• Journal of the Korean Society for Nondestructive Testing
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• v.22 no.2
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• pp.149-154
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• 2002

An attempt was made to evaluate the changes of microstructures and mechanical properties with increasing aging time in 2.25Cr-1Mo steel. In this study, it was verified the feasibility of the evaluation for degraded 2.25Cr-1Mo steel by isothermal heat treatment at $630^{\circ}C$ up to 1,000 hours using surface SH wave and investigated the change of attenuation coefficient and propagation time. Attenuation coefficient had a tendency to increase according to degradation and propagation time drastically in the beginning of deterioration. A good correlation between ultrasonic attenuation coefficient and hardness was found, which made sure that attenuation coefficient is an potential parameter for evaluation of aging degradation. In addition, it has verified experimentally the frequency dependence of ultrasonic group velocity and attenuation coefficient using wavelet transform.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.39 no.8
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• pp.759-763
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• 2015

The laser machining process has been proposed as an advanced process for the selective fabrication of electrodes without a mask. In this study, we adapt laser machining to metals that have different thermal properties. Based on the results, the metals exhibit a different surface morphology, heat-affected zone (HAZ), and a recast layer around the machined surface according to their thermal conductivity, boiling point, and thermal diffusivity. Then, we apply ultrasonic-assisted laser machining to remove the recast layer. The ultrasonic-assisted laser machining exhibits a better surface quality in metals with higher diffusivity than those having lower diffusivity.

• Journal of the Korean Society for Nondestructive Testing
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• v.20 no.5
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• pp.397-401
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• 2000

The corrosion-fatigue characteristics of the 12Cr steel, which is widely used in fossil power plants as a turbine blade material, are evaluated nondestructively by use of the Rayleigh surface wave. In this study, the frequency dependency of the Rayleigh surface wave is investigated indirectly by measuring the angular dependency of the backward radiation of the incident ultrasonic wave in the aged specimens, and then compared to the corrosion-fatigue characteristics. The width of the backward radiation profile decreases as the increase of the aging temperature, which seems to result from the increase of the effective degrading layer thickness. This parameter also shows an inversely proportionality to the exponent, m, in the Paris law which predicts the crack size increasement due to fatigue. The result observed in this study demonstrates high potential of the backward radiated ultrasound as a tool for the nondestructive evaluation of the corrosion-fatigue characteristics of the aged materials.

• Journal of the Korean Society for Nondestructive Testing
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• v.21 no.1
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• pp.32-38
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• 2001

Although the ultrasonic method has been developed and used widely in the fields, it has been used only for measuring the defect size and thickness loss. In this study, the relationship between surface wave attenuation through micro-crack growth and variation of velocity under repeated cyclic loading has been investigated. The specimens are adopted from 2.25Cr-1Mo steel, which is used for power plant and pipeline system, and have dimensions of $200{\times}40{\times}4mm$. The results of ultrasonic test with a 5MHz transducer show that surface wave velocity gradually decreases from the point of 60% of fatigue life and the crack length of 2mm with the increasing fatigue cycles. From the results of this study, it is found that the technique using the ultrasonic velocity change is one of very useful methods to evaluate the fatigue life nondestructively.

• Elastomers and Composites
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• v.40 no.4
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• pp.272-276
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• 2005

[ $C_{70}$ ]-gold nanoparticle multilayer films were self-assembled using a 'dirt-ball' method on the reactive surface of glass slides functionalized with 3-aminopropyltrimethoxysilane. The functionalized glass slides were soaked in the solution containing both unmodified $C_{70}$ and ${\omega}$-amino-functionalized gold nanoparticles. Organic reaction (amination) facilitated the assembly of multilayer $C_{70}$-gold nanoparticle films, which have grown up to several layers. Chemical stability of $C_{70}$-gold nanoparticle films was studied by monitoring the changes in absorbance after the immersion of the films in acidic solution. In addition, ultrasonic stability of these nanoparticle films was studied by exposing them to ultrasonic irradiated surrounding, which resulted in partial desorption and a little aggregation of nanoparticles on solid surfaces.

