• Proceedings of the Korean Vacuum Society Conference
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• 2013.08a
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• pp.284-284
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• 2013

중 에너지 이온 산란 분석법(Medium Energy Ion Scattering Spectrometer, MEIS)은 50~500 keV로 이온을 가속 후 시료에 입사시켜 시료의 원자와 핵간 충돌로 산란되는 일차이온의 에너지를 측정하여 시료를 분석하는 기법으로, 원자층의 깊이 분해능으로 초박막의 표면 계면의 조성과 구조를 분석 할수 있는 유용한 미세 분석기술이다. 본 실험에서 에너지 70~100 keV의 He+ 이온을 사용하여 Pulse Width 1 ns의 Pulsed ion beam을 만들어 Start 신호로 사용하고 Delay-line-detector에 검출된 신호를 End 신호를 이용한 TOF-MEIS System을 개발하였다. 활용 가능한 분석시편으로 Ultra thin film 시편으로 1, 1.5, 2, 2.5, 3, 4 nm의 HfO2, 1.8, 4nm의 SiO2 시편을 분석 하였으며 Ultra Shallow Junction 시편으로 As Doped Si, Cs Doped Si 시편 및 Composition, Core/shell 구조의 Q-dot 시편으로 CdSe, CdSe/ZnS등 다양한 분석 실험을 진행 하였다. Composition, Core/shell 구조의 Q-dot 시편은 Diamond Like Carbon(DLC)의 Substrate에 Mono-layer로 형성하여 분석하였다.

• Proceedings of the Acoustical Society of Korea Conference
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• autumn
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• pp.201-202
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• 2004

고성능 복합 차음패널 개발을 위해 다양한 복합패널의 차음 성능을 측정하고 이를 토대로 최적의 설계변수를 도출하여 , 설계제한조건 내에서 최대의 차음성능을 갖는 복합차음패널을 개발하였다. 특히, 본 연구에서는 Mini-chamber를 이용함으로서, 차음측정을 위해 사용되는 $10m^{2}$ 이상의 시편 대신 $0.6m^{2}$ 의 시편을 사용함으로써, 시편 제작비 및 개발기간을 대폭 줄일 수 있었다. 주요 설계안으로서 stud를 최적화 한 결과, Mini-Chamber에서는 약 5dB의 차음 성능을 향상 시킬 수 있었으며, 잔향실 측정의 경우 약 $2^{-3}dB$의 차음 성능이 향상되었다.

• Proceedings of the Korean Vacuum Society Conference
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• 2010.08a
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• pp.147-147
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• 2010

Ferroxyl Test는 박막의 치밀도를 측정하는 대표적인 방법이다. 본 연구에서는 Ferroxyl Test를 이용하여 박막의 치밀도를 정량적으로 측정할 수 있는 방법을 제안한다. 알루미늄(aluminum; Al)은 뛰어난 내부식성 때문에 모재의 부식을 막을 수 있는 보호막으로 널리 사용되고 있다. Al 박막의 치밀도를 측정하기 위해서 스퍼터링(sputtering)으로 철(Fe) 기판위에 Al 타겟(99.99%)을 이용하여 박막을 코팅하였다. Ferroxyl Test 용액은 순수(deionized water)에 Potassium Ferrocyanide와 황산(또는 염화나타륨과 염화암모늄)을 첨가하여 제작하며, 용액에 거름종이를 적셔 Al이 코팅된 철 시편위에 올려놓고 반응시킨다. 일반적인 Ferroxyl test는 거름종이에 나타난 파란색(prussian blue) 반점의 숫자와 면적으로 치밀도를 측정한다. 하지만 이러한 방법은 측정 오차가 발생할 수 있다. 본 연구에서는 시편에 나타난 반응 반점의 면적을 광학 현미경이나 전자 현미경으로 이미지화하고, 이미지 프로세싱 프로그램을 이용하여 반응 면적을 수치화함으로써 측정오차를 줄이고 정확도를 높이고자 한다. 이러한 측정 방법을 이용하여 알루미늄 박막의 치밀도를 측정한 결과, 최고의 치밀도를 갖는 Al 박막이 Bulk 밀도의 94% 이상으로 측정되었다.

• Journal of the Korean Society for Nondestructive Testing
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• v.18 no.5
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• pp.373-380
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• 1998

The prediction of bone strength by ultrasound velocity and broadband ultrasound attenuation was examined. Ultrasound velocity and broadband attenuation were measured for sixty specimens of human trabecular bone. Samples were divided into two equal groups and loaded in compression at the strain rates of $0.0004\;s^{-1}$ and of $0.08\;s^{-1}$. The ultimate strength was determined for each specimen. Specimens tested at $0.08\;s^{-1}$ had a mean value of strength 63% higher than the specimens tested at $0.0004\;s^{-1}$. Ultrasound velocity and broadband attenuation were significantly associated with compressive strength at both strain rates. Mechanical strength was also correlated strongly with a linear combination of ultrasound velocity and broadband attenuation for both the low and high loading rates. The use of ultrasound parameters may provide good clinical means for assessing the resistance of trabecular bone to both low and high energy trauma.

