• 제목/요약/키워드: 탈자화

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Sputering Pressure and Temperature Effects on Magnetization Reversal Behaviors of $Co(2\AA)/Pd(13\AA)$ Multilayers (스퍼터링압력 및 온도 효과에 의한 $Co(2\AA)/Pd(13\AA)$ 다층박막의 자화반전 거동)

  • 김성봉;정순영
    • Journal of the Korean Magnetics Society
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    • v.6 no.4
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    • pp.199-203
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    • 1996
  • To study the magnetization reversal behavior of Co/Pd multilayers, we first demagnetized the samples by the field-demagnetized method and then measured initial curves and minor loops. The coercivity and the perpendicular magnetic anisotropy were obtained from the perpendicular and parallel magnetization curves measured at different temperatures. We interpret our experimental results by applying several qualitative and semiquantative approaches. From these study, we found that the magnetization reversal behavior is dominated by the domain wall pinning for all samples and the coercivity incremental tendency can be explained by Kronmuller's formula $H_c(T)\;{\propto}\;r_0.K_u$.

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Demagnetization to Induce Vertical Magnetization in a Military Vessel (함정에 수직자화를 부여하기 위한 탈자)

  • Kim, Young-Hak
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2015.10a
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    • pp.1109-1112
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    • 2015
  • A milatary ship without degaussing coil has a vertical magnetization to compensate magnetization induced by the vertical magnetic field component of earth magnetic field during demagnetization process. Flash D is very useful to acquire vertical magnetization. However this is hard to predict vertical magnetization. This experiment was investicated on another method, which used the only vertical bias magentic field. The specimens were prepared by thin Zn coated steel sheet with a thickness of 0.15mm. The shapes of 3 specimes was rectangular, triangular and circular cylinders. These shapes were corresponded to the shapes of bow, mid and stern of a vessel. Through FEM analysis, the difference of magnetic signatures for these specimens was recognized and the residual magnetization curve was measured. magnetic field was generated by a solenoid coil and magnetic signature was measured by a magnetic field sensor. A linearity between a vertical bias magnetic field and a vertical manetzation existed and the vertical magnetization of a miltary vessel was predicted by the linearity.

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A Study on the magnetization of metal orthopedic prosthesis in magnetic resonance imaging (자기공명 영상장치에서 정형보철금속의 자화(磁化)에 관한 연구)

  • Kim, Hyeong-Gyun;Song, Duk-Chung;Choi, Seong-Dae
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.12 no.4
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    • pp.34-39
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    • 2013
  • For orthopedic artificial metal stainless steel, the magnetization of the magnetic field due to the presence of the titanium was to observe the change. Magnetic field meter (Tesla meters) a certain distance (ISO Centre) 1.5 Tesla magnetic field, the magnetization in the center with the passage of time were measured. Therefore, these artificial metal clip shape and magnetization of the sample size to produce a ferromagnetic material for comparison is the experimental dependence. For comparison of the experimental dependence of the magnetization, thereby producing a test piece size such as shaping prosthetic metal Clip is a ferromagnetic material. The experimental results, the metal orthopedic implants, there was no change in the magnetization indicated by ferromagnetic material in its natural state. However, in a magnetic field of 1.5T (Tesla), showed a sensitivity that is magnetized rapidly compared to the ferromagnetic material. In conclusion, high in the order of Clip, Stainless, of Titanium, the degree of dependence of the magnetization intensity of magnetization was the order Stainless, Titanium, of Clip in a magnetic field.

Effects of Residual Magnetization on MEL Non-destructive Inspection of Gas Pipeline (가스관의 자속누설탐사에서 잔류자화의 영향에 관한 연구)

  • Jang, Pyung-Woo
    • Journal of the Korean Magnetics Society
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    • v.14 no.4
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    • pp.143-148
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    • 2004
  • Effects of residual flux density M$_{res}$ and number of inspection on the detection voltage and flux density B of the gas pipeline were investigated in MFL inspection, which is widely used for the non-destructive inspection in a gas pipeline. A simulation equipment composed of the magnetizer and iron ring attached on an aluminum disc was constructed instead of a huge gas pipeline facility. With this system. the iron ring could be perfectly demagnetized and signals from the bolt screw stuck on the disc could be clearly detected so that the effects of M$_{res}$S and the inspection number on the detection voltage and B of iron ring were effectively investigated. With increasing the number of inspection, M$_{res}$, B of the iron ring and the detection voltage decreased and then kept at constant values while final M$_{res}$ increased with increasing initial M$_{res}$. If inspection condition were kept unchanged, the detection voltage was proportional to the last M$_{res}$ of the iron ring instead of B. This was probably due to magnetic hysteresis of the iron ring inherited from magnetic domain so that consideration on the magnetic hysteresis was inevitable in the analysis of MFL signal from defects of a gas pipeline. A new inspection scheme using the magnetizer with reversed magnetization in the subsequent inspection was proposed from the result that a high detection voltage could be obtained in the first inspection of gas pipeline with positive M$_{res}$.

