• 약학회지
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• 제28권1호
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• pp.21-23
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• 1984

High performance amino acid analyzing method has been developed for the routine analysis of taurine in preparations. Ion-exchange resin #2619 Hitachi Custom Ion-Exchange Resin, $2.6(I.D.){\times}150$(length)mm was used as column, buffer I, pH 3.3 as mobile phase. The retention time of taurine was 7 minutes. Calibration curve by peak height for standard taurine was linear from 2.5ppm to 25ppm. The reproducibility showed relative standard deviation $\pm$1.9% when analyzed 10 times for standard solution. The samples could be continuously analyzed without regenerating the resin between samples. Five samples were applied to column every 12 min. and then the resin was regenerated for 30 min. during one analyzing cycle time, 90 min. The automatic amino acid analyzer has made it possible to assay multiple samples in a relatively short period of time using the analytical magnetic program card. The high sensitivity and specificity of the analytical column of the automatic amino acid analyzer permits the routine analysis of taurine in preparations.

• Journal of Communications and Networks
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• 제17권6호
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• pp.634-646
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• 2015

Assuming perfect channel state information (CSI) at the transmitter and receiver, the optimization problem of maximizing the minimum Euclidean distance between two received signals by a linear precoder is considered for multiple-input multiple-output (MIMO) systems with arbitrary dimensions and arbitraryary quadrature amplitude modulation (QAM) input. A general precoding framework is first presented based on the Gram matrix, which is shown for 2-dimensional (2-D) and 3-dimensional (3-D) MIMO systems when employing the ellipse expanding method (EEM). An extended precoder for high-dimensional MIMO system is proposed following the precoding framework, where the Gram matrix for high-dimensional precoding matrix can be generated through those chosen from 2-D and 3-D results in association with a permutation matrix. A complexity-reduced maximum likelihood detector is also obtained according to the special structure of the proposed precoder. The analytical and numerical results indicate that the proposed precoder outperforms the other precoding schemes in terms of both minimum distance and bit error rate (BER).

• Advances in nano research
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• 제11권6호
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• pp.621-640
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• 2021

Effect of thickness stretching on mechanical behavior of functionally graded (FG) carbon nanotubes reinforced composite (CNTRC) laminated nanoplates resting on elastic foundation is analyzed in this paper using a novel quasi 3D higher-order shear deformation theory. The key feature of this theoretical formulation is that, in addition to considering the thickness stretching effect, the number of unknowns of the displacement field is reduced to four, and which is more than five in the other models. Single-walled carbon nanotubes (SWCNTs) are the reinforced elements and are distributed with four power-law functions which are, uniform distribution, V-distribution, O-distribution and X-distribution. To cover various boundary conditions, an analytical solution is developed based on Galerkin method to solve the governing equilibrium equations by considering the nonlocal strain gradient theory. A modified two-dimensional variable Winkler elastic foundation is proposed in this study for the first time. A parametric study is executed to determine the influence of the reinforcement patterns, power-law index, nonlocal parameter, length scale parameter, thickness and aspect ratios, elastic foundation, thermal environments, and various boundary conditions on stresses, displacements, buckling loads and frequencies of the CNTRC laminated nanoplate.

• 분석과학
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• 제19권6호
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• pp.519-528
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• 2006

본 연구에서는 뇨시료를 고체상 추출법으로 추출한 후 HPLC/DAD/ESI-MS(high-performance liquid chromatograph/diode array detector/electro-spray ionitation mass spectrometry)를 사용하여 분석하였다. 7종의 thyroid hormones의 HPLC 분리조건은 Hypersil ODS(octadecylsilica) 컬럼(4.6mm I.D., 100 mm length, particle size $5{\mu}m$)을 사용하고 ammonium formate buffer와 acetonitrile을 이동상으로 하여 기울기 용리한 결과 완전 분리가 가능하였으며, UV spectra 및 질량스펙트럼을 확인할 수 있었다. 고체상 추출법에 의한 전처리 최적 조건을 조사한 결과 시료를 pH 3으로 한 후 C18 고체상을 사용하여 4 mL의 methanol/ammonium hydroxide(9:1) 혼합용액으로 용리할 경우 회수율이 89.0-113.1%로 나타났다. HPLC/DAD를 이용하여 10-1000 ng/mL범위에서 검량선을 작성한 결과 $r^2$값은 0.992-0.998 으로 나타났으며 검출한계는 2-4 ng/mL(3.8-13.0 pmol/mL)로 계산되었다.

• 대한건축학회논문집:구조계
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• 제35권9호
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• pp.159-169
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• 2019

This work presents the three-dimensional extended strain smoothing approach in the framework of finite element method, so-called smoothed finite element method (S-FEM) for quasi-incompressible hyperelastic materials undergoing the large deformations. The proposed method is known that the incompressible limits, such as over-estimation of stiffness and distorted mesh sensitivity, can be overcome in two dimensions. Therefore, in this paper, the idea of Cell-based, Edge-based and Node-based strain smoothing approaches is extended to three-dimensions. The construction of subcells and smoothing domains for each methods are explained. The smoothed strain-displacement matrix and the stiffness matrix are obtained on each smoothing domain in the same manner with two-dimensional S-FEM. Various numerical tests are studied to demonstrate the validity and accuracy of 3D-S-FEM. The obtained results are compared with analytical solutions to express the efficacy of the methods.

