• Title/Summary/Keyword: 초음파합성

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Preparation of Biopolymer coated Magnetite And Magnetic Biopolymer Microsphere Particles for Medical Application (의학적 응용을 위한 생체 고분자로 피복 된 자성 나노 입자와 미소구체의 제조)

  • Ko, Sang-Gil;Cho, Jun-Hee;Ahn, Yang-kyu;Song, Ki-Chang;Choi, Eun-Jung
    • Journal of the Korean Magnetics Society
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    • v.16 no.4
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    • pp.221-227
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    • 2006
  • We have synthesized uniform nanometer sized magnetite particles using chemical coprecipitation technique through a sonochemical method with surfactant such as oleic acid. Magnetite phase nanoparticles could be observed from X-ray diffraction. Magnetite nanoparticles is surface phase morphology and biopolymer-microspheres for Application Medical. Magnetite nanoparticles coated biopolymer. Atomic Force Microscope (AFM) was used to image the coated nanoparticles. Magnetic colloid suspensions containing particles with sodium oleate, chitosan and $\beta$-glucan have been prepared. The morphology of the magnetic biopolymer microsphere particles were characterized using optical microscope. Magnetic hysteresis measurement were performed using a superconducting quantum interference device (SQUID) magnetometer at room temperature to investigate the magnetic properties of the biopolymer microspheres and magnetite coated biopolymer including magnetite nanoparticles. Magnetic Resonance (MR) imaging was used to investigate biopolymer coated nanoparticles and biopolymer microspheres.

The Study on Ultrasound Physical Characteristic and Synthesis of Tissue Mimicking Materials Used New Materials (신소재를 사용한 인체조직모사물질의 합성과 초음파 물리적 특성에 관한 연구)

  • Ma, Sang-Chull;Kim, Hwa-Sun;Ann, Young-Man
    • Journal of radiological science and technology
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    • v.33 no.3
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    • pp.245-252
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    • 2010
  • This study analyzed speed of sound, impedance, attenuation coefficient in accordance with acoustic characteristic standard of body soft tissue corresponding with Annex DD of IEC standard 60601-2-37(2007) which is about tissue mimicking materials (TMM) synthesized by polyurethane as a main material and new type of n-type scatter materials. This study reached the following conclusion after analyzing and evaluating image characteristic with SONOACE 9900 c PRIME (MEDESON Co.) and brightness, maximum penetration with convex probe (2.5~5.0 MHz). When n-type scatter materials are increasingly synthesised 0~8% with prepolymer as a main material and polyol mixture as a catalyst, 1. The more scatter materials are increased, the more sound speed of TMM becomes closely similar to soft tissue. 2. The more scatter materials are decreased, the more acoustic impedance becomes closely similar to soft tissue. 3. The more scatter materials are increased, the more attenuation coefficient is increased. 4. The more scatter materials are increased, the more average brightness of images is increased, but there is threshold. 5. The maximum penetration becomes closely similar to soft tissue at the 6% TMM as a scatter material.

Development of an Automatic Monitoring System for Ultrasound Signals Using Artificial Intelligence and Convolutional Neural Networks (인공지능을 활용한 초음파 신호와 합성곱 신경망 기반 자동 적조 모니터링 시스템)

  • Daehun Kim;Hyeon-Ju Jeon;O-Joun Lee;Hae Gyun Lim
    • Proceedings of the Korea Information Processing Society Conference
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    • 2023.11a
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    • pp.662-664
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    • 2023
  • 해양 식물플랑크톤의 성장은 유해적인 적조를 유발할 수 있으며, 이는 여러 국가의 생태계에 피해를 주는 상황이다. 적조를 모니터링하는 것은 식물플랑크톤 미생물의 증가를 예방하고 통제하기 위해 중요하다. 그러나 현재의 적조 모니터링 기술은 날씨, 시간 제약 및 실시간 모니터링에 대한 어려움으로 인해 측정 정확도에 영향을 미치는 한계가 있다. 본 연구는 특히 적조 발생을 감지하기 위한 목적으로 개발된 자동 실시간 모니터링 시스템의 성공적인 개발을 보여준다. 개발한 시스템은 음향 반사파 데이터 처리를 통해 합성곱 신경망(Convolutional neural networks, CNN)을 활용하여 식물플랑크톤 농도를 정확하게 구별할 수 있다. 특히, 이 CNN 모델은 음향 신호의 변환된 주파수 스펙트럼과 Cochlodinium polykrikoides (C. polykrikoides)의 농도 간의 상관 관계를 수립하는 데 뛰어난 효과를 나타냈다. 이 CNN 은 C. polykrikoides 를 감지하는 데 0.90 의 정확도를 보여준다. 이러한 모니터링과 CNN 분류의 활용은 실시간 측정의 중요한 잠재력을 보여주며, 추가적인 절차가 필요 없는 자동 모니터링 시스템을 구축할 수 있을 것으로 예상된다.

