• Title/Summary/Keyword: 2단계 접착제

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Effect of Er:YAG lasing on the dentin bonding strength of two-step adhesives (2단계 접착제의 상아질 결합강도에 대한 Er:YAG 레이저 조사 영향)

  • Song, Byeong-Choon;Cho, Young-Gon;Lee, Myung-Seon
    • Restorative Dentistry and Endodontics
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    • v.36 no.5
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    • pp.409-418
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    • 2011
  • Objectives: The purpose of this study was to compare the microshear bond strength (${\mu}$SBS) and bonding interfaces of two-step total-etching and self-etching adhesive systems to three etch types of dentin either the acid etched, laser etched or laser and acid etched. Materials and Methods: The occlusal dentinal surfaces of thirty human molars were used. They were divided into six groups: group 1, 37% $H_3PO_4$ + Single Bond 2 (3M ESPE); group 2, Er:YAG laser (KEY Laser 3, KaVo) + Single Bond 2; group 3, Er:YAG laser + 37% $H_3PO_4$ + Single Bond 2; group 4, Clearfil SE Primer + Bond (Kuraray); group 5, Er:YAG laser + Clearfil SE Bond; group 6, Er:YAG laser + Clearfil SE Primer + Bond. The samples were subjected to ${\mu}$SBS testing 24 hr after bonding. Also scanning microscopic evaluations were made on the resin-dentin interfaces of six specimens. Results: The ${\mu}$SBS of group 2 was significantly lower than that of groups 1 and 3 in Single Bond 2 (p < 0.05). There were significant differences among the uSBS of groups 4, 5, and 6 in Clearfil SE Bond (p < 0.05). Very short and slender resin tags were observed in groups 2 and 5. Long and slender resin tags and lateral branches of tags were observed in groups 3 and 6. Conclusions: Treatment of dentin surface using phosphoric acid or self-etching primer improved the adhesion of Er:YAG lased dentin.

Automotive Pre-primed Coatings with Automotive Structural Adhesive for Non-weldable Binding Process (자동차 구조용 접착제를 이용한 자동차용 Pre-primed 도료의 비용접식 접합공정 적용)

  • Moon, Je-Ik;Lee, Yong-Hee;Kim, Hyun-Joong;Noh, Seung Man;Nam, Joon Hyun;Kim, Min-Su;Kim, Jun-Ki;Kim, Jong-Hoon
    • Journal of Adhesion and Interface
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    • v.12 no.3
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    • pp.99-104
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    • 2011
  • Currently, automotive pre-primed coatings has been developed to overcome environmental regulations and to reduce manufacturing cost in automotive industry. By these reasons, an automotive pre-primed system has been investigated to remove the wash and pre-treatment process using a roll coating application. It is required to develop non-weldable pre-primed system for automotive structural adhesives, because pre-primed sheet coated with organic compounds is hard to be assembled by welding process. Primer 1 (polyester type) and primer 2 (urethane type) were designed to satisfy flexibility and formability for non-weldable pre-primed system. According to the results of physical property test of the primers, adhesion test such as single-lap shear test and T-peel test, primer 1 (polyester type) had better physical properties such as pencil hardness, solvent resistance, flexibility and adhesion with automotive adhesive than that of primer 2 (polyurethane type). In addition, the possibility of the non-weldable pre-primed system was applicable to automotive assembly process in place of welding process.

Improvement of existing drainage system for leakage treatment in exiting underground structures (운영중인 지하구조물의 누수처리를 위한 유도배수공법의 개선)