Exchange Decoupling Of $Fe_3$Fe_3B+Nd_2Fe_{14}B Spring Magnet Powder Compact (Fe_3B+Nd_2Fe_{14}B Spring magnet분말 압분체의 Exchange Decoupling)

  • 한종수;양충진;박언병
    • Journal of the Korean Magnetics Society
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    • v.11 no.5
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    • pp.232-238
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    • 2001
  • Experimentally it is well known that the magnetic properties significantly deteriorate when nanocomposite bonded magnet are made from nanocomposite ribbon. A decrease in maximum energy product of F $e_3$B+N $d_2$F $e_{14}$B nanocomposite from 14 MGOe in nanocomposite ribbon to 6.5 MGOe in powder compact was fecund to be general. Thus, the present study is focused on finding out the root of exchange decoupling of N $d_4$F $e_{73.5}$ $Co_3$H $f_{0.5}$G $a_{0.5}$ $B_{18.5}$ nanocomposite powder compacts. The exchange decoupling behavior of the powder compact of F $e_3$B+N $d_2$F $e_{14}$B composition was studied by measuring DC demagnetization and isothermal remanent demagnetization curves, which are essential for plotting produced $\delta$M curve. From the $\delta$M plot the deterioration in the magnetic properties resulted from the fact that the magnetostatic interaction became dominant rather thanthe exchange interaction in powder compact. It is concluded that the demagnetization behavior governed by the dominant magnetostatic interaction reduced the remanence magnetization, which caused the reduction of maximum energy Product of the powder compact. We also found that the elimination of residual stress which is unavoidably accumulated during grinding process enhanced the magnetic properties considerably.bly.bly.

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The Kinetics of Delignification in Oxygen·Alkali pulping (효소(酵素)·알칼리 증해(蒸解)의 탈(脱)리그닌에 관(関)한 동역학적(動力學的) 분석(分析))

  • Jo, Byoung Muk;Shin, Dong So
    • Journal of Korean Society of Forest Science
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    • v.56 no.1
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    • pp.26-50
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    • 1982
  • In order to obtain more detailed information concerning the degradation of lignin in the oxygen alkali pulping single stage isothermal delignification of pine wood meal (Pinus koraiensis S. et Z.) was studied in the oxygen alkali system at five temperature level ($110^{\circ}C$, $120^{\circ}C$, $130^{\circ}C$, $140^{\circ}C$, $150^{\circ}C$) for 60 min.. The rate constant, activation energy, oxygen and alkali consumption during the oxygen alkali delignification were determined by the kinetic method. The 2/5 of total lignin was eliminated at the start of the reaction. The delignification rate constant was about 3 times that of caustic soda pulping. The activation energy was about 1/3 lower than in caustic soda pulping. Like oxygen consumption, alkali consumption was also rapid early at the reaction and almost ceased after about 10 min.. The degradation reaction of lignin was strongly dependent upon the pH decrease of the cooking liquor by organic acid generated in pulping. The lignin in the oxygen alkali pulping degraded into lover molecular weight and had more hydrophillic properties. The methoxyl group decreased considerably at the first of oxygen alkali delignification, while the carbonyl, carboxyl and phenolic hydroxyl group increased rapidly.

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A Study on the Deperm of Ferromagnetic Material using Preisach Model (Preisach 모델을 이용한 강자성체의 탈자기법 연구)

  • Ju, Hye Sun;Park, Gwan Soo;Won, Hyuk
    • Journal of the Korean Magnetics Society
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    • v.23 no.2
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    • pp.54-61
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    • 2013
  • Ferromagnetic material's residual magnetization is remained because of the interaction between domains from external apply field, so the electrical and electronic industry and area of defense development request deperm protocol which makes the residual magnetization to 0. But the deperm protocols which are used theses days are developed by using only experience and experiment, so we have to develop deperm protocol considering hysteresis curve. In this paper, Anhysteretic Deperm, Deperm-ME, Flash-Deperm were analyzed using two dimensional finite element method and Preisach model that was formulated by property of magnetic materials. From that analysis, the relations between hysteresis curve and deperm variable are compared by analyzing the trace of Preisach plane. Also, an efficient current ratio of deperm protocol, is proposed.

