• Title/Summary/Keyword: 흡광

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Prediction of the Glucose Concentration Based on Its Optical Absorbance at Multiple Discrete Wavelengths (복수 개의 광파장에 대한 상대적 흡광 특성을 이용한 글루코스 농도 측정)

  • Kim, Ki-Do;Son, Geun-Sik;Lim, Seong-Soo;Lee, Sang-Shin
    • Korean Journal of Optics and Photonics
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    • v.19 no.6
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    • pp.416-421
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    • 2008
  • A scheme for predicting the concentration of a glucose solution based on its relative optical absorbance at multiple probe wavelengths was proposed and verified. The relative absorbance at each of the probe wavelength was obtained with respect to the absorbance at a reference wavelength. The single reference wavelength (1310 nm) and a group of four different probe wavelengths (1064, 1550, 1685, 1798 nm) were selected to exhibit the glucose absorbance with opposite signs, thereby enhancing the accuracy of the prediction. The final glucose concentration was estimated by taking the average of the predicted values provided by the four probe wavelengths. The absorbance of the glucose solution for the path length of 5 mm was $-1.42{\times}10^{-6}\;AU$/(mg/dL) at the reference wavelength of 1310 nm and peaked at $+8.12{\times}10^{-6}\;AU$/(mg/dL) at 1685 nm. The concentration of the glucose solution was decently predicted by means of the proposed scheme with the standard error of prediction of ${\sim}28\;mg/dL$. In addition, the influence of the ambient temperature and the fat thickness upon the prediction of the glucose concentration was examined. The absorption change with the temperature was $-9.1{\times}10^{-5}\;AU/^{\circ}C$ in the temperature range of $26{\sim}40^{\circ}C$ at the reference wavelength, and $-2.08{\times}10^{-2}\;AU/^{\circ}C$ at 1550 nm. And the absorption change with respect to the fat thickness was +1.093 AU/mm at the probe wavelength of 1685 nm.

Extraction of Freeze Dried Young Antler by Water and Protease (물과 단백질 가수분해 효소에 의한 동결건조 녹용의 추출)

  • 안용근
    • The Korean Journal of Food And Nutrition
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    • v.16 no.4
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    • pp.379-387
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    • 2003
  • The freeze dried young antler was extracted by water and proteases. In case of water extraction, the extraction rate was highest when it was reacted in 5% of concentration for 6 hours at 50$^{\circ}C$. The result of HPLC analysis of extract shows that high molecular peak in water extract was transformed into low molecular polk by proteases. The rate of low molecular peak was highest when bacteria protease was used, and its second highest rate was pepsin, but the effect of papain on it was low, The extraction rate of young antler reacted for 5 hours was 33.4%(absorbance 13.25 at 280nm) of bacteria protease, 22.4%(absorbance 10.06) of papain, and 30.2% (absorbance 11.34) of pepsin. The young antler was boiled for 30min and it was reacted by proteases for 5 hours at 50$^{\circ}C$. The extraction rate of it was 47,6%(absorbance 12,54) of bacteria protease, and 26,4%(absorbance 7,48) of papain, and 45.6%(absorbance 7.23) of pepsin, In protein content, water extract was 52,1%, bacteria protease extract was 37.8%, and in amino acid content, water extract was 16.3%, bacteria protease extract was 31.96%, in ash content, water extract was 8.8%, bacteria protease extract was 5.6% by dry base. In mineral content, water extract contains 3.6% of Ca, 8.6% of P, 0.01% of Mg, 1.4 % of Na, 0.02 % of F, and bacteria protease extract contains 2.5% of Ca, 11.8% of P, 0.046 % of Mg, 2.1 % of Na, 0.018 % of F by dry base.

Study on Optical Characteristics of 8-Hydroxyquinoline Synthesized Derivative as Sensing Material of the Fiber-Optic Copper Ion Sensor in Aqueous Environment (수질환경에서 광섬유 센서의 구리 이온 감지 물질로서 8-Hydroxyquinoline 합성유도체의 광학적 반응 특성 연구)

  • Kim, Beom Kyu;Park, Byung Gi
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.18 no.12
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    • pp.100-105
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    • 2017
  • An 8-hydroxyquinoline compound that was synthesized with 8-hydroxyquinoline-2-carboxaldehyde and 4-aminoantipyrine was investigated for use as the sensing material of a fiber-optic copper ion sensor in an aqueous environment. The experiment was conducted with a fiber-optic measurement system, in order to evaluate the relationship between the absorbance peak and copper ion concentration. The synthesized derivative exhibited a (highly selective) chromogenic phenomenon for copper ions among various metal ions in an aqueous environment and showed a specific absorbance peak at a wavelength of 530 nm for copper ions. The effect of mercury ions was investigated to evaluate the selectivity of the prepared synthesized derivatives toward Cu ions. The absorbance was measured at various concentration ratios of Cu and Hg ions (Cu:Hg ratios from 0.05 to 20), and it was found that the absorbance at 530 nm tended to increase with increasing Cu ion concentration. The experimental results also showed the linear relationship between the logarithmic concentration of copper ions and the specific absorbance peak at a wavelength of 530 nm. These results indicate that the synthesized 8-hydroxyquinoline compound has selectivity for copper ions and can be used as a sensing material for fiber-optic copper ion sensors.