  • Kim, Dong-Gyou;Yim, Min-Jin
    • Journal of Korean Tunnelling and Underground Space Association
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    • v.19 no.4
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    • pp.669-683
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    • 2017
  • The objective of this study is to propose a modification of the previously proposed drainage system for catching the partial leakage of underground concrete structures. Two techniques were proposed for applying the drainage system only to the leaking parts. One was for conveying leaking groundwater to the collection point in the drainage system and the other was for conveying the collected groundwater to the primary drainage system of the underground concrete structure. Four waterproofing materials for conveying leaking groundwater to the catchment point of the drainage system, Durkflex made of porous rubber material, KE-45 silicone adhesive with super strong adhesion, Hotty-gel made of polymeric materials and general silicone adhesive were evaluated for waterproofing performance. Hotty-gel only showed perfect waterproof performance and the other three waterproof materials leaked. The modified drainage system with Hotty-gel and drainage pipe with fixed saddle to convey the leaking groundwater from the catchment point to the primary drainage system were tested on the concrete retaining wall. The waterproof performance and the drainage performance were evaluated by injecting 1,000 ml of water in the back of the modified drainage system at the 7-day, 14-day, 21-day, 28-day, 2-month and 3-month. There was no problem in waterproof performance and drainage performance of the modified drainage system during 3 months. In order to evaluate the construction period and construction cost of the modified drainage system, it was compared with the existing leaching repair method in surface cleaning stage, leakage treatment stage, and protective barrier stage. Total construction period and construction cost were compared in considering the contents of work, repair material, construction equipment, working time, and total number of workers. As a result of comparing and analyzing in each construction stage, it was concluded that the modified drainage system could save construction period and construction cost compared to the existing leaching repair method.

Mixed Mode Analysis using Two-step Extension Based VCCT in an Inclined Center Crack Repaired by Composite Patching (복합재료 팻칭에 의한 중앙경사균열에서 2단계 확장 가상균열닫힘법을 사용한 혼합모우드해석)

  • Ahn, Jae-Seok;Woo, Kwang-Sung
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.32 no.1A
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    • pp.11-18
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    • 2012
  • This paper deals with the numerical determination of the stress intensity factors of cracked aluminum plates under the mixed mode of $K_I$ and $K_{II}$ in glass-epoxy fiber reinforced composites. For the stress intensity factors, two different models are reviewed such as VCCT and two-step extension method. The p-convergent partial layerwise model is adopted to determine the fracture parameters in terms of energy release rates and stress intensity factors. The p-convergent approach is based on the concept of subparametric element. In assumed displacement field, strain-displacement relations and 3-D constitutive equations of a layer are obtained by combination of 2-D and 1-D higher-order shape functions. In the elements, Lobatto shape functions and Gauss-Lobatto technique are employed to interpolate displacement fields and to implement numerical quadrature. Using the models and techniques considered, effects of composite laminate configuration according to inclined angles and adhesive properties on the performance of bonded composite patch are investigated. In addition to these, the out-of-plane bending effect has been investigated across the thickness of patch repaired laminate plates due to the change of neutral axis. The present model provides accuracy and simplicity in terms of stress intensity factors, stress distribution, number of degrees of freedom, and energy release rates as compared with previous works in literatures.

A Study on the Process Conditions of ACA( Anisotropic Conductance Adhesives) for COG ( Chip On Glass) (COG(Chip On Glass)를 위한 ACA (Anisotropic Conductive Adhesives) 공정 조건에 관한 연구)

  • Han, Jeong-In
    • Korean Journal of Materials Research
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    • v.5 no.8
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    • pp.929-935
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    • 1995
  • In order to develop COG (Chip On Glass) technology for LCD module interconnecting the driver IC to Al pad electrode on the glass substrate, Anisotropic Conductive Adhesive(ACA) process, the most promising one among COG technologies, was investigated. ACA process was carried out by two steps, dispensing of ACA resin in the bonding area and curing by W radiation. Load on the chip was ranged from 2.0 to 15kg and the chip was heated at about 12$0^{\circ}C$. In resin, the density of conductive particles coated with Au or Ni at the surface were 500, 1000, 2000 and 4000 particles/$\textrm{mm}^2$, and the diameter of particles were 5, 7 and 12${\mu}{\textrm}{m}$. As a result of the experiments, ACA process using ACA particle of diameter and density of 5${\mu}{\textrm}{m}$ and 4000 particles/$\textrm{mm}^2$ respectively shows optimum characteristic with the stabilzed bonding properties and contact resistance.