Precessional Motion of Ferromagnetic Pt/Co/Pt Thin Film with Perpendicular Magnetic Anisotropy (수직 자기 이방성을 갖는 Pt/Co/Pt 자성 박막의 세차 운동 측정 및 분석)

  • Yun, Sang-Jun;Lee, Jae-Chul;Choe, Sug-Bong;Shin, Kyoung-Ho
    • Journal of the Korean Magnetics Society
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    • v.21 no.6
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    • pp.204-207
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    • 2011
  • We developed a time-resolved magneto-optical Kerr effect microscope system to investigate ultrafast magnetization dynamics. Based on the pump-probe method, 0.1-ps time resolution was achieved by use of a fs Ti:Sapphire laser. The magnetization dynamics was then measured on Pt/Co/Pt thin films with various Co thicknesses. All the samples exhibited ultrafast demagnetization within a few ps by direct heating of pump laser. Some thicker samples showed precessional motion of magnetization, from which the Gilbert damping constant was determined based on the Landau-Lifshitz-Gilbert equation.

Biomodification of Ethanol Organolsolv Lignin by Abortiporus biennis and Its Structural Change by Addition of Reducing Agent (Abortiporus biennis에 의한 유기용매 리그닌의 생물학적 변환과 환원제 첨가에 따른 구조 변화)

  • Hong, Chang-Young;Park, Se-Yeong;Kim, Seon-Hong;Lee, Su-Yeon;Ryu, Sun-Hwa;Choi, In-Gyu
    • Journal of the Korean Wood Science and Technology
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    • v.44 no.1
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    • pp.124-134
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    • 2016
  • The main goal of this study was to investigate biomodification mechanism of lignin by white rot fungus, Abortiporus biennis, and to depolymerize ethanol organosolv lignin for industrial application. In nitrogen-limited culture, A. biennis polymerized mainly lignin showing a rapid increase of molecular weight and structural changes depending on incubation days. At the initial incubation days, cleavage of ether bonds increased phenolic OH content, while the results were contrary in of the later part of the culture. Based on these results, ascorbic acid as a reducing agent was used to induce depolymerization of lignin during cultivation with white rot fungus. As a result, the degree of increase of average molecular weight of lignin was significantly declined when compared with those of the ascorbic acid free-experiment, although the molecular weight of fungus treated sample slightly increased than that of control. Furthermore, lignin derived oligomers in culture medium were depolymerized with the addition of ascorbic acid, showing that the average molecular weight was 381 Da, and phenolic OH content was 38.63%. These depolymerized lignin oligomers were considered to be applicable for industrial utilization of lignin. In conclusion, A. biennis led to the polymerization of lignin during biomodification period. The addition of ascorbic acid had a positive effect on the depolymerization and increase of phenolic OH content of lignin oligomers in medium.

A Study on Decrease in Degree of Deacetylation of Low Molecular Weight Chitosan Prepared by H2O2 and Change of Whiteness upon Time (H2O2로 분자량이 조절된 저분자화 키토산의 탈아세틸화도와 백도변화에 관한 연구)

  • Kim, Hee-Jung;Jeon, Dong-Won
    • Fashion & Textile Research Journal
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    • v.5 no.5
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    • pp.529-538
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    • 2003
  • Chitosan should be satisfied a certain Mw range for the final application, Low molecular weight chitosan(LMWC) can be acquired by depolymerizing high molecular weight starting chitosan. Using $H_2O_2$ in depolymerizing chitosan is very effective and reproducible in controlling Mw of resulting LMWC. However, $H_2O_2$ can break glycoside linkage of chitosan and oxidize some $-NH_2$ groups in chitosan. It has been reported that decrease in DA(degree of deacetylation) of LMWC prepared by $H_2O_2$. However, any quantitative data of decrease in DA has not been reported yet. In this study, DA of initial chitosan and DA of $H_2O_2$ treated chitosan were measured and the change in DA of chitosan upon $H_2O_2$ treatment were investigated. Change in DA was very different upon $H_2O_2$ treatment condition. LMWC also showed DA change upon time passage. Pre-swelling treatment of initial chitosan and low ratio of $H_2O_2$/chitosan prevented a decrease in DA significantly. Yellowing of LMWC was detected upon time passage, however, decrease in DA was minimal (around 1%).