• Title/Summary/Keyword: 표면초음파

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액체/초임계 이산화탄소의 QCM을 이용한 초음파 세척 효과 연구

  • 박광헌;고문성;윤청현;김홍두;김학원
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2002.05a
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    • pp.2-2
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    • 2002
  • Quartz Crystal Microbalance(QCM)은 표면에 묻은 물질의 미량의 무게변화도 간단히 측정 할 수 있어 반웅기 내에서 일어나는 현상올 in-situ로 즉시 알 수 있는 장점을 가진 장치이 다. 이 장치를 이용하면 초엄계 이산화탄소 내에서 용해도를 알 수 있고, 대상물질이 녹아냐 가는 속도를 측정하면 확산계수를 구할 수 있다. 그리고, 초음파 혼을 반응용기 내에 설치하 고, 초음파 효과를 알아보았다. 먼저 static system에서 초음파 효과를 알아보았다. Cu(acac)2를 대상으로, 밀폐된 용기에서 수행한 실험에서, 액체와 초임계 이산화탄소 내에서 용해속도를 QCM으로 구할 수 있었다. 용해속도로부터 Cu(acac)2의 확산계수를 측정할 수 있었다. 액체 내에선 $10^{-4}{\;}cm2/sec$, 초임계상태에서 $10^{-2}{\;}cm2/sec$의 값을 갖는 것으로 나타 났다. 그리고, 초음파를 사용할 경우 이 확산계수값이 4-5배정도 증가하는 것으로 냐타났다. 이어서 dynamic system에서 반응을 알아보았다. Cyanex를 함유한 C02를 반응용기에 흘리 면서 QCM표면에 묻은 Co이온의 용해속도를 측정하였다. 초음파는 용해도에 아무 역활을 안하는 것으로 나타났다. 주어진 조건에서 13 microgram/gram-cyanex의 용해도를 갖는 것 으로 나타났다.

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Detection of a Surface-Breaking Crack Using the Surface Wave of a Laser Ultrasound (레이저 초음파의 표면파를 이용한 표면결함 측정)

  • Park, Seung-Kyu;Jung, Hyun-Kyu;Baik, Sung-Hoon;Lim, Chang-Hwan;Joo, Young-Sang;Kang, Young-June
    • Journal of the Korean Society for Nondestructive Testing
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    • v.26 no.2
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    • pp.84-89
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    • 2006
  • A laser ultrasonic inspection system is a non-contact inspection device which generates and measures ultrasounds by using laser beams. A laser ultrasonic inspection system provides a high measurement resolution because the ultrasonic signal generated by a pulse laser beam has a wide-band spectrum and the ultrasonic signal is measured from a small focused spot of a measuring laser beam. In this paper, we have investigated the detection techniques of a surface-breaking crack by using the laser ultrasonic surface waves. A crack acts as a low pass filter whose cut-off frequency is lowered in proportion to the depth of a crack. And, the center frequency value of a spectrum is decreased in proportion to the depth of a crack. In this paper, we extracted the crack information by using the frequency attenuation from the normalized transfer function spectrum of a surface-breaking crack. Also, we effectively measured the crack depth by using the decreasing value of the center frequency from a crack passed ultrasonic signal. The proposed measuring techniques of crack depths provided more precise information than the amplitude measuring technique.

Power Supply of Ultrasonic Phased Array for Focus Control of Acoustic Pressure (음압 초점제어를 위한 초음파 위상배열의 전원 장치)

  • Jung, Hyung-Jon;Kim, Ui-Young;You, Bum-Jae;Choy, Ick
    • The Journal of the Korea institute of electronic communication sciences
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    • v.14 no.1
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    • pp.137-146
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    • 2019
  • The ultrasonic phased arrays are used for treating tumors in the human body by the focus control of the acoustic pressure at the desired position. The magnitude and phase of the surface acoustic pressure in each ultrasonic transducer is controlled by the magnitude and phase of the applied voltage to it. In this paper, the relationship between the applied voltage and the surface acoustic pressure of the ultrasound transducer is modelled, and the desired voltage is realized by PWM technique. The validity of the proposed method is verified by computer simulation of the focus control of a ultrasonic phased array composed of 61 ultrasonic transducers.

Ultrasonic Backward Radiation on Randomly Rough Surface (무작위로 거친 표면에서의 후방복사 초음파)

  • Kwon, Sung-D.
    • Journal of the Korean Society for Nondestructive Testing
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    • v.25 no.1
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    • pp.9-14
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    • 2005
  • The angular dependence(profile) of backward radiated ultrasound was measured for glass specimens with random surface roughness using ultrasonic goniometer that ran changes the incident angle continuously. It was concluded that the roughened region had greater acoustic impedance than the unperturbed region. The comparison of backward radiations showed that the amplitude of peak and the area of radiation profile were increased with surface roughness. It was suggested from the sensitive dependence of the profile area that the profile of backward radiation could be applied to in the nondestructive evaluation of sulfate region. Inclined C-scan technique with the transducer inclined at Rayleigh angle showed the reverse of luminosity and the high signal to noise ratio so that it provided high resolution.

