• Proceedings of the Korean Vacuum Society Conference
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• 1999.07a
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• pp.38-38
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• 1999

KSTAR(Korea Superconducting Tokamak Advanced Research) 핵융합 실험 장치의 진공용기 및 진공용기 내부의 플라즈마 대향 부품들은 초고진공 (5$\times$10-9 Torr)의 달성을 위해 진공용기 내부의 이물질(H2, H2O, CO, CO2, CH4 등) 제거를 목적으로 SS316LN인 진공용기는 25$0^{\circ}C$, 탄소 물질인 플라즈마 대향부품은 35$0^{\circ}C$ 정도까지 가열(이하 베이킹)할 필요성이 있다. 이 가열방법으로 고온 질소가스를 진공용기 이중벽 사이로 흘려주는 방식과 코일에 저주파 교류전류를 흘려 진공용기를 유도가열하는 방식이 고려되고 있는데, 유도가열방식은 최대 유도 전력이 70kW 정도로 실제 베이킹에 필요한 열량을 공급하는데 있어 적잖이 부족하며 또 국부적인 가열 특성으로 인하여 KSTSR의 베이킹 방식은 전자의 가열방식을 우선적으로 채택하고 있다. 본 논문에서는 0-차원 해석을 통하여 진공용기와 플라즈마 대향 부품들에 대한 베이킹 계획을 결정하고 이를 만족시키기 위해 투입해야 할 열량을 직선적으로 증가하는 온도 곡선에서 각 부분의 온도 상승률을 다르게 설정한 세 경우와 F-자 형태로 변화하는 온도 곡선의 경우에 대해 각각 적용하여 시간에 따른 필요열량을 비교.검토하였으며, 이를 근거로 안정적인 베이킹 계획을 선정하였고 이 베이킹 계획의 실현을 위해 투입해야 할 고온 질소가스의 유량과 온도 도달시간까지 매 시간에서의 가스온도를 산출하였다. 토러스 형상의 토카막 진공용기와 플라즈마 대향 부품 및 다층단열재에 대한 해석 모델은 길이가 유한한 0-차원 실린더 모델로 가정하였고, 이에 대한 기하학적 성질 및 열역학적 성질은 유효계수를 고려하여 산출하였다. 진공용기 이중 벽 내부로 흐르는 질소가스의 유량과 온도의 계산은 진공용기 내벽과 외벽을 각각 독립적인 열전달 요소로 가정하여 구성한 모델을 이용하였다. 전체 해석에서 각 열전달 요소의 비열 값은 온도에 따라 변화하는 비열의 특성을 반영하였으며. 진공용기와 플라즈마 대향 부품의 방사율(emissivity)은 앞서 가정했던 각 온도 상승 곡선에 대해서 각각 0.1, 0.2, 1.3의 경우를 가정하여 계산하였다. 직선적으로 증가하는 온도 상승 곡선중 2$0^{\circ}C$/hr의 온도상승율을 갖는 경우가 다른 베이킹 시나리오 모델에 비해 효과적이라 생각되며 초대 필요 공급열량은 200kW 정도로 산출되었다. 실질적인 수치를 얻기 위해 보다 고차원 모델로의 해석이 필요하리라 생각된다. 끝으로 장기적인 관점에서 KSTAR 장치의 베이킹 계획도 살펴본다.

• Proceedings of the Korean Society for Applied Microbiology Conference
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• 1986.12a
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• pp.517.1-517
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• 1986

고온 호알카리성 Bacillus K-17의 Protease gene의 구조해명과 성질을 알기 위해서, E. coli HB101에 pER 322를 Vector로 하여 Protease gene을 Cloning하여 형질전환 된 균주를 선정하였다. 선정균주의 pretense activity를 Bacillus K-17의 상대활성도와 매우 유사하였으며 균체외에 보다 많은 효소 활성도를 지니고 있었다. 제한효소 Hind III로 절단하면 약 1.8kb와 0.4kb의 2개의 fragments 가 생성되었으며 Southern hybridization 결과 Cloning 된 gene이 Bacillus K-17에서 유래된 것임이 확인되었다.

