• Title/Summary/Keyword: 화학적 성분 분석

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Simultaneous Analysis of Cold Medicine Component by High-Performance Liquid Chromatography(HPLC) (고성능 액체크로마토그래피(HPLC)를 이용한 Cold Medicine 성분의 동시 분석)

  • Wonju Lee;Seung-Tae Choi;Keun-Sik Shin;Jin-Young Park;Jae-Ho Sim
    • The Journal of the Convergence on Culture Technology
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    • v.9 no.6
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    • pp.867-873
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    • 2023
  • In this study, for the purpose of standardized quality control of a cold medicine, we simultaneous analyzed four main chemical components of a cold medicine: acetaminophen, caffeine, methyl paraben, and propyl paraben. The sample was subjected to quantitative analysis using high performance liquid chromatography (HPLC), after pretreatment of four components. The experiment was carried out by using Isocratic elution at wavelength of 270nm. Acetonitrile and water (H2O) were used as a mobile phase at a flow rate of 1.0mL/min in a commercial C18 reversed-phase column. A volume of 10uL cold medicine were injected into the column with column oven temperature at 35℃. As a result of the experiment, the values of Resolution were 4.983, 1.596, 5.519, and 1.678 respectively-well over Rs >1.5, which indicates that the separation of four components were efficient. In addition, value of symmetry factor of the components was 1.056, 1.069, 1.032, and 1.133 respectively, to show its symmetrical stability. The calibration curve of all four components exhibits good linearity with R2 >0.9995 to 0.9999. Furthermore, the limit of detection(LOD) were between 0.0118 to 1.5973 mg/mL, while the limit of quantification (LOQ) were between 0.0353 to 4.7919 ㎍/mL with the recovery rate of 79.6% ~ 120.5%. The results of this study showed an efficient quality evaluation of a simultaneous analysis method for cold medicine components.

A Study on the Chemical Reaction of Crushed Aggregates (국내 쇄석골재의 화학반응성 연구)

  • 이장화;김성욱
    • Magazine of the Korea Concrete Institute
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    • v.7 no.1
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    • pp.136-144
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    • 1995
  • 근래 양질의 하천골재가 거의 고갈상태에 직면함에 따라 쇄석골재의 사용이 보편화되고 있는 우리나라의 실정에 비추어 볼 때 골재의 화학반응에 대한 연구의 필요성이 점차 증대되고 있다. 본 연구에서는 우리나라에서 실제 쇄석골재를 생산하는 238곳 중 63곳의 시료골재를 채취하여 화학적, 광물학적, 모르터 바 분석실험을 실시하여 골재의 화학반응성을 규명하였다. 분석시험 결과 대부분의 시료골재가 화학반응성을 나타내지 않았으나 광물학적 분석에서 유해광물로 알려진 성분들이 여러 시료골재에 포함되어 있었다. 따라서 해사의 사용 등 점차 화학반응 환경이 공존하게 되면 골재의 화학반응이 일어날 가능성이 커지므로 계속적이고 심도있는 연구가 요구되고 있다.

An Assessment of Factory Odor Evaluation with Indirect Olfactory Method (간접관능법에 의한 사업장 발산악취 평가)

  • 김학민;정의석;김선규;김선태;박주철
    • Proceedings of the Korea Air Pollution Research Association Conference
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    • 2002.11a
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    • pp.183-184
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    • 2002
  • 악취현상 평가방법은 냄새유발물질의 농도를 정량적으로 분석하는 화학성분분석법과 복합취기물질에 의란 감각수준을 다수의 악취판정인이 평가하는 관능측정법으로 대별할 수 있다. 특히, 관능측정법의 경우 자극의 세기를 표현하는 직접관능법과 최소냄새감지한계회석배수를 구하는 간접관능법으로 구분할 수 있으며, 환경악취현상을 객관적으로 평가하기 위해서는 성분분석과 감각수준을 평가하는 두 방법에 의한 측정결과를 종합적으로 고려하는 것이 타당한 것으로 알려져 있다. (중략)

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The Mineralogical and Geochemical Study on Korean Scheelites and its Application to the Ore Prospecting (한국산 灰重石鑛의 광물학적, 지화학적 연구 및 그의 探査에의 이용)

  • So, Chil-Sup;Park, Maeng-Eon
    • Economic and Environmental Geology
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    • v.12 no.2
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    • pp.79-93
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    • 1979
  • Twenty five samples of the scheelite-powellite series from twelve Korean tungsten deposits of various geologic settings were studied mineralogically and geochemically. Variations in the trace-element contents of the scheelite minerals are considered in relation to geologic settings and mineralogic properties. Scheelites from ore deposits developed in similar geologic settings and under similar physicochemical conditions are characterized by specific combinations of trace elements.

