• Journal of Powder Materials
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• v.29 no.5
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• pp.418-423
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• 2022

Carbon fibers (CFs) are considered promising composite materials for various applications. However, the high cost of CFs (as much as $26 per kg) limits their practical use in the automobile and energy industries. In this study, we developed a continuous stabilization process for manufacturing low-cost CFs. We employed a textile-grade polyacrylonitrile (PAN) fiber as a low-cost precursor and UV irradiation technique to shorten the thermal stabilization time. We confirmed that UV irradiation on the textile-grade PAN fibers could lower the initial thermal stabilization temperature and also lead to a higher reaction. These resulted in a shorter overall stabilization time and enhancement of the tensile properties of textile-grade PAN-based CFs. Our study found that only 70 min of stabilization time with UV irradiation was required to prepare textile-grade PAN-based low-cost CFs with a tensile strength of 2.37 ± 0.22 GPa and tensile modulus of 249 ± 5 GPa.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2011.11a
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• pp.307-311
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• 2011

This paper is concerned with anisogrid composite lattice structures whose load bearing shell is formed by systems of geodesic unidirectional composite ribs made by automatic wet winding process. Lattice structures are usually made in the form of conical shell and consist of systems of helical and hoop ribs fabricated by continuous filament winding from carbon and epoxy composites. Design variables of the structure which are the angle of helical ribs and ribs spacings are determined by cone geometry and geodesic line. and Fabrication methods for the conical composite lattice structure are presented.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2010.05a
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• pp.421-427
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• 2010

This paper is concerned with Anisogrid composite lattice structures whose load bearing shell is formed by systems of geodesic unidirectional composite ribs made by automatic wet winding process. Lattice structures are usually made in the form of cylindrical shell and consist of systems of helical and hoop ribs fabricated by continuous filament winding from carbon and epoxy composites. Design variables of the structure which are the angle of helical ribs, ribs spacings, and cross sectional areas are determined by the method of minimization of satety factors whick is described in the paper. And, fabrication methods and actual experimental results are presented.

• Composites Research
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• v.30 no.2
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• pp.116-125
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• 2017

The purpose of this study is to develop silicon carbide fiber showing an excellent mechanical properties under highly oxidative conditions at high temperature. Polycarbosilane(PCS) as a preceramic precursor was used for making the SiC fiber. PCS fiber was taken by melt spinning method followed by melting the PCS at $300{\sim}350^{\circ}C$ in N2 gas. The Curing of PCS fiber was carried out in air oxygen chamber, prior to high temperature pyrolysis. Degree of cure was calculated by characteristic peak's ratio of Si-H to $Si-CH_3$ in FT-IR spectra before and after curing of PCS fiber. The properties of SiC fiber was affected greatly by the degree of cure. The SiC fiber produced by controlling fiber tension during heat treatment showed good properties. The SiC fiber exposed to $1000^{\circ}C$ at air from 1 min. up to maximum 50 hrs showed around 60% reduction in tensile strength. We found that large amount of carbon content on the fiber surface after long-term exposure has resulted in lower tensile strength.

• Journal of Advanced Marine Engineering and Technology
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• v.18 no.3
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• pp.52-62
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• 1994

기계나 구조물 파괴의 대부분은 노치부를 기점으로 하여 발생하기 때문에 첨단복합재료를 노지부 재로서 안전하면서도 경제적으로 사용하기 위해서는 각종 조건하에 있어서 강도특성을 명확히 하는 것은 대단히 중요하다. 본 연구에서는 노치를 갖는 복합재료를 이용하여 각종조건하에서 강도특성평가실험을 행하였으 며, 얻어진 결과를 종합하면 다음과 같다. (1) 첨단복합재료 노치재는 試驗片의 幾可學的 形狀과는 관계없이 노치반경 p만에 의해 결정되는 최대탄성응력 $\sigma_{max}$일정의 條件下에서 破t짧된다. (2) 破斷時 최소단면에서의 공칭응력 $\sigma_{c}$와 응력집중계수 $K_{t}$와의 관계에 있어서,$\sigma_{c}$의 값이 $K_{t}$의 증대와 더불어 떨어지고 있는 부분과, $K_{t}$와 관계없이 거의 일정하게 되고 있는 부분으로 나누어지는 現象은 노치재의 回轉굽힘 또는 인장압축파열에서 보여지는 현상과 外觀上 對應하고 있다. 즉, 정적파괴와 피로파괴는 파괴의 양상이 비슷하다 (3) PEN수지단체의 경우, 피로균열발생은 점발생적 피로균열이 최대탄성응력에 의해 지배되며, 노치에 만감하며,균열전파수명은전수명에 비해 상당히 짧다. (4) 단탄소섬유강화복합재료의 경우, 피로균열은 섬유端에 응력이 집중하기 때문에 일반적으로 섬유端에서 아주 빠른 시기에 발생하지만, 섬유가 피로균열진전에 대해 방해물로 작용하기때문에 아주 천천히 전파한다. (5) 短탄소鐵維는 피로균열발생에 대해서는 負의 강화작용 전수명의 극히 초기단계에 피로균열 발생을, 피로균열전파에 대해서는 正의 강화작용을 한다. (6) 단탄소섬유를 PEN에 강화함으로 인해 정적강도 보다 피로강도에 더 큰 강화효과를 초래했으며, 선형노치역학의 개녀은 첨단 복합재료의 강도평가에 대단히 유효했다.