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The Study and Conservation of Woven Cigarette Inserts (담배 사은품 실크 인서트(Silk Inserts)에 관한 연구와 보존처리)

  • Lee, Young-Joo
    • Journal of the Korean Society of Clothing and Textiles
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    • v.30 no.3 s.151
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    • pp.447-457
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    • 2006
  • The purpose of this study is to document and preserve an unidentified textile purchased at a flea market. This study object is important because it is one of the very rare silk insert series from 1930s which were created for commercial use(as inclusion in cigarette packages). The investigation was conducted by researching the limited publications that discuss silk inserts, visiting many sites on the internet that offer such inserts for sale or catering to the collectors of these silk inserts, and especially visiting the collection of silk inserts, named the J.R. Burdick Collection, at the Metropolitan Museum of Art, New York. Several pieces matched the patches used in the study piece. But Buidick's description on time frame(1912-1915) did not indicate the full range of production of silk inserts. After the identification of object, the conservation treatment was carefully done using adhesives. The results of this study can be summarized as follows; 1. The silk inserts of the study object were included as promotions by some company owned by the American Tobacco Company, probably at some time between 1934 and 1939. 2. The initial stage in the conservation treatment was mechanical surface cleaning using a vacuum cleaner. After vacuuming, humidification was conducted to reduce creases in the top of the object. The damaged areas were backed with stabiltax coated with a solution of Elvace 45675 since the fiber of this object was too deteriorated. 3. Adhesive treatments using Elvace showed satisfactory results: flexibility, strength, no damaging effects on the study object, removability without damaging the object.

MARGINAL MICROLEAKAGE OF SINGLE STEP ADHESIVES (단일 단계 접착제의 변연 미세누출)

  • Cho, Young-Gon;Jeong, Jin-Ho;Ki, Young-Jae;Choi, Hee-Young;Jin, Cheul-Hee;Yoo, Sang-Hoon;Kim, Jong-Uk;Park, Byung-Cheul
    • Restorative Dentistry and Endodontics
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    • v.29 no.2
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    • pp.162-169
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    • 2004
  • This study evaluated the marginal microleakage of five single step adhesives. Class V cavity preparations with occlusal margins in enamel and gingival margins in dentin were prepared on both buccal and lingual surfaces of extracted human molar teeth. Prepared teeth were randomly divided into five groups and restored using one of the single step adhesives and composite resins:Prompt L-Pop/Filtek Z-250 (Group 1), AQ Bond/Metafil CX (Group 2), One-Up Bond F/Palfique Toughwell (Group 3). Futurabond/Admira (Group 4), Xeno III/Spectrum TPH (Group 5). The restored teeth were thermocycled. Microleakage was assessed by dye penetration using 2% methylene blue dye solution. The teeth were bisected buccolingually and evaluated for microleakage under steromicroscope. The data were statistically analysed by Kruskal-Wallis test and Mann-Whitney tests. The results of this study were as follows:1. Microleakage of enamel margins in group 3 was statistically higher than that in groups 1, 2, 4, 5 (p < 0.05). 2. Microleakage of dentin margins in group 1 was statistically higher than that in groups 2, 5, and that in group 3 was statistically higher than that in groups 2, 4, 5 (p < 0.05). 3. Dentin marginal microleakage was higher than enamel marginal microleakage in all experimental groups. In conclusion, Prompt L-Pop showed the least leakage at enamel margin, and AQ Bond showed at dentin margin in this study. Marginal miroleakage in dentin was higher than that in enamel.