Effect of Concentration of Tetraethoxysilane and Hydrochloric Acid on the Morphologies of Mesoporous Silica Microspheres (테트라에톡시실란 및 염산 농도에 따른 메조다공성 실리카 마이크로스피어의 모폴로지 변동에 관한 연구)

  • Ji, Sun-Kyung;Kim, Jong-Yun;Yoon, Suk-Bon;Choi, Yong-Suk;Jung, Sung-Hee;Song, Kyu-Seok;Lee, Bum-Jae
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.9 no.1
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    • pp.1-11
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    • 2011
  • Tetraethoxysilane(TEOS) as a silica precursor and hydrochloric acid as an acid catalyst have been used in a surfactant-template synthesis of micrometer-sized mesoporous silica microspheres based on the macroemulsion technique. Increase in the concentration of tetraethoxysilane of the reaction mixture has a serious destructive effect on the particle shape and pore structure. As the acid concentration increases, relatively small microspheres are formed without destroying their spherical morphology of the particles as well as the pore structures. However, due to the attractive interaction between particles in an acidic condition, strong silica agglomerates are formed, and therefore are subject to a post-ultrasonic treatment to separate into an individual single particle.

Synthesis and Crystallization of Hydrazinium Nitroformate(HNF) as Eco-friendly Oxidizer (친환경 산화제 HNF 합성 및 결정화 연구)

  • Kim, Jina;Kim, Min Jun;Min, Byoung Sun
    • Journal of the Korean Society of Propulsion Engineers
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    • v.19 no.4
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    • pp.69-76
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    • 2015
  • Recently, environmental sustainability of the transitional explosives and propellants is an issue of growing importance in energetic materials. For examples, ammonium perchlorate(AP) as an solid propellants oxidizer could create a poisonous gas and atmospheric pollutions, such as HCl. Among the several oxidizers, hydrazinium nitroformate(HNF) is an effective candidate substance for eco-friendly oxidizer, which has high density, pressure index, and less smog generating property during combustion for the Divert and Attitude Control System(DACS). This study was confirmed a synthesis through various conditions, was performed for the essential data of solubility the crystallization process. Also, crystallization process such as cooling, drowning-out and sonication were performed.

Change of Anti-reflective Optical Property by Nano-structural Control of Alumina Layer through Hydro-thermal Process (수열합성 공정을 통한 알루미나 코팅층의 나노구조 조절에 의한 반사방지 특성의 변화)

  • Lee, Yun-Yi;Son, Dae-Hee;Lee, Seung-Ho;Lee, Gun-Dae;Hong, Seong-Soo;Park, Seong-Soo
    • Applied Chemistry for Engineering
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    • v.21 no.5
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    • pp.564-569
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    • 2010
  • Highly anti-reflective optical property has been focussed in the field of thin film and display because of increasing demands to the high transparency and clearness of optical component. In this study, to obtain anti-reflective property, the formation of aluminium oxide with nanoscaled flowerlike frame structure was introduced as oxide material monolayer on the substrate by hydrothermal synthesis through sol-gel method. The properties of coating layer were measured by the means of UV-Vis spectroscopy, FT-IR spectroscopy, XRD, and FE-SEM. The morphology of coating layer in alumina-sol coated samples was controlled by hydrothermal temperature and time with aid of ultrasound. It was found that high transparency and anti-reflective optical properties were obtained the formation of flowerlike nanoframe structure.

