• Title/Summary/Keyword: 1,2-IND

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Post-treatment Enhancement of Ninhydrin-treated Fingermark Using 1,2-IND/Zn (1,2-IND/Zn를 이용한 ninhydrin으로 처리한 지문의 후속 증강 연구)

  • Park, Eun-Jee;Jung, Ha-Na;Hong, Sung-Wook
    • The Journal of the Korea Contents Association
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    • v.18 no.5
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    • pp.105-114
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    • 2018
  • Ninhydrin traditionally used to develop fingerprints on paper is often limited in its use depending on background color and its enhancement effect differs depending on reagent reaction condition. Recently 1,2-indanedione(1,2-IND), etc. which has no limitation of background color has been used to visualize the fingermark on paper. Therefore, this study was carried out for enhancement of fingerprints after 1,2-IND/Zn treatment on paper treated with ninhydrin. Comparison between 1,2-IND/Zn reaction after ninhydrin treatment and single ninhydrin reaction were conducted under various methods. Result shows the fingerprints were enhanced when ninhydrin-treated fingerprints were treated with 1,2-IND/Zn, and their enhancement was observed even after 6 months.

Enhancement of fingerprint in blood deposited on the surface of thermal paper by using the mixture of polyvinylpyrrolidone and 1,2-indanedione (Polyvinylpyrrolidone과 1,2-indanedione 혼합물을 이용한 감열지에 부착된 혈흔지문의 증강)

  • Kim, Dongman;Ryu, Heayeon;Jeong, Seunghoon;Joo, Inseon;Hong, Sungwook
    • Analytical Science and Technology
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    • v.34 no.3
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    • pp.122-127
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    • 2021
  • A mixture of polyvinylpyrrolidone and 1,2-indanedione (PVP-IND) is known to be the best reagent for developing latent fingerprints deposited on the surface of a thermal paper. However, no study has evaluated whether PVP-IND could enhance fingerprints in blood deposited on the surface of thermal paper. Therefore, in this study, the ability of PVP-IND to enhance the fingerprints in blood was investigated. Furthermore, aqueous amido black solution, which is known to be the best reagent for enhancing fingerprints in blood deposited on the surface of thermal paper, was used for comparison with PVP-IND. Therefore, while enhancing the fingerprints in diluted blood, PVP-IND enhanced the quality of fingerprints compared to aqueous amido black solution. The ridge diffused when the undiluted fingerprints in blood were enhanced with PVP-IND because PVP reacted with amino acids in blood; however, amido black solution yielded better results. When treated with PVP-IND, it is presumed that the ridge diffused due to the reaction of PVP and amino acids contained in the blood.

Development of latent footwear impression on porous surfaces using DL-alanine solution and 1,2-indanedione solution (DL-alanine과 1,2-indanedione을 이용한 종이에 남은 족적의 증강)

  • Hong, Sungwook;Kim, Euna;Park, Miseon;Lee, Eunhye
    • Analytical Science and Technology
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    • v.30 no.6
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    • pp.303-311
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    • 2017
  • A new method for obtaining the photoluminescence of footwear impression by using 1,2-indandione (1,2-IND) solution, which is a latent fingerprint-developing reagent, was studied. A binary complex of DL-alanine and 1,2-IND was prepared by spraying a DL-alanine solution and the 1,2-IND solution (an amino acid sensitive reagent) onto dry or wet origin footwear impression deposited on the surface of printed A4 paper. This binary complex reacts with the trace metal component in the footwear impression to form a ternary complex that exhibits photoluminescence. However, when 5-methylthioninhydrin (5-MTN) solution was used instead of 1,2-IND, no consistent photoluminescence was observed even under identical treatment conditions. In addition, when footwear impressions treated with DL-alanine and 1,2-IND solutions were stored under various temperature conditions (30, 40 and $50^{\circ}C$) and various humidity conditions (30 %, 40 %, 50 % and 60 % RH), the contrast between the footwear impression and the background decreased. Optimal footwear impression photoluminescence was obtained when the footwear impressions treated with DL-alanine and 1,2-IND solutions were stored at $30^{\circ}C$ and 30 % RH for 1 h. The sensitivity of the developed method was ccompared with the sensitivities of three known methods - black gelatin lifting, 2,2'-dipyridyl treatment, and 8-hydroxyquinoline treatment. The results showed that the sensitivity of the developed method was worse than that of the black gelatin lifting method but better than that of 2,2'-dipyridyl or 8-hydroxyquinoline treatment method.

