• Journal of the Korean Chemical Society
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• v.15 no.4
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• pp.191-197
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• 1971

Ruthenium content in highly purified palladium metal (99.9%) was determined by counting $^{105}Rh$ nuclide which was produced by $^{104}Ru(n,{\gamma};{\beta}^-)^{105}Rh$ nuclear reaction. Palladium sample and ruthenium standard were irradiated by neutron with the Pneumatic Transfer System of TRIGA MARK II reactor. Palladium and ruthenium were dissolved by treating with aqua-regia and by fusing with sodium peroxide flux respectively. $^{105}Rh$ was separated through anion and cation exchange resin columns. The ruthenium content was determined by comparing the $^{105}Rh$ activities, obtained from the palladium sample, with that from pure ruthenium standard. The detection limit of ruthenium by the present method is about 1 ppm of ruthenium in 10 mg of palladium, which is approximately 40 times more sensitive than that of the conventional radioactivation method which employs $^{102}Ru(n,{\gamma})^{103}Ru$ nuclear reaction.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.20 no.12
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• pp.418-424
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• 2019

The present study investigated the effects of the moment arm length on balance and walking when carrying a backpack. In total, 30 normal adults without orthopedic and neurological injuries were assessed. For each subject, balance and gait were measured under three conditions: 1) the no backpack condition, 2) the general backpack condition, and 3) the decreased length of moment arm backpack condition. There were significant differences in the center of the pressure area and velocity between the three conditions, whereas there was no significant difference in the center of the pressure area and velocity according to the moment arm length. There were significant differences in double limb support time and walking velocity under the three conditions, and there was a significant difference only in double limb support time according to the moment arm length. The results of the present study showed that a change in the length of the moment arm can be helpful for walking when carrying a backpack.

• The Journal of the Korea Contents Association
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• v.10 no.4
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• pp.375-385
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• 2010

The purpose of this study is to examine the influence of the fellowship of an organization empowerment of security officers. By using stratified cluster random sapling, 264 people from private security enterprises which are located in Seoul, 2009, were selected as final samples. However, the cases used in the final analysis were counted as 238. The reliability of the questionnaire used in the study was measured by Cronbach's $\alpha$ statistics, being over .761. The collected data were analyzed by factor analysis, reliability analysis, t-test, F-test, and multiple regression etc., using SPSSWIN 17.0. The conclusions were drawn as following. First, there are difference in fellowship according to the demographic characteristics of security officers. Second, there are difference in organization empowerment according to the demographic characteristics of security officers. Third, the fellowship of security officers affects an organization empowerment. That is to say, when vigorous and active participation, and independent and critical thinking are perceived more highly, the intensity of influence, meaning, capability, and self-determination increase.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.35 no.11
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• pp.1391-1398
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• 2011

Biomechanical analysis of arm motion during steering was performed using a motion analysis technique. Three-dimensional position data for each part of arm are fed into an interactive model combining a musculoskeletal arm model and the mechanical steering system to calculate joint angles and torques using inverse kinematic and dynamic analyses, respectively. The analysis shows that elbow pronation/supination, wrist flexion/extension, shoulder adduction/abduction, and shoulder flexion/extension have significant magnitudes. Sensitivity analysis of the arm joint motion with respect to seating posture and steering wheel configuration is carried out to investigate the qualitative influence of the seating posture and driver's seat configuration on the steering behavior.

• Journal of the Korean Society of Food Science and Nutrition
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• v.31 no.2
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• pp.184-188
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• 2002

The fatty acid contents of egg yolk from various chicken eggs such as general egg, ginseng egg, gamgoal egg and docosahexaenoic acid (DHA) egg were analysed during storage at 4$^{\circ}C$ for 3 weeks. The major fatty acids of all egg yolk oils were oleic acid (18 : 1) and palmitic acid (16 : 0). The contents of both fatty acids reached maximum at the first or second week and decreased at the third week. DHA was detected from 4 kinds of eggs stored for 2 or 3 weeks. The n-6/n-3 ratio was obtained under recommended intake range in fresh gamgoal egg and in general and DHA eggs stored far 0~3 weeks. For 3 weeks, polyunsaturated fatty acid / monounsaturated fatty acid/ saturated fatty acid (P/M/S) ratio of DHA e99 did not chance, but that of ginseng e99 gradually increased. The P/M/S ratio was generally maintained under recommended intake range in general egg stored for 3 weeks, in ginseng egg stored for 2 weeks and in DHA egg during all the storage period.

• The Journal of Korean Academy of Orthopedic Manual Physical Therapy
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• v.15 no.1
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• pp.79-85
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• 2009