Continuous Processing of Monodispersed Zirconia Powders (초음파 혼합 연속공정에 의한 단분산 지르코니아 분체의 합성)

  • Rhee, Jhun;Jo, Dong-Soo
    • Journal of the Korean Ceramic Society
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    • v.29 no.12
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    • pp.919-925
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    • 1992
  • Continuous synthesis process for monodispersed zirconia powders with ultrasonic wave mixing was developed. Reactant solutions were flowed through a T-tube with small diameter and then mixed in a microscale with ultrasonification. Reaction and aging were followed during the mixed solution of reactants is in plug flowing through a narrow long teflon tubing. Zr(n-OC4H9)4 in ethanol and H2O in ethanol were used as reactants. From this process monodispersed, spherical, non-agglomerated, singlet hydrated zirconia powders with 0.6 $\mu\textrm{m}$ average size were obtained. Geometrical standard deviation of the particle size distribution was less than 1.2 with ultrasonic mixing, and the geometrical standard deviation was not affected by the flow rate of the reactants.

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Tx/Rx Bi-Directional Focusing by Using Multi-Element Defocusing Method in Ultrasonic Imaging System (초음파 영상시스템에서 다수 소자의 역 초점화 방법을 이용한 송수신 양방향 빔집속)

  • 이용호;송태경;안영복
    • Journal of Biomedical Engineering Research
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    • v.20 no.6
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    • pp.583-589
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    • 1999
  • 본 논문에서는 다수의 변환자 소자를 사용해서 빔을 역 초점화하는 새로운 방법을 제안한다. 제안된 방법은 64개의 소자를 사용해서 한 개의 소자에서 얻은 것과 거의 동일한 모양의 구면파를 얻을 수 있다. 이렇게 얻은 구면파는 합성집속에서 영상의 신호 대 잡음비를 높이는데 사용된다. 실험에서 제안된 방법은 영상의 해상도를 저하시키지 않고 신호대 잡음비를 크게 향상시킬 수 있음을 보여주었다. 특히 제안된 방법은 기존의 역초점화 방법에 의해 우수한 잡음 특성을 갖는다. 여기서 영상은 송수신의 양방향 빔집속에 의해서 얻었다.

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Preparation of the Copper Oxalate Powder by Ethanol Oxalic Acid Method (수산에타놀법을 이용한 수산동 분말의 합성)

  • Choi, H.L.;Lee, B.W.
    • Journal of Power System Engineering
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    • v.9 no.4
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    • pp.124-129
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    • 2005
  • Copper oxide, CuO, are very important components include of high temperature super- conductors, and widely used. The properties of sintered materials were affected by the size and shape of copper oxide with starting materials in the solid-phase reaction. A homogeneous and fine CuO powder was prepared by thermal decomposition of the copper oxalate precursor. Copper oxalate was precipitated by the addition of copper nitrate solution to an oxalic acid solution. The influence of various factors such as temperature, pH, concentration as well as ultrasonic irradiation in the solution were investigated.

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Distance Estimation Using Discretized Frequency Synthesis of Ultrasound Signals (초음파의 이산 주파수 합성을 이용한 거리 측정)

  • Park, Sang-Wook;Kim, Dae-Eun
    • Journal of Institute of Control, Robotics and Systems
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    • v.17 no.5
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    • pp.499-504
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    • 2011
  • In this paper, we suggest a method for discretized frequency modulations of ultrasonic signals. A continuous sweep of frequency modulation signals can be modelled with fine levels of discretization. If the ultrasound signals are modulated with monotonically decreasing frequencies, then the cross-correlation between an emitted signal and received signal can be used to identify the distance of multiple target objects. For the discretized frequency synthesis, CF ultrasounds with different frequencies are serially ordered. The auto-correlation test with the signal shows effective results for distance estimation. The discretized frequency syntheses have better distance resolution than CF ultrasound signals and the resolution depends on the number of the combined ultrasound frequencies.