• Polymer(Korea)
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• v.30 no.6
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• pp.545-549
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• 2006

Blends of poly(acrylic acid- co-maleic acid) (PAM) with poly (vinyl alcohol) (PVA) were pre -pared in distilled water PVA/PAM/saponite (PVA/PAM/SPT) nanocomposite films were prepared with various clay contents by using the solution intercalation method. The variations of the dispersion, morphology, and thermo-mechanical properties of the nanocomposites with clay content in the range 0 to 9 wt% were examined. Up to 3 wt% clay loading, the clay particles were homogeneously dispersed in the PVA/PAM blends. However, some agglomerated structures form in the polymer matrix above a clay content of 7 wt%. The thermal stability of the hybrids was increased linearly with increasing the clay loading up to 9 wt%. The maximum strength and modulus were obtained at a clay content of 7 wt%. Thus, the addition of small amounts of clay to the PVA/PAM blends produced PVA/PAM nano-composites with improved the thermo-mechanical properties.

• Journal of the Korean Chemical Society
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• v.40 no.9
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• pp.607-614
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• 1996

The structural changes and dielectric properties of Pb1-x(Na1/2La1/2)x(Mg1/3Nb2/3)O3 compounds substituted by 0∼50 mol.% of Na+/La3+ mixed ions were investigated by X-ray diffraction method, IR and Raman spectroscopy, and LCR meter. The amount of perovskite phase increased with the increases of Na+/La3+ substituents and sintering temperatures. Although the superlattice lines due to 1:1 ordering were not detected by X-ray diffraction method, it was found, from the Raman spectroscopy and the increase of diffuseness coefficient, that the ordering behavior was related to the decrease of A site ion size. Dielectric properties in Pb1-x(Na1/2La1/2)x(Mg1/3Nb2/3)O3 were affected by the amount of perovskite phase, grain size, and density. The phase transitions were broadened and phase transition temperatures were lowered by the increase of Na+/La3+ ions.

• Journal of IKEEE
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• v.2 no.2 s.3
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• pp.212-224
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• 1998

There are two major factors of degrading the performance in the forward link of DS/CDMA systems. One is the multiple access interference (MAI) caused by using the same frequency bands simultaneously and the other is the multipath lading due to multipath propagation. PN codes which have minimum cross correlation properties among spread spectrum codes are necessary to reduce the MAI. In the conventional IS-95A system, the PN sequence has the period of $2^{15}$ and is of the length of 64 chips for spreading each data. In this case, since the length of PN code per bit is very short compared to the period of the PN code, the performance of the conventional system is not satisfied in view of suppressing the multipath interference. However, the correlation property of the PN codes at the demodulation can be improved by increasing the interval of Integration at the demodulation. This paper proposes a demodulation method to reduce the cross correlation among PN codes. The performance of the proposed demodulation method is investigated through computer simulations. We used multipath Ray lading channel and AWGN channel in the simulation. Our simulation results show the improved performance of $0.25{\sim}0.5dB$ SNR in a given BER compared to the conventional demodulation scheme.

• Journal of the Korean Magnetics Society
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• v.7 no.3
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• pp.140-145
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• 1997

The amorphous state of $NdFe_{10.7}TiB_{0.3}$ and its nanocrystallization have been studied by X-ray diffraction, 모스바우어 spectroscopy, and a vibrating sample magnetometer (VSM), $NdFe_{10.7}TiB_{0.3}$ amorphous ribbons were fabricated by a sigle-roll melt-spinning method. The average hyperfine field $H_{hf}$(T) of the amorphous state shows a temperature dependence of $[H_{hf}(T)-H_{hf}(0)]/H_{hf}(0)=-0.46(T/T_c)^{3/2}-0.34(T/T_c)^{5/2}$ for $T/T_c<0.7$ indicative of spin wave excitation. The quadrupole splitting just above the Curie temperature $T_c$ is 0.46 mm/s, whereas the average quadrupole shift below $T_c$ is zero. The Curie and crystallization temperatures are determined to be $T_c$=380K and $T_x=490K$, respectively, for a heating rate of 5 K/min. The occupied area of nanocrystalline phase at around 770K is about 65%. Above the Curie temperature, VSM data show magnetic moments increases again. The formation of $\alpha$-Fe is the main reason for the increasing moment as conformed with the 모스바우어 measurements.

