• 제목/요약/키워드: 초음파염색

검색결과 54건 처리시간 0.025초

은(Ag) 광증착에 의한 폴리우레탄/$TiO_2$ 하이브리드 멤브레인 필름의 항균특성 (Antibacterial Properties of PU/$TiO_2$ Hybrid membrane Films after Photodepositing of Silver)

  • 조성민;민병길;지광환
    • 한국염색가공학회:학술대회논문집
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    • 한국염색가공학회 2012년도 제46차 학술발표회
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    • pp.50-50
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    • 2012
  • 투습방수필름으로 많이 사용되고 있는 폴리우레탄(PU)에 광촉매 기능성을 가지고 있는 나노-$TiO_2$(Degussa P25)를 1~10wt% 복합시킨 후, 은(Ag)이온 수용액에서 자외선 조사에 의한 광증착시키는 과정을 거쳐 은이 도핑된 PU/$TiO_2$/Ag 하이브리드 멤브레인 필름을 제조하였다. (주)비에스지에서 제공받은 PU/DMF/MEK 용액에 $TiO_2$를 초음파로 균일하게 분산배합한 후, 필름캐스팅하여 만든 필름을 AgNO3 수용액에 침지시키고 254nm의 자외선을 30~120초 동안 조사하는 광증착법으로 은을 환원시켜 도핑시켰다. 은 도핑된 하이브리드 필름을 Shaking flask method에서 폐렴간균, 황색포도상구균에 대한 항균성을 측정하고, Clear zone method에서 대장균에 대한 항균성을 측정한 결과, $TiO_2$ 함량이 3wt% 이상이고 UV조사시간이 60초 이상인 경우 99.9% 이상의 항균성을 나타내는 것을 확인하였다.

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초음파 직물수세기의 구성 및 구동 특성 (Assemblage and Driving Characteristics of a Ultrasonic Fabric Washing Machine)

  • 이춘길;이광수
    • 한국염색가공학회지
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    • 제12권3호
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    • pp.207-217
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    • 2000
  • A new, high-efficiency ultrasonic fabric washing machine was developed to be an energy-efficient washing machine and to enhance fabric washing quality in washing processes of the dyeing and finishing process in the textile industry. This system is composed of ultrasonic wave generator, air blowing nozzle, torque motor for fabric tension control, and enclosed washing bath, multi-tube type exchanger, noiseless heater, air cylinder, expander roller, mangle upper and lower rollers, bend bar, dancer, shower spray nozzle, and solenoid valve, and so on. These elements are synergised for fabric washing. One of the very important principles is the low tension fabric running system. For an efficient washing effect, a counter flow system is also adopted. The new system also adopts the dancer and torque motor to control fabric tension and prevent fabric creasing. Shower spray nozzle, counter flow and overflow apparatus, and air-blowing apparatus are adopted to enhance the fabric washing effect. In this study, peach yoryu, exter, and moss crepe fabrics were washed by the general and ultrasonic washing systems under different conditions respectively. The washing efficiency was affected by the fabric running speed and characteristics of fabrics. Size content after washing increased with increasing the fabric running speed. The values in the general washing system were higher than those of the ultrasonic washing system. The changes of conductivity in the ultrasonic and the cooling bath were affected by the running time under the ultrasonic generating. The values of conductivity decreased as the experimental time passed.

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초음파를 이용한 해도직물의 감량 가공에 관한 연구 (A Study on the Weight Loss of Island-in-a Sea Fabrics by Ultrasonic)

  • 신현세;윤철수;임병완
    • 한국염색가공학회지
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    • 제16권1호
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    • pp.40-47
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    • 2004
  • Alkaline treatment gives Sea-Island type yam to produce microfiber and silk-like touch. But this treatment have some problems in dyeing and finishing process. To solve some problem occurred in dyeing and finishing of polyester fabric, the ultrasonic treatment technique was used recently. This study was carried out to confirm the effect of the ultrasonic treatment on alkaline weight loss finishing of polyester fiber under general alkaline treatment conditions; NaOH concentration 2, 3, 4, and 5%, treatment time 5, 10, 15, and 20 minutes, treatment temperature 70, 80, 90, and 99'E, respectively. On the other hand, the three way lay out method was used to test of significant obtained data from alkaline treatment. It was found that weight loss increased with increasing the NaOH concentration, temperature, and time. Also, in case of PET/Co-PET fabrics by ultrasonic, weight loss and dissolution of microfiber were superior to PET/Co-PET fabrics without ultrasonic. Tensile strength and modulus decreased with increasing NaOH concentrations and hydrolysis time. Therefore, the effect of alkali hydrolysis by ultrasonic application was better than that of the conventional method.

