• Title/Summary/Keyword: 황 회수

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Comparative Study on the Adsorptive Loss of Reduced Sulfur Compounds (RSC) by the Selection of Tubing Materials (튜빙의 종류에 따른 환원황화합물들의 흡착손실 비교 연구)

  • Kim Ki-Hyun;Ahn Ji-Won;Choi Ye-Jin
    • Journal of the Korean earth science society
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    • v.26 no.7
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    • pp.668-673
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    • 2005
  • To collect or transfer samples of gaseous pollutants, various types of tubing are used. Hence, to analyze the uncertainties associated with the use of tubings, a series of comparative test were designed and conducted using the RSC standards with different concentration ranges. For the purpose of this study, we prepared tubings made of six different types of material which include: [1] silco-steel (S1), [2] stainless steel (S2), [3] silicone (S3), [4] PTFE Teflon (T1), [5] tygon (T2), and [6] brass (B). The patterns of RSC loss on to tubing walls, when compared on the basis of the least reactive material S1, exhibited that the extent of RSC loss varied dynamically. It was found that Teflon is highly stable. However, other materials tend to exhibit contrasting patterns of loss. S2 and B show significant loss of light RSC $(H_2S\;and\;CH_3SH)$, while S3 and T2 experience notable loss of heavy RSC (DMS and DMDS).

난자가 체외성숙된 시간에 따른 한우 체세포 복제수정란의 발달과 MPF(Maturation Promoting factor)의 변화

  • 김동훈;이상기;양병철;임기순;정운원;박효숙;김세웅;황인선;서진성
    • Proceedings of the KSAR Conference
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    • 2004.06a
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    • pp.255-255
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    • 2004
  • 본 연구는 한우 체세포 복제수정란의 발달에 있어서 난자가 체외성숙 된 시간이 미치는 영향을 확인하고, 또한 체외성숙 시간별 성숙난자의 MPF 활성도 변화를 조사함으로서 소 복제수정란 생산을 위한 적정 체외성숙 조건을 살펴보는데 목적이 있었다. 도축된 한우로부터 채취된 난소로부터 미성숙 난자를 채취하여, 1 ㎍/㎖ FSH와 1 ㎍/㎖ E2가 첨가된 TCM-199 배양액에서 18, 20, 22시간 체외성숙 후에 각각 성숙난자를 회수하여 22시간째 제핵을 실시하였다. (중략)

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Analytical Techniques for Sulfur Compounds by the Combination of GC/PFPD. (GC/PFPD를 이용한 악취성 황화합물의 분석기법에서의 회수율에 대한 연구)

  • 김기현;최여진;오상인
    • Proceedings of the Korea Air Pollution Research Association Conference
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    • 2003.11a
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    • pp.283-284
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    • 2003
  • 환원황 성분들은 사람들이 일상적으로 생활하는 환경권역에서 고농도 (ppb 수준 이상)로 존재할 경우, 악취의 주요원인물질로 작용한다는 점에서 상당한 주목을 받고 있다. 국내의 경우, 환경부에서는 이미 '92년 8월 대기환경보전 법을 개정하여, 황화수소를 위시한 4개의 황화합물과 트리메틸아민, 암모니아, 아세트알데히드, 스티렌을 포함하는 총 8개 화합물을 악취물질로 지정하여 관리하고 있다. 이러한 황화합물을 분석하는데 spectrophotometry, polarography, fluorescence, coulometry, impregnated filter 방식 등이 활용되고 있다 (Blank et al., 1978). (중략)

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Development of Analysis Method of Gardenia Yellow as Natural Colorants and Content Survey in Commercial Foods by HPLC (HPLC를 이용한 천연착색료인 치자황색소의 분석법 개발 및 시판 식품중 함유량조사)

  • Kim, Hee-Yun;Kim, So-Hee;Hong, Ki-Hyoung;Lee, Chul-Won;Kim, Kil-Saeng;Ha, Sang-Chul;Jo, Jae-Sun
    • Korean Journal of Food Science and Technology
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    • v.31 no.4
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    • pp.945-951
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    • 1999
  • A simple and practical method for the determination of gardenia yellow in foods was developed. In this method, analysis of gardenia yellow in food products has been carried out by the detection of crocetin and/or geniposide as indicator compounds. As a new analytical method for gardenia yellow, we adopted crocetin, which is produced from colored components of gardenia yellow by alkaline hydrolysis, as an indicator compound. The analysis of gardenia yellow was performed by reverse phase high performance liquid chromatography using a Capcell pak $C_{18}$ column at wave length 240 nm (geniposide) and 435 nm (crocetin). The recovery rates of geniposide and crocetin were found to be 93.4% and 87.8% for Dan Mu Ji, 90.2% and 85.9% for milk, 92.8% and 86.5% for snack, respectively. With this method, the range of crocetin and geniposide contents $({\mu}g/g)$ were as follows: $ND{\sim}1.7$ and $ND{\sim}14.1$ for Dan Mu Ji, $ND{\sim}0.2$ and $ND{\sim}13.6$ for milk, $ND{\sim}1.6$ and $ND{\sim}0.9$ for snack, respectively. The detection limits of crocetin and geniposide were 0.07 ${\mu}g/g$ and 0.05 ${\mu}g/g$, respectively.

