• Title/Summary/Keyword: 2중 파장법

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A Study on Projective Calibration for Arbitrary Display Surface using Digital Moire Method. (Digital Moire를 이용한 임의의 영사면에 대한 투영보정에 관한 연구)

  • 유원재;김도훈;강영준;백성훈
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2003.06a
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    • pp.292-295
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    • 2003
  • Moire topography method is a well-known non-contacting 3-D measurement method. the automatic 3-D measurement by moire topography has been required since the method was frequently applied to the engineering and medical fields. 3-D measurement using digital projection moire topography is very attractive because of its high measuring speed and high sensitivity. In this study, digital two-wavelength phase shilling moire is applied to the entertainment fields. recently. as promoting the growth of the VR-Game, display devices which attract public attention such as HMD or Projector are being appeared in order to deliver effectively the absorption sense. this study realized the Auto-calibrating system for arbitrary display surface using digital moire method which satisfied the shape measurement of display surface and the request of FOV(Field of View) output. also when large screen wasn't prepared, this auto-calibrating system was applied to enjoy games or movies at home with a projector and walls

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Simultaneous Determination and Mornitoring of Aflatoxin and Ochratoxin A in Food (식품 중 아플라톡신과 오크라톡신 A의 동시분석법 개발 및 모니터링)

  • Park, Ji-Won;Yoo, Myung-Sang;Kuk, Ju-Hee;Ji, Young-Ae;Lee, Jin-Ha
    • Journal of Food Hygiene and Safety
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    • v.28 no.1
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    • pp.75-82
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    • 2013
  • The simultaneous analysis and monitoring of aflatoxin $B_1$, $G_1$, $B_2$, $G_2$ and ochratoxin A in foods were carried out by HPLC with fluorescence detection. The samples were extracted with methanol/water mixture. The extract was centrifuged, diluted with phosphate buffer saline (PBS), filtered, and applied to an immunoaffinity column containing antibodies specific to both aflatoxins and ochratoxin A. After washing the column with PBS and water, the toxins were eluted from the column with methanol, and quantified by HPLC, with a run time of approximately 30 min. The recoveries for aflatoxin $B_1$, $G_1$, $B_2$, $G_2$ and ochratoxin A in foods were 78.4~101.5%, 73.3~102.1%, 81.7~106.7%, 67.0~104.6% and 78.7~120.8%, respectively. The limits of detection of aflatoxins and ochratoxin A ranged from 0.05 to $0.18{\mu}g/kg$. According to monitoring result with the established method, aflatoxin $B_1$ and ochratoxin A were found in 13 of 151 domestic commercial foods. The contamination levels were $0.32{\sim}1.80{\mu}g/kg$ for aflatoxin $B_1$ and $0.97{\mu}g/kg$ for ochratoxin A. Therefore, this study showed all commercial foods monitored were safe under the Korean standards for aflatoxins and ochratoxin A.

Development of Analytical Method of Organophosphates in Sea water by Finger Printing Fluorescence Spectroscopy (형광분석을 이용한 지문방식의 해수중 유기인의 분석 방법)

  • PARK Mi-Ok
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.30 no.3
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    • pp.377-387
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    • 1997
  • Primary fluorescence characteristics of ten standard solutions of organophosphates, sea water, and water from agricultural land were investigated by fluorescence contour. All the standard solutions of organophosphates has shown characteristics countours. Their emission maxima were shown between 296 nm and 437 nm. According to their numbers of emission maxima on the fluorescence contours, the organophosphates can be categorized in two different groups. Ateric and Diazinon are the first group with two emission maxima. DDVP with other seven standard organophosphates belong to the second group. The second group has two subgroups. One is characterized by the similar emission and excitation maxima, which are 310 nm and 280 nm, respectively. Those are DDVP, Hinosan, Kitazin, Locsion, Meta. The other sub-group shows quite different emission and excitation maxima from the first sub-group. They are Monopho, Thaconyl and Gropho and their emisson maxima were in far longer (437 nm) or shorter wavelength (296 nm). From agricutural samples, one of the investigated organophosphates was detetected by its characteristic retention time $(t_r=12min)$. HPIC-fluorescence data gave an additional parameter for differentiation between two organophosphates which has similar excitation and emission maxima.