Spectral Characteristics associated with Heavy Metal Concentration and Mineral Composition in Cropland and Rice Field Soils from Downstream of an Abandoned Coal Mine (폐석탄광 하류 밭토양 및 논토양의 중금속 함량과 광물조성에 따른 분광학적 특성)

  • Seo, Jihee;Yu, Jaehyung;Koh, Sang-Mo;Lee, Bum Han
    • Economic and Environmental Geology
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    • v.53 no.6
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    • pp.743-753
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    • 2020
  • This study analyzed heavy metal concentration, mineral composition, and spectral characteristics of heavy metal contaminated soil samples of cropland and rice field located in downstream of abandoned Okdong coal mine. X-ray fluorescence analysis detected heavy metal elements including cadmium, copper, arsenic, lead, zinc and nickel in the soils. Both cropland and rice field samples were severely contaminated with arsenic showing higher concentration over the concerned standard. The pollution index of cropland samples was higher than that of rice field samples. X-ray powder diffraction analysis identified that the mineral composition of cropland and rice field samples is similar with quartz, calcite, kaolinite, illite, smectite, magnetite and hematite. The range of organic matter content were more widely distributed in cropland samples. The spectral analysis showed that the reflectance spectra and the absorption features of cropland and rice field samples were alike. The absorption features that appeared near 490nm and 900nm were attributed to the ferric iron, and clay minerals such as kaolinite and smectite caused the absorption features at 1410nm, 1910nm and 2200nm. The reflectance of the soil spectral decreased with an increase in organic content. The absorption depths of both types of soil samples decreased with higher organic matter content at 490nm and 1916nm as well as higher heavy metal concentration.

작업환경중 금속시료의 적정 분석에 관한 연구(크롬)

  • Kim, Seok-Won
    • 월간산업보건
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    • s.90
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    • pp.2-8
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    • 1995
  • 원자 흡수 분광법과 용매 추출을 이용한 크롬의 정량분석 조건을 연구하였다. tertiary amine류 중 octy기를 갖는 trioctylamine(TOA)과 quaternary ammonium salt류 중 octy1 기를 갖는 trioctylmethylammonium chloride(TOMAC)가 음이온 교환기로 사용되었다. 또한 첨가되는 산의 종류와 산의 농도 변화에 따라서 원자흡수분광기를 이용하여 흡광도를 측정하였다. TOA사용시 염산의 농도가 0.1M-0.3M사이, TOMAC사용시 염산의 농도가 0.03M-0.1M사이에서 최대 흡광도를 나타내었다. 산이 첨가된 MIRK에 용해된 TOA나 TOMAC와 Cr과의 mole농도 비율이 1:1이상이 된 것이 최대 추출효율을 보았다. 추출과정을 검토한 결과, 본 실험에서 사용된 방법은 비슷한 다른 방법들과 비교하여 보면 크롬의 추출효율이 좋은 것으로 판명되었다.

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토양속의 인산 가용화를 위한 Pantoea agglomerans 배양의 최적 조건 및 균주 고정화를 위한 안정성 조사

  • Jeong, Il;Yang, Song-Won;Kim, Gil-Yong;Yu, Ui-Yeon;Park, Don-Hui
    • 한국생물공학회:학술대회논문집
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    • 2000.11a
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    • pp.364-367
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    • 2000
  • 토양속의 인산 가용화를 위한 Pantoea agglomerans 배양의 최적조건과 균주 고정화를 위한 안정성을 조사한 결과 $30^{\circ}C$, pH 7.0, 공기유량 2vvm에서 각각의 흡광도 값이 51시간에서1.756과 1,713, 50시간대에 1.819로써 가장 균의 성장이 활발한 것으로 나타났으며, 1% $CaCl_2$ 용액에서 172시간대에 흡광도값 2.361로 가장 안정하였다.

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A Study for TOC & UV/VIS Absorbance of Humic Acid in Ozonation (오존처리시 부식산의 흡광도 및 총유기탄소량 변화에 관한 연구)

  • Kim, Kei-Woul;Han, Mi-Duck;Shin, Sung-Hee;Rhee, Dong-Seok
    • Journal of Industrial Technology
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    • v.18
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    • pp.417-423
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    • 1998
  • Experiments were performed to evaluate UV/VIS absorbance and TOC of humic acid solutions which were ozonated at different pH values. The optimum conditions for ozonation of humic acid from this study are pH 9 (buffered) and 0.84 ($H_2O_2/HA$, w/w) for $H_2O_2$ dosage.

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