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Reduced sulfur gas loss in the bag sampling procedure - Comparison by calibration slope values (악취황 성분의 채취와 샘플백 내부의 시료 유실율 비교: 검량선의 기울기를 이용한 평가)

  • Kim, K.H.;Choi, Y.J.;Ahn, J.W.
    • Analytical Science and Technology
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    • v.18 no.4
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    • pp.338-343
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    • 2005
  • In this work, sample loss of reduced sulfur compounds (RSC) was investigated with respect to bag sampling techniques. For comparison purpose, calibration slopes were obtained by analyzing standards prepared by 'within syringe dilution' (WSD) method against those made either by 'Tedlar bag dilution' (TBD) or by 'polyester aluminum bag dilution' (PBD) method. The results indicated that the recovery rate of TBD showed the mean values of about 87%, while those of PBD about 77%. Despite the fact that sample loss is inevitable, precise sampling of reduced sulfur compounds may still be possible, if one acknowledges and be prepared for such loss rates of bag sampling methods.

Gold Recovery from Geumsan Concentrate Using Microwave-nitric Acid Leaching and Lead-fire Assay (마이크로웨이브-질산용출과 납-시금법을 이용한 금산정광으로부터 금 회수)

  • Lee, Jong-Ju;On, Hyun-Sung;Park, Cheon-Young
    • Journal of the Mineralogical Society of Korea
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    • v.32 no.2
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    • pp.113-126
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    • 2019
  • This study aimed to effectively dissolve sulfide minerals through microwave-nitric acid leaching of invisible gold concentrate and then recover gold from the solid-residue with fire assay. For the purposes, this study conducted microwave-nitric acid leaching experiments to examine nitric acid concentration, time of microwave leaching, and sample addition effect. As results of the experiments, this study discovered that the weight loss rate of solid-residue increased as nitric acid concentration and microwave leaching time increased while weight loss rate decreased as sample addition increased. In an XRD analysis with solid-residue, it was discovered that pyrite completely disappeared when the nitric acid concentrate was 6 M and the microwave leaching time was 18 minutes. When a fire assay was carried out with solid-residue, gold particles with more content were recovered as nitric acid concentration and microwave leaching time increased whereas gold particles with more gold content were recovered as the sample addition decreased.

A Study on Stabilization of Underwater TAS Winch System Deploy/Recover Operation Performance (수중용 TAS윈치 전개/회수 성능 안정화 방안에 관한 연구)

  • Chang, Ho-Seong;Cho, Kyu-Lyong;Hwang, Jae-Gyo;Lee, Sang-Yong;Kim, Yong-Tae
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.20 no.6
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    • pp.472-482
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    • 2019
  • This paper describes the stabilization of underwater TAS winch system Deploy/Recover operation performance. TAS winch installed on the stern of submarine performs to deploy/recover sensor, towing cable and rope tail which is deployed from the stern and separated from submarine itself. Also TAS winch provides transmission path of power to the sensor and data transmitting/receiving path which data are acquired from underwater environment like sound, depth and temperature. At the step of TAS winch evaluation test, sporadic standstill and rotating speed oscillation phenomenon were occurred. Winch motor provides the available torque to deploy/recover TAS and root cause analysis to the winch motor was done to find exact reason to sporadic malfunction. When winch motor was disassembled, eccentricity of rotor, slip-ring and the other composition part for winch motor were found. These might cause magnetic field distortion. To make TAS winch system more stable and block magnetic field distortion, this paper suggests methods to enhance fixing status installed in winch motor. For reliable data acquisition for TAS winch operation, the deploy/recover function of the improved type of TAS winch was verified in LBTS making similar condition with sea status. At the end of stage, improved type of TAS winch was tested on some functions not only deploy/recover function, but sustainability of TAS operation on specific velocity, steering angle of submarine in the sea trial. Improved type of TAS winch was verified in accordance with design requirement. Also, validity of suggested methods were verified by the sea trial.

Feasibility Study on Thermal Power Plant Condenser Heat Recovery for District Heating and Fuel Line Preheating (발전소 복수기 배열회수의 지역난방 및 연료라인 예열용 활용타당성 검토)

  • Jung, Hoon;Hwang, Gwang-Won
    • New & Renewable Energy
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    • v.5 no.3
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    • pp.40-48
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    • 2009
  • Recovered heat has been considered as a renewable energy in Europe since 2008 because its great effect on energy saving and carbon decreasing in plant process. Energy saving and decreasing green gas are critical issue today, so various technologies to save energy and decrease carbon dioxide in plant process have been applied to many industrial area. In this paper, the feasibility of condenser heat recovery by heat pump in power plant for district heating and fuel line preheating were reviewed by verifying energy (heat) balance and mass balance of power plant model. Some ways to compose proper system to recover heat of condenser are suggested and their possibilities are also reviewed. Limitations on heat recovery in power plant are also reviewed. The results are verified by calculating input/output energy based on actual performance test data of Taean Thermal Power Plant in Korea. There is noticeable improvement of plant performance in some cases which demand low temperature (<100 C) heat like distrcit heating, fuel line heating, and so forth.

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A New Slip Power Recovery System by Switch Mode Converter (스위치모드 컨버터에 의한 새로운 슬립전력 회수시스템)

  • 박한웅;박성준;김철우;황영문
    • The Transactions of the Korean Institute of Power Electronics
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    • v.4 no.1
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    • pp.73-81
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    • 1999
  • A new slip power recovery system applying a switch mode converter to the rotor circuit of the wound rotor induction machine is proposed and investigated in this paper. With the analysis of the steady-state performances of the proposed system, it can be shown that the speed can be controlled by the duty ratio of the converter switch and the several characteristics of a conventional system can be also improved. In particular, the low power factor and the harmonic components in the line current, which are the main disadvantages of the conventional system, is significantly improved, and linear speed regulation can be obtained. Theoretical and experimental results are presented and illustrated to demonstrate the satisfactory working of the proposed system.