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Use of Spectrophotometry for Quantitative Determination of Soil Clay Content (분광광도계를 이용한 점토함량 분석)

  • Park, Soon-Nam;Kim, Kye-Hoon;Kang, Ji-Young
    • Applied Biological Chemistry
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    • v.48 no.2
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    • pp.183-188
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    • 2005
  • This study was conducted to develop a method for the quantitative determination of soil clay content by spectophotometry. The optimum wavelength obtained with reference clay minerals for spectrophotometry was 500 nm. For the proposed spectrophotometry, 0.5 g of soil sample was put in the 250 ml Erlenmeyer flask and 100 ml dispersing agent was added. After shaking the flask at 130 rpm with a mechanical shaker overnight, the flask was removed from the shaker and was shaken up-and-down for 30 seconds. With a micro-pipet, 4 ml of the suspension was transferred into the previously-inserted cell and the absorbance was measured instantly. Results by the spectrophotometry for clay content analysis were compared with those by the conventional sedimentation technique (the pipet method). The proposed equation was $y\;=\;38.03x_1-0.17x_2-1.17$, where y, $x_1$, and $x_2$ were clay content (%) by the pipet method, water content corrected clay content (%) by spectrophotometry, and organic matter content ($g{\cdot}kg^{-1}$), respectively. The regression coefficient for the equation was $r\;=\;0.984^{**}$, indicating highly significant correlation between the results of the two methods.

Chemical Bath Deposition법에 의해 제조된 CdS 박막의 특성

  • Gong, Seon-Mi;So, U-Bin;Kim, Eun-Ho;Jeong, Ji-Won
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.02a
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    • pp.294-294
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    • 2010
  • CdS는 $CuInSe_2$계, CdTe계 이종접합 태양전지의 junction partner로 많이 이용되어 왔다. CdS는 전극으로 쓰일 뿐만 아니라 빛을 투과시키는 창문층으로 사용되어 높은 변환 효율을 나타낸다. 이종접합 태양전지에서 창문층은 가시광 영역에서 광투과율이 높고, 전기적으로 비저항이 낮아야 에너지 손실 없이 태양광을 광흡수층까지 투과시킬 수 있다. CdS 박막은 CBD법(solution growth technique), 진공증착법(vacuum evaporation), 스퍼터법(sputtering), 스프레이 열분해법(spray pyrolysis), 전착법(electrodeposition)에 의해 제조되고, 그 중 용액성장법(solution growth technique)이라고도 불리는 CBD법(chemical bath deposition)을 이용하여 CdS 박막을 제조하였다. CBD법은 다른 방법에 비해 제조 과정이 비교적 간단할 뿐만 아니라 제조 단가가 저렴하고, 넓은 면적의 박막 제조가 가능하며 재현성도 우수하다는 장점이 있다. CdS 박막을 제조하기 위한 cadmuim 이온공급원으로는 $CdSO_4$를 사용하였고 sulfur 이온공급원으로는 $SC(NH_2)_2$를 사용하였다. CBD법에서 박막의 물성에 영향을 미칠 수 있는 요인인 sulfur 이온공급원과 cadmium 이온공급원의 비, 용액의 온도, pH를 변화시켜 CdS 박막을 제조하였다. 각각의 조건에 의해 제조된 CdS의 박막의 두께는 Tencor P-1을 이용하여 측정되었고, UV-Visible spectrometer를 이용하여 파장에 따른 광투과율을 측정하였다. CdS 박막의 결정 구조를 조사하기 위해 X선 회절분석(XRD ; X-ray diffraction)을 하였고, AFM(Atomic Force Microscope)으로 표면 특성을 관찰하였다.

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Double-pass Second Harmonics Generation of Tunable CW Infrared Laser Beam of DOFA System in Periodically Poled LiNbO3 (PPLN 비선형 결정과 이중통과법을 이용한 DOFA 시스템에서 증폭된 연속발진형 파장가변 적외선 레이저광의 제 2고조파 발생)

  • Yoo, Kil-Sang;Jo, Jae-Heung;Ko, Kwang-Hoon;Lim, Gwon;Jeong, Do-Young
    • Korean Journal of Optics and Photonics
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    • v.19 no.3
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    • pp.229-236
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    • 2008
  • The optimum conditions of second harmonic generation (SHG) can be successfully achieved experimentally using single pass and double pass methods of a pumping beam. The beam has a power of several Watts radiated by a DOFA (Diode Laser Oscillator & Fiber Amplifier) system, which is a high power CW wavelength tunable infrared laser system, in a PPLN (Periodically Poled MgO doped Lithium Niobate) nonlinear crystal. In the case of a single pass method, the parameters are the wavelength of 535 nm for SHG and the output power of 245 mW generated from the pumping input beam with wavelength of 1070 nm and the power of 2.45 W at phase matching temperature of $108.9^{\circ}C$. The conversion efficiency of SHG was 10%. In order to enhance the output of SHG, the double pass method of the SHG system of a PPLN using a concave mirror for the retroreflection and a pair of wedged flat windows for phase compensation was also presented. In this double pass system, we obtained the SHG output beam with the wavelength of 535 nm and the maximum power of 383 mW at optimum phase matching temperature of $108.5^{\circ}C$ by using an incident pumping beam with wavelength of 1070 nm and the power of 2.45 W. The maximum conversion efficiency is 15.6%, which is more than that of the single pass method.