초음파 처리된 대나무섬유와 케냐프섬유 복합재의 기계적 특성 비교 연구 (Comparative Study on Mechanical Properties of Sonicated Bamboo and Kenaf Fiber Composite)

  • 이수경;박은영;박태성;안승국
    • 한국염색가공학회지
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    • 제32권4호
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    • pp.274-280
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    • 2020
  • This study compared the mechanical properties of bamboo fiber composites and kenaf fiber composites through physical treatment (ultrasonic treatment). Kenaf, a composite of PP reinforced with bamboo fiber, was made using injection molding technology. PP was used as a binder and the ultrasonic treatment time of bamboo and kenaf was increased by 30 minutes to compare and study various mechanical properties of bamboo and kenaf composites through physical treatment. Interfacial properties such as internal cracks and internal structure of the wave cross section were confirmed using a scanning electron microscope (SEM). As a result of the ultrasonic treatment, most of the characteristics were fragile as the ultrasonic treatment time was increased, and it was confirmed that the natural characteristics of the twisted fibers had a great influence on the characteristics of the composite material.

개의 위에서 발생한 골수외 형질세포종 (Gastric Extramedullary Plasmacytoma in a Dog)

  • 채웅주;권도형;권진아;김재훈;정주현
    • 한국임상수의학회지
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    • 제29권4호
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    • pp.356-359
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    • 2012
  • 암컷, 8년령, 3.2 kg의 시츄견이 간헐적인 구토를 주증으로 내원하였다. 기본 혈액검사 및 방사선 검사에서 특별한 이상 소견은 관찰되지 않았다. 복부 초음파 검사에서 위벽에서 유래한 것으로 생각되는 저에코의 둥근 종괴가 관찰되었다. 위 내시경 검사에서 둥근 종괴가 유문동 벽에서 내강으로 돌출되어 있고, 종괴 및 주변 점막의 비정상적인 소견은 관찰되지 않았다. 이에 위 종괴 절제술을 실시하였고, 면역 염색을 포함한 조직학적 검사에서 extramedullary plasmacytoma로 진단되었다. 환자는 임상 증상이 개선되었으며, 약 2년 동안 재발 및 전이 소견 없이 건강한 상태이다.

말티즈 개에서 발생한 갑상선수질암 (Medullary Thyroid Carcinoma in a Maltese Dog)

  • 현희진;정수교;김재훈
    • 한국임상수의학회지
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    • 제31권5호
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    • pp.435-438
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    • 2014
  • 11세령, 체중 2.67 kg, 암컷 Maltese의 기관 인근 경부에서 3주 전부터 종괴가 촉진되어 동물병원에 내원하였으며, 방사선 및 초음파 검사 결과 기관 및 미주신경 주위에 불투과성의 종괴가 확인되었다. 외과적으로 절제된 단일한 종괴의 크기는 $3.5{\times}2{\times}0.8cm$였다. 병리조직학적으로 큰 종양 병소가 정상 갑상선 조직과 혼재되어 있었다. 종양 병소는 형질세포와 같은 형태를 보이는 종양세포들이 모여 있는 다양한 크기의 소포로 구성되어 있고, 이 소포들은 미세한 섬유혈관중격에 의해 구획되어 있었다. 종양세포들은 인근 결합조직과 피막으로 침습하는 경향을 나타내었다. 면역조직화학염색을 실시한 결과 종양세포들은 사이토케라틴(AE1/AE3), 크로모그래닌 A, 신경원 특이 에놀라제(NSE)에 대하여 강한 양성 반응을, vimentin에는 음성 반응을 보이고 있었다. 육안병변, 병리조직학적 및 면역조직화학 염색의 특징을 토대로 본 증례는 갑상선수질암으로 진단되었다.