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The study of the Composition and Physico-chemcal Characteristics of MSW in urban and gangwon area (수도권 및 강원지역 도시고형폐기물의 조성과 물리·화학적 특성연구)

  • Lee, Keon-Joo
    • Journal of the Korea Organic Resources Recycling Association
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    • v.16 no.3
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    • pp.65-74
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    • 2008
  • In this study, the composition and physico-chemical characteristics of municipal solid waste (MWS) which was treated in four different area were investigated. It is necessary to measure the characteristics of MSW to build a waste treatment and Refuse Derived Fuel (RDF) facility, the data-base and total managing of the landfill. It was found that the average density of solid wastes is in the range of $78.15-199.8kg/m^3$. This MSW was composed of 8.87% of food wastes, 38.8% of papers, 34.12% of plastics & vinyls, 7.16% of textiles, 0.96% of wood, 1.3% of rubber & leathers and others, respectively. Most of MSW are composed of food, paper and plastic waste and more than 94% was combustible waste. For three components, moisture is 17.38%, combustible component is 69.03% and ash is 6.24%. The chemical element has the high order of carbon, oxygen, hydrogen on the dry basis of wastes. And the low heating value of the MSW which is measured by calorimeter is calculated as 2973.8 kcal/kg and high heating value of the MSW is calculated as 5209.94 kcal/kg.

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The Study of Physico-chemcal Characteristics of Municipal Solid Waste (MSW) in Gangwon Area (강원지역 도시폐기물의 물리·화학적 특성 연구)

  • Lee, Keon-Joo
    • Journal of the Korea Organic Resources Recycling Association
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    • v.17 no.2
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    • pp.101-111
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    • 2009
  • In this study, the physico-chemical characteristics of municipal solid waste (MWS) which was treated in gangwon area were investigated. It is necessary to measure the characteristics of municipal solid waste for build a waste treatment and RDF facility and for data-base and total managing of the landfill. It was found that the average density of solid wastes is in the range of $101.8{\sim}199.8kg/m^3$. This MSW was composed of 30.7% of food wastes, 36.3% of papers, 15.8% of plastics & vinyls, 1.9% of textiles, 3.2% of wood and 1.5% of rubber & leathers respectively. Most of MSW are composed of food, paper and plastic waste and the combustible waste is more than 90%. For three components, moisture is 44.6%, combustible component is 47.7% and ash is 7.7% respectively. The chemical elements are carbon, oxygen, and hydrogen on the dry basis of wastes. The low heating value of the MSW measured by calorimeter was obtained as 2,631 kcal/kg, and the high heating value of the MSW was obtained as 3,310 kcal/kg.

Analysis of the Urushiol in Korean Lacquer (한국산 옻칠의 우루시올 성분 분석)

  • Kim, Jung-Bae
    • The Korean Journal of Food And Nutrition
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    • v.19 no.3
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    • pp.267-270
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    • 2006
  • In Korea, for a long time Rhus verniciflua has traditionally been used as an herbal medicines plants. A stem of Rhus verniciflua has been used to treat gastrointestinal trouble with in form of boiled chicken as a folk medicine. But it has been recognized as an extremely active allergen causing skin reactions. The chief allergenic component, urushiol, is found within the oleoresinous sap of Rhus verniciflua. Most components of urushiol have unsaturated side chains. These unsaturated side chains of urushiol are important to polymerization of these natural products. The urushiol components in Korean lacquer were isolated by reversed phase HPLC. The molecular weight of purified urushiol was determined as 340 from mass analysis. This compound was identified as Heptadecatetraenyl catechol (MW 340).