Establishment of Analytical Method for Carpropamid in Agricultural Commodities using HPLC-DAD/MS (HPLC-DAD/MS를 이용한 농산물 중 살균제 Carpropamid의 정밀 잔류분석법 확립)

  • Lee, Hyeri;Choi, Hoon;Kim, Eunhye;Lee, Young Deuk;Kim, Jeong-Han
    • The Korean Journal of Pesticide Science
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    • v.19 no.3
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    • pp.185-194
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    • 2015
  • This study was performed to establish a single residue analytical method for determining fungicide carpropamid residues in various agricultural commodities. Korean cabbage, apple, brown rice and green pepper were selected as representative crops. Samples were homogenized, extracted with acetone and purified by liquid-liquid partition and Florisil column chromatography. Carpropamid residues were analyzed at 220 nm with reversed phase HPLC equipped octylsilyl and octadecylsilyl column and confirmed using mass spectrometry. ILOQ (Instrumental limit of quantitation) of carpropamid was 2 ng and MLOQ (Method LOQ) was 0.02 mg/kg. Mean recoveries from four kinds of crop samples fortified at three levels (MLOQ, 10LOQ, 100LOQ) in triplicate were in the range of 84~112%. Relative standard deviations of the analytical method were all less than 10%, irrespective of crop types.

Development of technique to detect weeds in paddy field using spectrophotometric analysis (분광특성 분석에 의한 논 잡초 검출법 개발)

  • 서규현;서상룡;성제훈
    • Proceedings of the Korean Society for Agricultural Machinery Conference
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    • 2002.02a
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    • pp.438-443
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    • 2002
  • 본 연구는 수도작에서 토양과 식물체의 분광반사특성과 영상처리를 이용한 기계시각 잡초검출 센서를 개발하기 위한 기초연구로서 분류하고자 하는 대상체들의 분광반사율을 조사하여 주요한 파장을 선정하고 선정된 파장을 이용한 판별분석을 통해 각 대상체에 대한 분류 정확도를 중심으로 잡초검출 가능성을 조사하기 위하여 수행하였으며, 실험으로부터 얻은 결론은 다음과 같다. 1. 토양과 식물체를 구분하는데 효과적인 파장은 마른 토양의 경우 680 nm, 배수 토양에 있어서는 810 nm로 선정하였고, 토양을 배제한 후 벼와 잡초를 구분하기에 효과적인 파장은 580, 680 nm로 선정하였다. 2. 토양과 식물체를 구분하기 위한 판별분석 결과 2가지 토양상태 모두 식물체와 완전히 구분 가능한 것으로 나타났다. 벼와 잡초를 구분하기 위한 실험에서, 벼는 98%의 분류정확도로 구분이 가능하였고, 잡초는 83%의 분류정확도로 구분이 되는 것으로 나타났다. 따라서 차후 분광학적 원리를 이용한 센서를 제작할 때 본 연구에서 선택한 주요 파장과 판별함수를 이용하여 장치를 구성하고 알고리즘을 제작한다면 벼, 잡초, 토양을 효과적으로 구분이 가능할 것으로 판단되었다. 3. 컬러 CCD 카메라를 사용하는 경우에 있어 식물체와 토양을 구분하기 위해 3 종의 파장 중 630 nm 파장만의 이용을 고려하여 그 분류성능을 분석한 결과, 식물체와 토양은 소수의 관측치를 제외하고 완전히 구분이 가능했고, 벼와 잡초를 구분한 결과에서는 비교적 높은 분류능력을 가진 것으로 나타나 차후 컬러 CCD 카메라를 이용하여 장치를 구성하는데 좋은 기초가 될 것으로 판단된다. 배양체의 접종작업은 모든 배양실이 인력에 의존하였으며, 배양체를 배지와 분리하여 불필요한 부분을 제거하고 배양작물에 따라 생육정도를 2~3등급으로 구분하여 배양용기의 배지 위에 치상하는 과정으로 수행되었으며, 작업능률은 호접란의 경우 배양병에 25본을 접종하는데 시간당 6병, 심비디움은 원형 플라스크에 25본을 접종하는데 시간당 10병 정도였다. 바. 식물체의 대량증식에 사용되는 플라스크, 배양병, PE용기 등 배양용기의 세척작업은 농원의 1개배양실에서 간이식 세척기, 이 외의 9개배양실은 모두 물에 담겨 두었다가 세제와 브러쉬 등을 사용하여 인력으로 세척하고 있어 생력화 기술개발이 요구되었다.도가 빠를수록 건조속도가 빨라졌으며, 건조에너지도 1,334kcal/kg.water로 비슷하게 소요되었다. 마. 시험구와 대비구의 건감률은 시험구에서 1.08~1.36w.b./h로 나타나 대비구보다 약 9.9~18.3%가 높게 나타났고, 건조에너지는 10.2~14.6%가 절감되었다. 발아율은 열풍온도가 낮을수록 높게 나타났고 시험구가 대비구보다 발아율이 낮게 나타났으며, 동할률 증가량도 원적외선.열풍 복합건조방법이 높게 나타나 이것은 곡물 표면에 원적외선 방사에의한 복사열이 전달되어 열장해를 받았기 때문으로 판단되며, 금후 더 연구하여 적정 열풍온도 및 방사체 크기를 구명해야 할 것이다.으로 보여진다 따라서 옻나무 유래 F는 포유동물의 생식기능에 중요하게 작용하는 것으로 사료된다.된다.정량 분석한 결과이다. 시편의 조성은 33.6 at% U, 66.4 at% O의 결과를 얻었다. 산화물 핵연료의 표면 관찰 및 정량 분석 시험시 시편 표면을