• Journal of the Korean Society for Nondestructive Testing
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• v.28 no.5
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• pp.395-400
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• 2008

Alternating magnetic field was used for detection of surface flaws on nonmagnetic and magnetic metallic specimens. The nondestructive sensor probe was composed of the planar coil with inductive magnetic thin film yoke as a sensing component and a single straight typed exciting coil. The planar inductive coil sensor with magnetic yoke was fabricated by sputtering, electroplating, dry etching and photolithography process. The alternative currents with the range of 0.1A to 1.0A (0.7 MHz to 1.8 MHz) were applied to the exciting coil. The specimens were prepared with the slit shaped artificial surface flaws (minimum depth and width; 0.5 mm) on metallic plate (Al; nonmagnetic metal and FeC; magnetic metal). The detected signal for the positions and shapes of surface flaws on specimens were obtained with high sensitivity and high signal to ratio. The measured output signals by the non-contacted scanning on surface of FeC specimen with micron-sized crack were converted to the images of the flaws. And these results were compared with the optical images, respectively.

• Composites Research
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• v.13 no.2
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• pp.1-7
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• 2000

A new ultrasonic test method is proposed to obtain elastic constants of unidirectional composite materials nondestructively. In the proposed test method, only longitudinal transducers are used to measure wave velocities by through-transmission method. An aluminum wedge and a flat aluminum rectangular block are placed on each side of the test specimen. Oblique incident longitudinal wave is transmitted from a wedge to the specimen and the mode conversions are occurred sequentially at two interfaces between the specimen and aluminium. Measuring wave velocities converted to longitudinal waves in the rectangular block give all information to determine elastic constants of the composites. In order to determine shear stiffness coefficients, transverse wave velocity is measured indirectly from received longitudinal wave. Effects of anisotropy on waves are also considered in this study.

• Composites Research
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• v.23 no.6
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• pp.61-66
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• 2010

In this paper, the variation of mechanical properties of T800 carbon/epoxy composites according to the forming pressure, which was referred to previous studies on a filament winding process, were investigated. The specimens of all the tests were fabricated by an autoclave de-gassing molding process controlling forming pressure (absolute pressures of 0.1MPa, 0.3MPa, 0.7MPa including vacuum) and water jet cutting after fabricating composite laminates. Various tensile tests were performed for in-plane properties and interlaminar properties were also measured by using Iosipescu test jig. Fiber volume fraction was measured to correlate the property variation and the forming pressure. This properties are expected to be utilized in the design of Type III pressure vessel for hydrogen vehicles which uses the same carbon fiber (T800 carbon fiber) for the filament winding process.

• Journal of the Microelectronics and Packaging Society
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• v.23 no.3
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• pp.63-67
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• 2016

In this paper, we present an indirect method of elastic modulus measurement for various lamination layers formed on polymer-based compliant substrates. Although the elastic modulus of every component is crucial for mechanically reliable microelectronic devices, it is difficult to accurately measure the film properties because the lamination layers are hardly detached from the substrate. In order to resolve the problem, 3-point bending test is conducted with a film-substrate specimen and area transformation rule is applied to the cross-sectional area of the film region. With known substrate modulus, a modulus ratio between the film and the substrate is calculated using bending stiffness of the multilayered specimen obtained from the 3-point bending test. This method is verified using electroplated copper specimens with two types of film-substrate structure; double-sided film and single sided film. Also, common dielectric layers, prepreg (PPG) and dry film solder resist (DF SR), are measured with the double-sided specimen type. The results of copper (110.3 GPa), PPG (22.3 GPa), DF SR (5.0 GPa) were measured with high precision.

• Korean Chemical Engineering Research
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• v.49 no.2
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• pp.206-210
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• 2011

We fabricated rod-like poly(lactic acid)(PLA) specimens through applying various methods of equal-channel angular extrusion(ECAE) process and investigated the change of thermal and mechanical properties of specimens before and after each ECAE process. Combining three re-injection routes(A, BC, and C) and three pass counts(1, 2 and 4) allowed us to fabricate 7 different PLA specimens. Thermal properties of each specimen were measured by both differential scanning calorimeter and thermo-gravimetric analyzer. Shear strains of each specimen with respect to applied loads were measured by indentation hardness tester. Field emmision scanning electron microscopy was used to observe internal microstructure of cross-section of each specimen. The observed microstructures qualitatively supported the explanation of hardness test results. Among 7 specimens, PLA-P2A showed the biggest shear strain probably due to its dense microstructure.

• Composites Research
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• v.31 no.3
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• pp.99-103
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• 2018

This paper visualizes the full-field permittivity distribution at the standard specimens having known electromagnetic characteristics using a scanning free space measurement (SFSM) system. First, in the two Teflon specimens with different thicknesses, the real and loss tangent of permittivity could be measured and the results agreed to the theoretical and other measurement values. Then the system has been applied to Glass/epoxy and visualized different permittivity distribution depending on the material kind. Therefore, this approach will overcome the point measurement limitation of FSM and can be used for even sub-structural full-field electromagnetic evaluation of stealth and radome structures.