/Al composites. The CTE measurement was conducted using strain gages in a heating oven.

• The Journal of Advanced Prosthodontics
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• v.12 no.5
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• pp.322-328
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• 2020

PURPOSE. This study evaluated the shear bond strength between 3D printed provisional resin and conventional provisional resin depending on type of conventional provisional resin and different surface treatments of 3D printed resin. MATERIALS AND METHODS. Ninety-six disc-shaped specimens (Ø14 mm × 20 mm thickness) were printed with resin for 3D printing (Nextdent C&B, Vertex-Dental B. V., Soesterberg, Netherlands). After post-processing, the specimens were randomly divided into 8 groups (n=12) according to two types of conventional repair resin (methylmethacrylate and bis-acryl composite) and four different surface treatments: no additional treatment, air abrasion, soaking in methylmethacrylate (MMA) monomer, and soaking in MMA monomer after air abrasion. After surface treatment, each repair resin was bonded in cylindrical shape using a silicone mold. Specimens were stored in 37℃ distilled water for 24 hours. The shear bond strength was measured using a universal testing machine at a crosshead speed of 0.5 mm/min. Failure modes were analyzed by scanning electron microscope. Statistical analysis was done using one-way ANOVA test and Kruskal-Wallis test (α=.05). RESULTS. The group repaired with bis-acryl composite without additional surface treatment showed the highest mean shear bond strength. It was significantly higher than all four groups repaired with methylmethacrylate (P<.05). Additional surface treatments, neither mechanical nor chemical, increased the shear bond strength within methylmethacrylate groups and bis-acryl composite groups (P>.05). Failure mode analysis showed that cohesive failure was most frequent in both methylmethacrylate and bis-acryl composite groups. CONCLUSION. Our results suggest that when repairing 3D printed provisional restoration with conventional provisional resin, repair with bis-acryl composite without additional surface treatment is recommended.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09b
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• pp.948-949
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• 2006

An infiltration technique using W-Cu composite powder has been developed to enhance microstructural uniformity of W-Cu pseudo-alloy. W-Cu composite powder, manufactured by reduction from $WO_3$ and CuO powder mixtures, were blended with W powder and then cold iso-statically pressed into a cylindrical bar under 150 MPa. The pressed samples were pre-sintered at $1300^{\circ}C$ for 1 hour under hydrogen to make a skeleton structure. This skeleton structure was more homogeneous than that formed by using W and Cu powder mixtures. The skeleton structures were infiltrated with Cu under hydrogen atmosphere. The infiltrated W-Cu pseudo-alloy showed homogeneous microstructure without Cu rich region