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Investigation of Absorption Cross-Section Effects on the Formaldehyde Column Density Retrieval from Direct Sun Measurement (태양 직달광 관측 자료로부터 포름알데히드 연직 농도 산출 시 흡수단면적이 미치는 영향 연구)

  • Gyeong Park;Jeonghyeon Park;Hanlim Lee
    • Korean Journal of Remote Sensing
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    • v.39 no.5_1
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    • pp.551-561
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    • 2023
  • In this study, we investigated the effects of the spectral fitting window and absorption cross-section on the retrieval of the formaldehyde (HCHO) slant column density (SCD) from the direct-sun measurement of pandora spectrometer system using differential optical absorption spectroscopy (DOAS). Pandora Level 1 data observed at Yonsei University in Seoul from October 12 to 31, 2022 were used. The HCHO column density was retrieved under eight ranges including the spectral fitting window used in the Second Cabauw Intercomparison campaign for Nitrogen Dioxide measuring Instruments (CINDI-2) and seven types of absorption cross-section composition. The spectral fitting window was selected from 336.5 to 359.0 nm with minimum residual and HCHO SCD error. When the nitrogen dioxide (NO2) absorption cross-section at 220 K was added to the cross-section composition used in the CINDI-2 campaign among seven types, the residual and HCHO SCD error were the smallest and the HCHO column density wasstably retrieved. The average HCHO SCD with the highest retrieval accuracy and the values retrieved under other conditions differed from a minimum of 4% to a maximum of 40%.

Determination of Cr(Ⅲ) Iron by Chemiluminescence Method (화학발광법을 이용한 Cr(Ⅲ)이온의 정량)

  • Lee, Sang Hak;Ju, Ik Su
    • Journal of the Korean Chemical Society
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    • v.46 no.2
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    • pp.145-150
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    • 2002
  • A Method to determine Cr(III)ion in aqueous solution by chemiluminescence method using a stopped flow system has been studied. The method is based on the increased chemiluminescence intensity with the addition of Cr(III) to a solution of lucigenin a nd hyrogen peroxide. The effects of pH, injection volumes of reagent and sample, and concentration of lucigenin and hyrogen peroxide on the chemiluminescence intensity have been investigated. The calibration curve for Cr(III) ion was linear over the range from 1.0${\times}$$10^{-6}$ to 1.0${\times}$$10^{-3}$M and the detection limit was 5.2${\times}$$10^{-8}$M under the optimal experimental condition of 437nm, 12.8,and 1.0${\times}$$10^{-6}$ and 2.0M for emission wavelength, pH, and concentration of lucigenin and hyrogen peroxide, respectively.