• Journal of the Korean Society for Nondestructive Testing
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• v.23 no.5
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• pp.418-428
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• 2003

Fiber fracture is one of the dominant failure phenomena affecting the total mechanical Performance of the composites. Fiber fracture locations were measured through the conventional optical microscope and the nondestructive acoustic emission (AE) technique and then were compared together as a function of the epoxy matrix modulus and the fiber surface treatment by the electrodeposition method (ED). Interfacial shear strength (IFSS) was measured using tensile fragmentation test in combination of AE method. ED treatment of the fiber surface enlarged the number of fiber fracture locations in comparison to the untreated case. The number of fiber fracture events measured by the AE method was less than optically obtained one. However, fiber fracture locations determined by AE detection corresponded with those by optical observation with small errors. The source location of fiber breaks by AE analysis could be a nondestructive, valuable method to measure interfacial shear strength (IFSS) of matrix in non-, semi- and/or transparent polymer composites.

• Journal of the Korean Ceramic Society
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• v.41 no.7
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• pp.560-566
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• 2004

To fabricate the continuously porous alumina bodies by multi-extrusion process, carbon powder and ethylene vinyl acetate were used as a pore forming agent and a binder, respectively. As the change of extrusion pass number, reduction ratio as well as the volume fraction of core and tube, the porous alumina bodies having various kind of pore size and porosity could be obtained. The porous bodies showed continuous pore shape, high specific surface as well as high bending strength, which were compared with those of commercial alumina bodies. In-vitro study was carried out using MG-63 osteoblast cells to investigate of their biocompatibility. As a result, the cells grew well on top and bottom as well as inside surface of pore. From the result of in-vivo study of 3-dimensional porous alumina bodies using rats, it was confirmed that any inflammatory response was not found in the subcutaneous tissue around porous body. Also the porous bodies removed from the rats were fully covered with well-developed fibrous tissues and showed the formation of new capillary blood vessels.

• Transactions of the Korean Society of Automotive Engineers
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• v.25 no.3
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• pp.350-359
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• 2017

This paper presents a new holistic development approach for the carbon continuous-fiber composite frame of an automotive sunroof assembly. The original steel frame has been designed to get higher bending stiffness with its corrugated cross-sectional shape. The new approach uses the prepregs of a fast cure epoxy and PCM manufacturing processing. For higher productivity, the new frames feature a very simple plat cross sectional shape but achieve high bending stiffness through the laminate design. The sandwich structure with a PET foam core was presented. The frames were made of carbon UD laminae covered single carbon fabric on the outer surfaces. The fabrics provide torsional stiffness and also hold the carbon UD fibers floating in the low viscous epoxy resin of prepregs at the curing temperature during processing. The final product yields approximately 18 % savings in weight compared with the original.

• Composites Research
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• v.33 no.6
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• pp.383-389
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• 2020

Thermoplastic composite is introduced to design an automotive door impact beam, and the manufacturing process is demonstrated. The safety regulation for vehicles has been steadily tightened, and weight-reduction has become a mandatory factor in the automotive industry. Hence, both high-performance and lightweight are demanded for automotive components. The aim of the present study is to develop an automotive door impact beam using fiber-reinforced thermoplastic composites to reduce the weight of the impact beam while increasing its mechanical performance. A new production method which combines continuous fiber-reinforced composite and LFT(Long Fiber-reinforced Thermoplastic) is implemented by using insert injection molding process. The mechanical performance of the composite impact beam was evaluated using 3-point bending tests. Thermoplastic composite will expand its application range to various automotive components due to its light-weight design capability and high productivity.

• Korean Journal of Materials Research
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• v.4 no.2
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• pp.194-205
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• 1994

In this research, we attempt to fabricate an excellent CFRC(Carbon Fiber Reinforced Carbon), which has good thermal and mechanical properties, with 8H/satin woven fabric prepreg, high modulus and high strength type continuous carbon fiber and raw coal tar pitch(RCTP) matrix or THF soluble fraction(THFSP) matrix which has good graphitizability. Green bodies were fabricated with hot press molding technique and CFRC samples were made after carbonization, impregnation, recarbonization and graphitization steps. For the purpose of characterization of the physical properties, SEM, polarized light microscope, TGA were observed, and tested flexural strength, modulus and ILSS. After heat treating the THFSP matrix up to $2300^{\circ}C$, the value of $C_0$/2 was 3.380$\AA$, which is analogous to the structure of natural graphite and the value of 2$\theta$ is $26.276^{\circ}$ approached to the Bragg's angle of natural graphite. As a result of TGA to test the high temperature air oxidation, the THFSP matrix, graphitized up to $2300^{\circ}C$, exhibited the best air oxidation resistance. And mechanical properties were increased up to 65~70% as fiber volume fraction increased. Because of the good orientation graphitizability, the fracture surface of THFSP matrix CFRC is very good.