Effects of sonication on physicochemical properties and pore formation of maize starch (초음파처리가 옥수수전분의 이화학특성과 기공 형성에 미치는 영향)

  • Choi, Eun-Hee;Lee, Jae-Kwon
    • Korean Journal of Food Science and Technology
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    • v.49 no.5
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    • pp.507-512
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    • 2017
  • The physicochemical properties of maize starch sonicated at various amplitudes (100, 200, and 300 W) and times (10, 30, and 50 min) were examined. The amount of enzyme-susceptible starch increased marginally after sonication. Sonication increased the amount of oil absorbed in the starch although the degree of oil absorption decreased with an extension of the sonication time, implied that different types and extent of damages occurred. Scanning electron microscopy revealed that ultrasound sonication did not form pores on the surfaces, but caused damages such as depression and erosion. Pasting viscosity of starch decreased with an increase in the severity of sonication conditions because of the weakened polymer network. X-ray diffraction suggested that the crystalline domains in starch were not susceptible to sonication and were more resistance to degradation. Sonicated starch formed more pin-holes on the surfaces in the initial glucoamylase reaction; subsequently, as the reaction proceeded, porous starch with enlarged pores was formed and finally, disrupted granular fragments were observed.

Evaluation of Elastic Properties and Analysis of Contact Resonance Frequency of Cantilever for Ultrasonic AFM (초음파원자현미경 캔틸레버의 동특성 해석과 탄성특성 평가)

  • Park, Tae-Sung;Kwak, Dong-Ryul;Park, Ik-Keun;Kim, Chung-Seok;Jhang, Kyung-Young
    • Journal of the Korean Society for Nondestructive Testing
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    • v.31 no.2
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    • pp.174-180
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    • 2011
  • Nondestructive surface imaging of elastic characteristic and mechanical property has been studied on nanoscale surface with ultrasonic AFM. Resonance frequency variation of cantilever is theoretically analyzed with respect to contact mechanics as well as experimentally measured. The contact resonance frequency is calculated theoretically using the spring-mass and Herzian model in accordance with the resonance frequency of UAFM cantilever measured experimentally. Consequently, the topography and amplitude images could be obtained successfully and the elastic characteristic at the nanoscale surface was evaluated qualitatively by amplitude signals.

A Study on the ultrasonic wave-assisted pd activation for electroless Ag plating (무전해 은도금시 팔라듐 활성화 단계에서의 초음파의 영향 고찰)

  • Lee, Chang-Myeon;Lee, Hong-Gi;Heo, Jin-Yeong;Lee, Min-Hyeong;Lee, Ho-Nyeon
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2011.05a
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    • pp.149-150
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    • 2011
  • 미세화된 반도체 배선에 무전해 은도금을 적용하고자 새로운 Pd 활성화 공정을 제안하였다. 시편 표면에 작은 크기의 Pd 입자를 균일하게 분포시키기 위하여 Pd 활성화 도중 초음파을 가하였다. 추가적인 무전해 은 도금을 실시하여, 초음파에 의한 Pd 입자 분산이 은도금 피막 형성에 미치는 영향에 대하여 고찰하였다.

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Granite Strength Estimation of Construction Considering Surface Roughness Effect on Ultrasonic Velocity Method (화강석 건조물의 표면 거칠기별 초음파속도법에 의한 강도 추정)

  • Kim, Jeong-Sup;Shin, Yong-Seok;Kim, Jeong-Hoon
    • Journal of the Korea Institute of Building Construction
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    • v.10 no.1
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    • pp.137-145
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    • 2010
  • The mechanical properties of stone structures are generally characterized according to the strength of the stone used. An ultrasonic velocity method that does not damage cultural heritages is used to measure the strength of stone. However, there is no correction involved for surface roughness and thickness of the stone in the ultrasonic method currently used. In addition, a contact agent such as grease can cause contamination on the surface of a cultural heritage. Accordingly, this study suggests an indirect method of strength estimation formula for stone structures based on the surface roughness of the structure, its thickness, and the type of contact agent. (1) Rock strength estimation formula using ultrasonic velocity method of dabbed finish : $f_{su}=30.51\;Vp^{0.82}(R^2=95)$ (2) Rock strength estimation formula using ultrasonic velocity method of harsh finish : $f_{su}=61.52\;Vp^{0.32}(R^2=92)$.

The Evaluation Technique of Surface Region using Backward-Radiated Ultrasound (후방 복사된 초음파를 이용한 표면 지역의 평가 기술)

  • Kwon, S.D.
    • Journal of the Korean Society for Nondestructive Testing
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    • v.16 no.4
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    • pp.241-250
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    • 1997
  • The velocity dispersion of surface acoustical wave(SAW) of Si layer/mesh Au/Si substrate was measured by the frequency analysis technique of backward radiation at liquid/solid interface. The difference of backward radiation patterns depending on used transducers (2, 5, 10MHz) confirmed that the backward radiation phenomenon was caused by the energy radiation from SAW generated in surface region. An ultrasonic goniometer was constructed to measure continuously the angular dependence of backscattered intensity. The angular dependences of backward radiation(5MHz) were measured for Ni layer/Al substrate specimens that were bonded by epoxy involving different content of Cu powder. It was known that the width and pattern of backward radiation had informations such as the velocity dispersion, bonding quality and structure of surface region.

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Elastic Imaging of Material Surface by Ultrasonic Atomic Force Microscopy (초음파 원자 현미경을 이용한 재료 표면의 탄성 이미지화)

  • Kim, C.S.;Park, Tae-Sung;Park, It-Keun;Lee, Seung-Seok;Lee, C.J.
    • Journal of the Korean Society for Nondestructive Testing
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    • v.29 no.4
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    • pp.293-298
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    • 2009
  • The ultrasonic atomic force microscope(UAFM) has been developed in order to enhance the characterization technology for nano-scale surface combining ultrasonic property to atomic force microscope. This UAFM technique enables elasticity imaging due to the physical properties on the heterogeneous surface in addition to the novel topography of surface height in the nano-surface layer. In this study, the prototype UAFM system was constructed and applied to several materials, silicon deposited wafer, spherodized cold heading steel, and carbon fiber reinforced plastic specimen. Clear elastic contrast was successfully obtained using this developed prototype UAFM.