Synthesis and Biological Evaluation of 4-Phenyl-1-(indoline-5-sulfonyl)-2-imidazolone Derivatives as Potential Antitumor Agents

  • Park, Dongrak;Lee, Jungah;Hyunsook Hwang;Lee, Dugkeun;Sungjune Yoon;Yongho Chung;Sanghun Jung;Lee, Moonsun
    • Proceedings of the Korean Society of Applied Pharmacology
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    • 1997.04a
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    • pp.73-73
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    • 1997
  • A series of 4-phenyl-1-(indoline-5-sulfonyl)-2-imidazolone derivatives has been synthesized starting from 2-bromoacetophenone. Reaction of 2-aminoacetophenone obtained from 2-bromoacetophenon by Delepin synthesis and potassium cyanate affords 1,3-dihydro-4-phenyl-2-imidazolone. This key intermediate was treated with sodium hydride and N-trifluoroacetyl-indoline-5-sulfonylchloride, and trifluoroacetyl group was deprotected to give 4-Phenyl-1-(indoline-5-sulfonyl)-2-imidazolone. Various substituents were introduced on the nitrogen of indoline. Antitumor activity of this series of compound was evaluated by MTT method. Nearly all of the compounds showed broad-spectrum activity.

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DW1350, a Newly Synthetic Anti-osteoporotic Agent: 2. Effect on Ovariectomized Osteoporosis Rat Model, a Histomorphometrical Aspect

  • Lee, Jin-Soo;Ku, Sae-Kwang;Jung, Da-Hee;Jin, Youn-Goo;Park, Jae-Hoon;Yang, Hee-Bok;Jung, Yong-Ho;Ryu, Jei-Man
    • Proceedings of the PSK Conference
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    • 2003.04a
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    • pp.155.1-155.1
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    • 2003
  • In the present study, the effect of DW-1350, a newly synthesized anti-osteoporotic agent, was evaluated in ovariectomized Rat. Female SD Rat mice underwent bilateral ovariectomy for prevention study that test article was administered from 2 days after ovariectomy for 6 weeks, for therapeutic study it was conducted from 6 weeks after ovariectomy for three months. (omitted)

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Abundances and Species Composition of Microzooplankton during Summer in Kwangyang Bay, Korea (여름철 광양만 소형동물플랑크톤의 출현량과 종조성)

  • CHA Seong-Sig;PARK Kwang-Jae
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.33 no.4
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    • pp.361-366
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    • 2000
  • To study the abundances and species composition of microzooplankton during summer, microzooplankton were sampled fortnightly from 22 May to 3 August in Kwangyang Bay, Korea, The dominant species were Tintinnopsis spp. and Coaonellopsis sp. of tintinnids, and eggs and nauplii of copepods, They occupied $83.8{\%}$ of the total microzooplankton. The abundance of microzooplankton on 22 May was $374.6 ind./l$. It increased to 1,276.0 ind./l and 1,234.9 ind./l in June, and then reduced to $528.2{\~}609.8 ind./l$ in July and August. The abundances and species composition of microzooplankton were affected by the predation of fish larvae.

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Characteristics of distribution and community structure of marcrobenthic Invertebrates caught in the coastal waters of middle East Sea, Korea (동해 중부해역 저서무척추동물의 분포특성 및 군집구조)

  • YOON, Byoung-Sun;CHOI, Young-Min;SOHN, Myong-Ho;KIM, Jong-Bin;YANG, Jae-Hyeong;PARK, Jeong-Ho
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.52 no.4
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    • pp.372-385
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    • 2016
  • This present study investigated characteristics of distribution and community structure of macrobenthic invertebrates through the survey of commercial Danish seine fisheries from 2011 to 2013. In this study, a total of 28 species were sampled with a mean density of $32,568ind./km^2$ and mean biomass of $1,649.5kg/km^2$. The dominant species, comprising over 1.0% of the total number of individuals, were Chionoecetes opilio ($11,203ind./km^2$, 34.4%), Pandalus eous ($9,247ind./km^2$, 28.4%), Ophiuridae spp. ($5,750ind./km^2$, 17.7%), Argis lar ($2,631ind./km^2$, 8.1%), Neocrangon communis ($994ind./km^2$, 3.1%), Berryteuthis magister ($612ind./km^2$, 1.9%), Sepiola birostrata ($499ind./km^2$, 1.5%) and Strongylocentrotidae sp. ($424ind./km^2$, 1.3%). The dominant species, in terms of biomass, comprising over 1.0% of the total biomass, were C. opilio ($1,167.2kg/km^2$, 70.8%), B. magister ($130.3kg/km^2$, 7.9%), P. eous ($102.4kg/km^2$, 6.2%), Ophiuridae spp. ($84.6kg/km^2$, 5.1%), Enteroctopus dofleini ($45.5kg/km^2$, 2.8%), A. lar ($35.7kg/km^2$, 2.2%), Strongylocentrotidae sp. ($25.0kg/km^2$, 1.5%) and S. birostrata ($22.1kg/km^2$, 1.3%). Among them, S. birostrata, E. dofleini, Strongylocentrotidae sp. and Ophiuridae spp. were higher abundance and biomass in the shallow water (<200 meters in depth), whereas C. opilio, P. eous, A. lar, N. communis and B. magister were higher in the deep water (301 ~ 500 meters in depth). As the results of cluster analysis and non-metric multidimensional scaling (nMDS) analysis based on the Bray-Curtis similarity of fourth root transformed data for number of species and individuals, the macrobenthic invertebrates community by Danish seine survey was divided into two groups of station in the shallow water (<200 meters in depth, Group A) and the deep water (201 ~ 500 meters in depth, Group B). The major individual-dominant species was S. birostrata, Ophiuridae spp. and immature C. opilio in group A. But Group B was P. eous, A. lar, B. magister and mature C. opilio.