IS 지식에 대한 IS 실무자와 전공 교수 간의 인식 차이 분석

  • Lee, Hyeon-Woo;Lee, Hye-Jin;Go, Seok-Ha
    • Proceedings of the Korea Society of Information Technology Applications Conference
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    • 2007.05a
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    • pp.281-299
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    • 2007
  • IS/IT 분야 실무자가 지니고 있어야 한다고 생각되는 지식과 전문 기술들을 '지식/능력 영역'과 '소프트웨어 전문 기술 영역'으로 구분하여 각각 세부 항목을 명세하였다. 그리고 분류된 두 영역에 대하여 IS/IT 분야 실무자가 생각하는 필요한 지식 및 전문 기술들의 중요도와 IS/IT 전공 교수가 생각하는 IS/IT 실무자에게 필요한 지식 및 전문 기술들의 중요도를 조사하여 두 그룹간의 인식차 비교를 시도하였다. 조사지역은 실무자는 충청지역 및 수도권 지역에 분포하는 SI 업체를 대상으로 이루어 졌다. IS/IT 실무자를 대상으로 한 조사는 실무자 본인의 일장에서 IS/IT 실무자가 갖추어야 된다고 판단되는 지식 및 전문 기술들의 중요도를 측정하였다. 그와 더불어 그들이 수행하는 IS 활동에 대하여 투자한 시간을 기준으로 군집분석을 실시하여 세가지 그룹으로 구분하여 실무자 전체와 세 그룹간의 비교가 가능하도록 조차되었다. 비교 결과, 지식/능력 영역에서는 IS 실무자들이 상대적으로 '하드웨어에 대한 지식', '특정 조직', '운영체제에 대한 지식'에 대해 더 높은 중요도를 부여하고 있는 것으로 나타났다. 소프트웨어 전문 기술 영역에서는 실무자보다 전공교수가 생각하는 중요도가 보편적으로 더 높게 나타났다. 전공 교수는 '프리젠테이션 도구', '객체지향 언어(C++, Java 등)'에 4점 대의 높은 점수를 주어 중요한 것이 무엇인가 하는 인지가 있는 것으로 보이나 실무자 그룹에서는 특별히 중요시 여기는 항목이 명확히 드러나지 않고 보편적인 값이 median 값 주변에 위치하고 있다. 이는 현재 실무자들이 빠르게 변화하고 있는 IS/IT 환경에서 본인의 경력경로 (career path)을 위해 무엇이 중요한 갓인지 아직 명확히 하고 있지 못하는 것으로도 해석이 가능하다. 자세한 비교/분석 및 해석은 현재 진행 중이며, 여러 흥미로운 해석이 가능할 것으로 기대 된다.합형 파괴가 증가하는 경향을 나타내었다. 이상의 결과로, 상아질 접착제의 접착단계/과정이 결합내구성에 영향을 미침을 알 수 있었다. 따라서 접착과정의 단순화가 반드시 접착에 효과적이라고 할 수 없다.는 저작 운동 잔에는 2군에서 Heliomolar가 Pyramid보다 변연적합도가 우수하였고 (p < 0.05) 그 외의 군에서는 유의차가 없었으며, 저작 운동 후에는 모든 군에서 재료간 유의차가 없었다. 각 부위별 변연적합도를 비교하면, 저작 운동 전 Pyramid에서는 교합면 변연에서는 4군이 2군에 비해 높은 변연적합도를 보였고 (p < 0.05), 인접면과 치은면에서는 군 간 유의차를 보이지 않았다. Heliomolar에서는 교합면 변연에서 2, 4군이 1군에 비해 높은 변연적합도를 보였고 (p < 0.05), 인접면과 치은면에서는 군간 유의차를 보이지 않았다. 저작 운동 후 Pyramid에서는 교합면 변연에서는 3군이 1, 2군에 비해 높은 변연적합도를 보였고 (p < 0.05), 인접면과 치은면에서는 군간 유의차를 보이지 않았다. Heliomolar에서는 교합면에서 2, 3, 4군이 1군에 비해 변연적합도가 높았으며 (p < 0.05), 인접면과 치은면에서는 군간 유의차를 보이지 않았다 이번 연구를 통하여 복합레진을 간헐적 광중합시킴으로써 변연적합도가 향상될 수 있음을 알 수 있었다.시장에 비해 주가가 비교적 안정적인 수준을 유지해 왔다고 볼 수 있다.36.4%)와 외식을 선호(29.1%)${\lrcorner}$ 하기 때문에 패스트푸드를 이용하게 된 것으로 응답 하였으며, 남 여 대학생간에는 유의한 차이(p<0.05)가 인정되었다. 응답자의 체형은 ${\ulcorner}$적당하다${\lrcorner}$고 응답한 경우가 가장 많이 이러한 음식을 즐겨 먹었으며(49.5%), 그 다음은 뚱뚱한 경우도 비교적 많이 먹고