Hydrochemistry and Formation Environment of $CO_2$-rich Springs from the Kangwon Province (강원지역에서 산출되는 탄산천의 수리화학 및 생성환경)

  • 정찬호
    • Journal of the Mineralogical Society of Korea
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    • v.17 no.1
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    • pp.61-73
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    • 2004
  • The purposes of this study are to investigate the occurrence, the hydrochemical characteristics and the origin of the $CO_2$-rich springs from the Kangwon Province, and to reanalyze the previous studied results of other researchers. The $CO_2$-rich water samples were collected at 13 locations in the Kangwon Province. The $CO_2$-rich water shows a high $CO_2$ concentration ($P_{CO2}$ 0.787 to 4.78 atm), weak acidic pHs, electrical conductivity values ranging from 422 to 2,280 $\mu$S/cm, and high Fe and F contents. The chemical compositions of $CO_2$-rich water from this study area are classified into three types; $Ca-HCO_3$, Ca(Na)-$HCO_3$, $Na-HCO_3$ types. The chemical data of $CO_2$-rich waters and their host rocks indicate that $Na-HCO_3$ type water are mainly influenced by biotite, K-feldspar granite, and Ca(Na)-HC $O_3$, type water is chiefly influenced by gneiss and carbonate minerals in granite. F and Fe contents of $CO_2$-rich waters are abundant in $Na-HCO_3$, and $Ca-HCO_3$ types, respectively. The results of this study suggest that the chemical composition $CO_2$-rich water is mainly controlled by the mineralogical composition of aquifer host rocks. Oxygen and deuterium isotope data indicate that $CO_2$-rich water is meteoric origin. The $\delta^{13}$C values (-0.3$\textperthousand$ to -6.2$\textperthousand$ PDB) suggest that dissolved carbonates are mainly derived from a deep-seated $CO_2$ and partly from carbonate minerals.

A Study on Fire Explosion Characteristics via Physico-chemical Analysis of Petroleum Residues (석유 부산물의 물리화학적 분석을 통한 화재폭발 특성연구)

  • Kim, Hyeonggi;Lee, Young-Seak
    • Applied Chemistry for Engineering
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    • v.30 no.5
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    • pp.556-561
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    • 2019
  • In this study, the physical and chemical analyses of petroleum residues (pyrolized fuel oil, PFO) were conducted and major components were selected to investigate their fire and explosion characteristics. Major component distribution areas of the PFO were identified via the GC-SIMDIS and MALDI-TOF analyses. In addition, the qualitative analysis of major component distribution areas was performed by GC-MS analysis. Major components of pyrolysis residue were selected based on the results of various analyses such as EA, SARA and TGA. As a result, benzene, toluene and xylene were selected as major components. Finally, the process hazard analysis software tool (PHAST) analysis was performed to investigate the range of maximum damage effect in case of fire and explosion. Toluene presented the highest risk due to the radiation effect of $227kW/m^2$ and 118 m in the case of jet fire. Xylene and benzene showed the maximum radiant heat values of 114 and $151kW/m^2$, respectively. It was also confirmed from the analysis of pasquill stability and wind speed that the radiant heat increased up to 55% according to wind speed in benzene, which was considered to be a main factor increasing the influence range.

The Composition and Physico-chemcal Characteristics of school waste in B area, Kyunggi-do (경기도 B 지역 학교폐기물의 성상 및 물리∙화학적 특성)

  • Lee, Keon Joo
    • Journal of the Korea Organic Resources Recycling Association
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    • v.16 no.1
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    • pp.70-78
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    • 2008
  • In this study, the composition and physico-chemical characteristics of school waste which is located in B area, kyunggi-do was investigated. It is necessary to measure the characteristics of school waste to build the data-base for resource and recycling of waste. This school waste was composed of 12.25% of food wastes, 56.26% of papers, 9.26% of plastics&vinyls, 1.52% of textiles, 3.70% of wood, 0.11% of rubbers&leathers and others, respectively. Most of school wastes are mainly composed of paper and plastic waste and composition of combustible waste was about as 90%. From 3-components analysis, contents of moisture, combustible component, and ash was 5.72%, 88.29% and 5.98%, respectively. Moisture content was higher in Agricultural Dwelling school area compare to the urban dwelling school area. The chemical element of the school waste has the high order of carbon, oxygen, hydrogen on the dry basis of wastes and the low heating value of the MSW which is measured by calorimeter is shown as 3720.44kcal/kg.

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