• Journal of the Korean Magnetics Society
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• v.5 no.4
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• pp.281-286
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• 1995

In order to study the effect of additives $SiO_{2}$ on the magnetic properties of hexaferrite sheet magnet, we used X-ray diffractometer, Mossbauer spectrometer, and VSM magnetometer. We have prepared $Ba_{0.25}Sr_{0.75}Fe_{12}O_{19}$ green sheets by the Dr. Blade method. Most of samples have a magnetoplurnbite crystal structure of typical M-type hexaferrite. The lattice parameters are found not to be affected by the addition of $SiO_{2}$. ${\alpha}-Fe_{2}O_{3}$ phase develops above $SiO_{2}$ 2.0 wt.%. Isomer shifts indicate that the valence of Fe ions is trivalent. Curie temperatures decrease slightly with increasing $SiO_{2}$ concentrations. It means that the $Si^{4+}$ subsitution for 12k-site $Fe^{3+}$ has an effect on the superexchange interactions Fe-O-Fe, which change the distance and the angle between cations and anions. It was suggested that ${\alpha}-Fe_{2}O_{3}$ phase results from the excessive Fe produced by subsituting $Si^{4+}$ for $Fe^{3+}$. Based upon the results of $Ba_{0.25}Sr_{0.75}Fe_{12}O_{19}$ added with $SiO_{2}$, we concluded that $H_{c}$, $M_{s}$ and $M_{r}$ depend more strongly on the microstructure chracteristics than on the cation substitution.

• Journal of the Korean Chemical Society
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• v.23 no.1
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• pp.7-14
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• 1979

Changes in CD, ORD and uv-spectra during the mutarotation of poly(trans-5-methyl-L-proline) (PTMP) were studied. The forward mutarotion of PTMP occurred in strong organic acids and trifluoroethanol, while the reverse mutarotation was observed by dilution of the trifluoroethanol solution with excess aliphatic alcohols. The changes in CD, ORD and uv-spectra during the forward and reverse mutarotation proceeded paralell to those found for the mutarotation of polyproline. The chemical shift of the ${\alpha}CH-$proton was shifted downfield about 0.3 ppm during the forward mutarotation. The reduced viscosity for the forward mutarotation increased from 0.15 to 0.26 (dl/g) during 5 days. The equilibrium between form I and form II was estabilished in an appropriate solvent mixture. All changes in solution properties mentioned above are similar to those found for polypoline. These results support that the two forms of PTMP are the same conformations as polyproline form I and form II, i. e., a right-handed helix with all cis amide bonds and a lefthanded helix with all trans amide bonds.

• Korean Journal of Materials Research
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• v.11 no.4
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• pp.300-304
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• 2001

Effect of Cd addition on the fatigue properties of Al-Cu-Mn cast alloy was investigated by low and high cycle fatigue tests. With increasing Cd content, fatigue life and tensile strength were increased. It was found that the fatigue strength was 115MPa and the fatigue ratio was 0.31. Metallographic observation revealed that the fatigue crack initiated at the surface and propagated along the grain boundary. This propagation path was attributed to the presence of PFZ along the grain boundary. The tensile strength increased from 330MPa in the Cd-free Al-Cu- Mn cast alloy to 401MPa in the 0.15%Cd-containing alloy.

• The Journal of Natural Sciences
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• v.4
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• pp.59-68
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• 1991

$\beta$-Galactosidase(EC 3.2.1.23) from pathogenic Neisseria lactamica 2118 was purified by p-aminopheny1-$\beta$-D-thiogalactopyranoside agarose affinity chromatography. Then some properties of the purified $\beta$-galactosidase were investigated.$\beta$-Galactosidase form Neisseria lactamica 2118 was constitutive enzyme, not induced by lactose and IPTG. Optimal activity was observed at $35^{\circ}C$ and pH 7.5 and the enzyme was stable at the range of pH 6.0-9.0 and at temperature below $50^{\circ}C$. The enzyme activity was inhibited by cations such as $Hg^(2+)$ and $Co^(2+)$.