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Manufacture and Properties of White Charcoal Board in Relation with Final Mat Moisture Content and Charcoal Particle Size (백탄파티클 크기와 최종매트함수율에 따른 백탄보드의 제조와 성능)

  • Lee, Hwa Hyoung;Cho, Youn Mean;Park, Han Sang
    • Journal of the Korean Wood Science and Technology
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    • v.33 no.3 s.131
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    • pp.22-29
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    • 2005
  • This research was carried out not only to examine the proper manufacturing condition for white charcoal board in relation to charcoal particle size and final mat moisture content (FMC), but also to maintain the advantageous properties of white charcoal as a well being building material against the sick house problem. Excellent functional white charcoal board was produced with two groups of FMC 20~25% and FMC 36~60%. The latter showed best results among tested samples in two types which are #40-60type-P15%, M5%, FMC 60% and mixed type-P15%, M5%, FMC36% with non formaldehyde adhesives [MDI (M), poly vinyl acetate emulsion (P)] and three stage pressing cycle of 30-10-$30kgf/cm^2$ (1 min.-1.5 min.-6 min.). The former gave highly acceptable results in two types which are #6 over-M15%FMC25% and mixed type-M25%FMC20%. White charcoal board gave excellent in dimensional stability, gas adsorption and far-infrared emission.

ESTIMATION OF RELATION BETWEEN TECHNIQUES OF DYE PENETRATION FOR MICROLEA-KAGE AND SEM EVALUATION FOR MARGINAL ADAPTATION OF THE RESTORATION (수복물의 미세누출도와 변연적합도 측정에 사용되는 방법 사이의 상관 관계 평가)

  • Hwang, Soon-Joo;Shin, Dong-Hoon
    • Restorative Dentistry and Endodontics
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    • v.31 no.5
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    • pp.337-343
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    • 2006
  • The purpose of this study was to estimate the relation between techniques used for microleakage from dye penetration and for marginal adaptation from SEM evaluation of the restoration. Using high speed #330 bur class V cavities ($4{\times}3{\times}1.5 mm$ around CEJ) were prepared on the buccal surface of 20 extracted human molars. Six dimples as reference points for SEM and dye penetration evaluation were made with 1/2 round bur. Cavity was bulk filled with microhybrid composite resin (Esthet X) and all-in-one adhesive (Xeno III). Teeth were stored in saline solution for one day, after then, they were finished and polished using Sof-Lex system. Fifty percent silver nitrate dye solution was used for the evaluation of microleakage and resin replica was used for marginal adaptation. All of these were done after 1000 times thermocycling between 5 and $55^{\circ}C$. Vertical sections were made through three dimples of restoration to obtain samples for the evaluation of dye penetration and inner marginal adaptation. Outer adaptational estimation was done with an intact restoration before sectioning. Dye penetration was determined in three degrees and percentage of outer and inner leaky margin was estimated from SEM image The data were analysed statistically: Spearman's rho test were used to check relationships between two methods. The result were as follows : 1. There were significant relationships between degree of dye penetration and inner and outer marginal adaptations each (p < 0.01). 2. However, there was no significant relationship between the results or inner and outer marginal adaptation. Within the results of this study, relationship between the percentage of marginal adaptation and microleakage shows significant relationship. However, inner and outer marginal adaptation did not show any significant relationship mutually.