• Journal of the Korean Society for Nondestructive Testing
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• v.34 no.2
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• pp.171-175
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• 2014

In this study, we suggest a method to measure the thickness of thin films nondestructively using the dispersion characteristics of a surface acoustic wave propagating along the thin film surface. To measure the thickness of thin films, we deposited thin films with different thicknesses on a Si (100) wafer substrate by controlling the deposit time using the E-beam evaporation method. The thickness of the thin films was measured using a scanning electron microscope. Subsequently, the surface wave velocity of the thin films with different thicknesses was measured using the V(z) curve method of scanning acoustic microscopy. The correlation between the measured thickness and surface acoustic wave velocity was verified. The wave velocity of the film decreased as the film thickness increased. Therefore, thin film thickness can be determined by measuring the dispersion characteristics of the surface acoustic wave velocity.

• Applied Chemistry for Engineering
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• v.29 no.5
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• pp.503-509
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• 2018

In this study, we used the ultrasonic extraction process as a method to extract antioxidant substances from kudzu, and measured the content of iso-flavonoids puerarin, daidzein, daidzin contained in kudzu. The response surface methodology which is a statistical analysis method for optimizing the extraction amount of iso-flavonoids from the kudzu and the process condition for maximizing the yield was applied. It is the final objective of this study to effectively derive the condition of the process that matches the target response with a minimum number of experiments and analyze the effect of each process condition on the response. In the response surface methodology, the central composite design was applied and the optimum condition was analyzed, and the three independent variables were set to ultrasonic irradiation time, volume ratio of ethanol/ultrapure water, ultrasonic irradiation power. Using the response surface methodology, the optimum conditions with the maximum extraction yield and the content of iso-flavonoids were evaluated as ultrasonic irradiation time (24.75 min), ethanol / ultrapure water volume ratio (39.75 vol%), ultrasonic irradiation power (592.36 W). The overall satisfaction level appears as high as 0.8938, which is recognized at a significance level within 5%. As a result of analyzing the optimization process, it was confirmed that the ultrasonic irradiation time is the factor that most affects the responses.

• Bulletin of Food Technology
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• v.24 no.4
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• pp.605-612
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• 2011

• Proceedings of the Acoustical Society of Korea Conference
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• spring
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• pp.395-398
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• 1999

본 연구에서는 초음파현미경에서 다중의 동작주파스를 사용하여 얻어진 영상을 합성하여 깊이분해능이 개선된 초음파영상을 복원하는 방법을 연구하였다. 실험을 위하여 중심주파수가 5MHz이고 비대역폭이 $35\%$인 초음파변환기를 사용하여 초음파현미경을 구성하였다. 시편은 알루미늄을 이용하여 표면에 깊이가 $100{\mu}m$이고 지름이 2mm인 원형결함을 제작하였다. 실험결과, 동작주파수가 5MHz인 단일 주파수를 사용하여 얻어진 영상에서 결함이 존재하는 면과 그렇지 않은 면에 대한 콘트라스트가 0.098로 나타났다. 반면에 동작주파수를 $4.4MHz\~5.6MHz$ 범위에서 200kHz씩 변화시키면서 획득한 데이터를 합성하여 얻어진 영상에서 결함이 존재하는 면과 그러하지 않은 면에 대한 영상 콘트라스트가 0.398로 나타났다. 따라서 초음파현미경에서 다중의 동작주파수를 사용한 경우, 피사체의 깊이 변화에 대한 영상의 콘트라스트가 단일주파수를 사용한 경우에 비하여 개선되어 나타났으며 깊이분해능이 향상되었다. 앞으로의 과제는 초음파현미경에서 음향렌즈의 집속도 변화에 대한 적절한 동작주파수의 동작범위와 영상의 분해능과의 관계에 대한 연구가 계속되어져야 한다고 본다.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.11 no.6
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• pp.252-258
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• 2001

($Ba_{0.7}Sr_{0.3})TiO_3$thin films were perpared on ITO-coated glass substrate by spin-coating method. The sol was sonicated in an ultrasonic bath to promote homogenization and the results were compared with untreated case. By application of the sonication process, crystallization temperatures of films were reduced, microstructers of films were more uniform and denser and the surface roughness of the films was lower from 8.4nm to 5.6nm. In addition, optical transmittances and electrical properties of films prepraed from sonicated sol were superior to those of films from untreated.