목적 : 브라운시쿼드는 대부분 척추손상과 수질외 척추 종양에서 주로 나타난다. 드물게 경추 디스크가 브라운시쿼드의 원인이 된다. 경추디스크에 의한 브라운시쿼드 증세의 수술후 물리치료 및 도수치료 결과를 보고하기 위함이다. 방법 : 50세 남자로써 브라운시쿼드 증세로 진단을 받고 수술후 좌측 팔과 다리에 운동신경에 의한 마비증세가 있었으며(팔>다리), 우측으로 감각과 온도감각이 저하된 경우이다(팔>다리). 측정방법은 통증지수(VAS), 근력(Distal PowerTracII$^{TM}$ test), 지구력(Ergometer) 측정과 심리상태(설문)를 치료전과 후를 비교하였다. 물리치료에서는 기능적 전기자극 치료와 도수치료 및 운동치료 방법을 실시하였다. 도수치료는 통증완화와 근력강화를 위한 MET, MFR, Mobilization 등을 실시하였으며, 운동은 슬링시스템 등을 이용한 운동과 견관절의 불안정을 위해 안정화운동을 실시하였다. 결과 : 이 케이스는 수술후 이상 징후가 척수압박으로 인하여 보다 넓게 통증이 나타났으며, 운동 및 감각신경이 둔해지고 온도에 대한 감각이 반대편 결손으로 나타났으며, 좌측 어깨, 팔 견갑부의 근육 마비와 우측의 감각이 떨어진 현상이 나타났다. 물리치료 후 단기목표와 장기목표에 있어서 통증과 운동 및 감각 기능이 회복되어 각각 팔 통증에서는 VAS 8 ${\rightarrow}$ 1, 상지 하지의 운동기능은 Trace ${\rightarrow}$ Good 로 평가 회복되었으며, 근력측정에서 모두 유의한 차이를 보였다. 모든 치료과정 결과에서 심리적 상태의 설문에서도 높은 점수를 얻어 긍정적 신뢰가 높아 진 것으로 나타났다. 검사결과 다리의 근력이 증가는 걷기 운동 및 에르고메터의 지구력 및 균형이 레벨1의 10분 수행능력이 레벨 20에서 30분 수행능력으로 향상되어 일상적인 활동이 가능해졌다. 결론 : 예상하지 못했던 수술 후유증(side effects)에 대한 치료과정이 환자의 심리에 심각한 부정적인 생각이 신체의 기능과 감정의 손상에 영향을 미치기 때문에 체계적이고 장기적인 치료 과정에서 기능적 향상과 더불어 정신적인 심리의 정서 안정이 매우 필요하다고 사료된다.

• Resources Recycling
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• v.26 no.3
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• pp.26-31
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• 2017

LIX 63 showed a selectivity for the extraction of Pd(II) over other PGMs, such as Pt(IV), Ir(IV) and Rh(III) from 6 M HCl solution. Moreover, HCl solution has significant effect on the oxidation-reduction reaction between Ir(IV) and LIX 63. Therefore, the applicability of employing LIX 63 for the separation of the 4 PGMs was investigated from 3 M HCl solution. From 3 M HCl solution, only Pd(II) was selectively extracted by LIX 63 and its extraction percentage was higher than from 6 M HCl solution. Extraction of the Pd(II) free raffinate with TBP led to the selective extraction of Pt(IV). After oxidation of Ir(III) with $NaClO_3$ to Ir(IV), extraction of the Pt(IV) free raffinate with Aliquat 336 selectively extracted Ir(IV). For each extraction step, optimum stripping conditions were obtained. By this process, it was possible to separate the 4 PGMs by solvent extraction from 3 M HCl solution.

• Journal of Digital Convergence
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• v.14 no.7
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• pp.73-81
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• 2016

This study examined the effects of followership characteristics on LMX, knowledge sharing, job satisfaction and turnover intention for coffee speciality store members. 317 questionnaire samples are used to test 4 hypotheses using structural equation model with AMOS. Results of hypotheses testing are as follows: First, goal congruence and active participation factors of followership characteristics influence positively LMX. Second, LMX influences positively knowledge sharing, and knowledge influences job satisfaction and turnover intention. This study emphasizes the importance of knowledge sharing in coffee speciality store members relations. In addition, this study shows that followership, LMX, knowledge sharing are important for members' increasing job satisfaction and decreasing turnover intention, and human resource management. Implications and limitations of this study were also suggested.

• Journal of Digital Convergence
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• v.15 no.2
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• pp.411-419
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• 2017

This study was to investigate whether a trunk correction taping plus scapular setting exercises has an effect on trunk muscle activation and trunk balance and upper extremity function in patients with stroke. Twenty stroke patients were randomly divided into a trunk correction taping with scapular setting exercise group (n=10) and a scapular setting exercise group (n=10), and each group performed given interventions for 30 minutes for 4 weeks. In the experimental group, there were significant increases in muscle activation, K-TIS, and MFT (p<.05), and a significant improvement was detected in K-TIS and MFT compared to the control group (p<.05). This study suggests that a trunk correction taping with scapular setting exercises was more effective on trunk muscle activation, trunk balance, and upper extremity function in stroke patients compared to a scapular setting exercise. It could be clinically more significant if the change in the onset time of muscle activity is confirmed in the further researches.

• Journal of the Korean Chemical Society
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• v.37 no.4
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• pp.423-430
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• 1993

New Palladium(0)-olefin complexes, $(PMe_3)_2Pd{CH_2=C(CH_3)COOH} \;and\;(PMe_3)_2Pd{(CH_3)CH=CHCOOH}$ have been prepared by treating $Pd(PMe_3)_2$(styrene) with methacrylic acid and trans-crotonic acid, respectively. These complexes were characterized by elemental analysis, IR and $^1H-,\;^{13}C-,\;and\;^{31}P$-NMR spectroscopy. The carboxylic acid entity was found non-bonded with palladium while ${\pi}$-bond is formed between the olefin double bond and Pd(0). The results are compared with the metallacycle formation the reaction of Pd(PMe3)2(styrene) with 3-butenoic acid.