진해만 안골 바지락 양식장 대형저서동물 군집의 구조

  • Park Yeong Min;Yun Byeong Seon;Kim Gu Hwan;Yun Seong Gyu
    • Proceedings of the Korea Society of Environmental Biology Conference
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    • 2003.11a
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    • pp.92-97
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    • 2003
  • Community structure of macrobenthos was studied on Angol clam farming ground of Chinhae Bay in the southern coast of Korea. Macrobenthos samples were collected monthly using a quadrate at each station from March 1998. Macrobenthos samples were seived by 1.0mm mesh seive. Mean grain size was 0.267 mm. A total of 111 macrobenthos species were sampled with a mean density of 1,651ind/m$^2$and biomass of 1466.7wwt.g/m$^2$. Annelida was density-dominant faunal group with a mean density of 818ind/m$^2$, comprising of 49.6% of the total density of the macrobenthos. It was followed by Mollusca with 660ind/m$^2$(40.0%). Mollusca was biomass-dominant faunal group. Major dominant species in the number of individual were Ruditapes philippinarum (375ind/m$^2$), Batillaria cumingi (208ind/m$^2$), Cirrformia tentaculata (167ind/m$^2$), Ceratonereis erithraeensis (151ind/m$^2$), Capitella capitata (111ind/m$^2$) and Sigambra tentaculata (91ind/m$^2$). Major dominant species in the biomass were Ruditapes philippinarum (1156.6wwt.g/m$^2$), Batillaria cumingi (111.0wwt.g/m$^2$) and Cyclina sinenis (106.2wwt.g/m$^2$). The species diversity was increased gradually during the study period. Increasing of species diversity was due to not only increasing of number of species but also decreasing of dominance of some polycheates. Contents of silt-clay was increased gradually in the intertidal zone.

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Cytotoxic Constituents form the Roots of Anthriscus sylvestris

  • Lim, Young-Hee;Leem, Moon-Jeong;Shin, Dong-Hyuk;Chang, Hwan-Bong;Hong, Seung-Woo;Moon, Eun-Yi;Lee, Dug-Keun;Yoon, Sung-June;Woo, Won-Sick
    • Archives of Pharmacal Research
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    • v.22 no.2
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    • pp.208-212
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    • 1999
  • Activity-guided fractionation of the roots of Anthriscus sylvestris resulted in the isolated and characterization of five cytotoxic compounds, deoxypodophyllotoxin (1), falcarindiol (2), and angeloyl podophyllotoxin (5) from the hexane soluble fraction and morelensin (3), bursehernin (4) from the choloroform soluble fraction. It is the first report of the occurrence of compound 5 in nature.

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Synthesis and Cytotoxic Activity of 1-(1-Benzoylindoline-5-sulfonyl)-4-phenylimidazolidinones

  • Sang-Hun Jung;Hui-Soon Lee;Nam-Soo Kim;Hwan-Mook Kim;Moonsun Lee;Dong-Rack Choi;Jung-Ah Lee;Yong-Ho Chung;Eun-Yi Moon
    • Archives of Pharmacal Research
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    • v.27 no.5
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    • pp.478-484
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    • 2004
  • The novel 1-(1-benzoylindoline-5-sulfonyl)-4-phenyl-4,5-dihydroimidazolones 2 shows highly potent and broad cytotoxicities. Their cytotoxicities against human lung carcinoma A549, human chronic myelogenous leukemia K562, and human ovarian adenocarcinoma SK-OV-3 are compatible with doxorubicin. Compound 2p (1-[(4-aminobenzoyl)indoline-5-sulfonyl])-4-phenyl-4,5-dihydroimidazolone) exhibits a cytotoxicity that is far more potent than doxorubicin and also exhibits highly effective antitumour activities against murine (3LL, Colon 26) and human xenograft (NCI-H23, SW620) tumor models.