• Advances in concrete construction
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• 제7권3호
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• pp.151-166
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• 2019

This paper introduces a new efficient analytical method, based on shear deformations obtained with 2D elasticity theory approach, to perform an explicit closed-form solution for calculation the interfacial shear and normal stresses in plated RC beam. The materials of plate, necessary for the reinforcement of the beam, are in general made with fiber reinforced polymers (Carbon or Glass) or steel. The experimental tests showed that at the ends of the plate, high shear and normal stresses are developed, consequently a debonding phenomenon at this position produce a sudden failure of the soffit plate. The interfacial stresses play a significant role in understanding this premature debonding failure of such repaired structures. In order to efficiently model the calculation of the interfacial stresses we have integrated the effect of shear deformations using the equilibrium equations of the elasticity. The approach of this method includes stress-strain and strain-displacement relationships for the adhesive and adherends. The use of the stresses continuity conditions at interfaces between the adhesive and adherents, results pair of second-order and fourth-order coupled ordinary differential equations. The analytical solution for this coupled differential equations give new explicit closed-form solution including shear deformations effects. This new solution is indented for applications of all plated beam. Finally, numerical results obtained with this method are in agreement of the existing solutions and the experimental results.

• 한국공간구조학회논문집
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• 제1권1호
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• pp.157-166
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• 2001

In general, the cutting pattern of the membrane structures is determined by dividing the complicated curved 3-D surface into several 2-D plane strip by using flattening technique. In this procedure, however, some discrepancies ore occurred between actual stresses of equilibrated state and designed uniform stresses because the material properties are not considered. These deviations can cause the critical structural problems, wrinkling or overstress, and thus a optimization process should be considered. In this paper, a new analytical method for determining an optimum cutting pattern considering material properties is presented. Here, iterative procedure is introduced to decrease the errors caused in numerical process. The optimization method proposed can diminish the deviations occurred by material properties and numerical errors, simultaneously. As a results, it is shown that the final stress distributions for the HP shell model are sufficiently near to design stress distributions, and it can be concluded that this method can be used to obtain the optimized cutting pattern of membrane structures.

• 대한전기학회논문지:시스템및제어부문D
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• 제49권3호
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• pp.95-101
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• 2000

In this paper, an improved method for magnetic inspection to detect surface of a conductor is presented. The presented method is based on the technique of ECP(Electric Current Perturbation), which is to measure the variation of current flow due to defects with a magnetic sensor. The inspection performance is improved by using high frequency current behaviors in order to concentrate the current near the defect and employing the resonant frequency of a search coil as an operating frequency. By analytical results and experiments of the test specimens, the feasibility of the inspection method is shown.

• 한국복합재료학회:학술대회논문집
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• 한국복합재료학회 2001년도 춘계학술발표대회 논문집
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• pp.38-41
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• 2001

A new 2-D braided textile metal matrix composite was developed and characterized. The constituent materials consist of PAN type carbon fiber as reinforcements and pure aluminum as matrices. The braided preforms of different braider yarn angles were fabricated. For a fixed bundle size of 12K, three braider yarn angles was selected: $30^{\circ}$, $45^{\circ}$, and $60^{\circ}$. The braided preforms were infiltrated with pure Al by vacuum assisted squeeze casting. Through the investigation of melt pressing methods and the effects of process parameters such as applied pressure, and pouring temperature, the optimal process conditions were identified as follows: applied pressure of 60MPa, pouring temperature of $800^{\circ}C$. Using the measured geometric parameters, 3-D engineering constants of metal matrix composites have been determined from the elastic model, which utilizes the coordinate transformation and the averaging of stiffened and compliance constants based upon the volume of each reinforcement and matrix material.

• Structural Engineering and Mechanics
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• 제85권5호
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• pp.593-605
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• 2023

This work presents a comparison between analytical and finite element analysis for bending of porous sandwich functionally graded material (FGM) plates. The plate is rectangular and simply supported under static sinusoidal loading. Material properties of FGM are assumed to vary continuously across the face sheets thickness according to a power-law function in terms of the volume fractions of the constituents while the core is homogeneous. Four types of porosity are considered. A refined higher-order shear with normal deformation theory is used. The number of unknowns in this theory is five, as against six or more in other shear and normal deformation theories. This theory assumes the nonlinear variation of transverse shear stresses and satisfies its nullity in the top and bottom surfaces of the plate without the use of a shear correction factor. The governing equations of equilibrium are derived from the virtual work principle. The Navier approach is used to solve equilibrium equations. The constitutive law of the porous FGM sandwich plate is implemented for a 3D finite element through a subroutine in FORTRAN (UMAT) in Abaqus software. Results show good agreement between the finite element model and the analytical method for some results, but the analytical method keeps giving symmetric results even with the thickness stretching effect and load applied to the top surface of the sandwich.