초음파를 적용한 PET 직물의 알칼리 가수분해에 관한 연구(II) - 기공특성과 올리고머 분석 - (A Study on the Alkali Hydrolysis of PET fabrics with Ultrasonic Application(II)- Surface Porosity and Oligomer Analysis -)

  • 김삼수;서말용;박성우;윤태희;이승구;허만우
    • 한국염색가공학회지
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    • 제14권6호
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    • pp.305-312
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    • 2002
  • In order to give a silk-like touch to PET fabrics, the PET fabrics were treated with NaOH alkaline solution in various conditions. In alkaline treatment, the liquor flow type pilot weight reduction apparatus with magnetostrictive ultrasonic transducer was used for the study. The effects of ultrasonic application, treatment time and temperature at NaOH 4% and 6"A solution on the decomposition rate of PET fabrics. From the results of the decomposition rate of PET fabrics, the qualitative and quantitative analysis of oligomer after decomposition of PET fabrics carried out by the HPLC. On the other hand, the surface pore characteristics of decomposition PET fabrics measured by porosimetery. The pore characteristics on the surface of treated PET fiber depended on the decomposition rate and did not depend on the ultrasonic cavitation. The pore diameter of alkaline untreated PET fiber were 15A and those of treated PET fibers were 5~6$\AA$ at the maximum pore volume. The average pore sizes of fiber before and after treatment were 141 h and 160h, respectively. Total amount of oligomer of the untreated PET fibers were 1.70wt% and 67.7% of total oligomer occupied with PET cyclic trimer and PET cyclic tetramer. Total amount of oligomer of fiber with 26.9% and 48.0% of weight loss without ultrasonic application were 1.78wt% and 1.79wt%, respectively. Also total amount oligomer of fibers which were reduced 27.7% and 48.2% of weight loss with ultrasonic application were 1.74wt%. This result showed that the removal rate of oligomer in the process of alkaline hydrolysis with ultrasonic higher than that of without ultrasonic application.tion.

호부직물의 초음파 수세에 의한 역학적 특성의 변화 (On the Change of Fabric Mechanical properties in Ultrasonic Fabric Washing System)

  • Lee, Choon-Gil;Park, Sung-Diuk;Oh, Bong-Hyo
    • 한국염색가공학회지
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    • 제9권4호
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    • pp.28-38
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    • 1997
  • Peach skin fabrics were washed by the general and ultrasonic washing systems using different conditions. The physical properties of the washed fabrics were estimated. The following results were obtained through experimental data and their analysis. The tensile properties were changed due to fabric running speed and washing methods. The lower the running speed, the higher the extensibility and resilience and the lower the linearity and tensile energy. In the general washing method, the extensibility and resilience had lower values than those of the ultrasonic washing method and the linearity and tensile energy had the higher values than those of the ultrasonic washing system. The bending properties, bending moment and histeresis, were estimated. These values were generally lower in the ultrasonic washing system than those of the general washing system. The faster the washing speed, the higher the value of hysterisis. The shear properties were affected by the fabric running speed and washing methods. Shear stiffness and hysteresis of shear forces increased according to the increase of the fabric running speed. The values were higher in the general washing system than those of the ultrasonic washing system. The compressional energy was affected by the fabric running speed. The higher the fabric speed the higher the compressional energy. The ultrasonic washing system had lower compressional energy than the general washing system. The higher the running speed, the lower the coefficient of friction and geometrical roughness. The values of geometrical roughness were infienced by the removal of the sizing agent. The higher the remaining sizing agent, the higher the fabric weight and the thicker the thickness of fabric.

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개의 신우 이행상피암종의 면역조직화학적 진단 (Immunohistochemical Diagnosis of Renal Pelvis Transitional Cell Carcinoma in a Dog)

  • 양형석;강상철;김재훈
    • 한국임상수의학회지
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    • 제30권4호
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    • pp.292-295
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    • 2013
  • 9세령의 수컷 도베르만견이 5개월간 간헐적인 혈뇨, 구토 및 당뇨증상을 보여 동물병원에 내원하였다. 초음파상에서 종대된 좌측 신장의 수질부위에 종괴가 발견되었다. 육안적으로 좌측 신장의 피질 및 수질부는 현저하게 위축되어 있었으며 신우 부위는 종괴로 인하여 확장된 수신증을 나타내었다. 크기 4~5.5 cm의 유두상으로 돌출된 꽃자루와 같은 단일종괴가 신우 부위에 있으며, 요관으로 뻗어 있었다. 병리조직학적으로 종괴는 나뭇가지 모양으로 무수히 돌출된 유두상의 돌기들로 구성되어 있었다. 이 돌기들은 섬유혈관성 중심부와 뚜렷한 이형태성을 가지는 여러 층의 종양화된 이행상피들로 피복되어 있었다. 면역조직화학염색을 실시한 결과 종양세포들은 사이토케라틴(cytokeratin: CK) 7, 19, CK clone MNF116 및 CK HMW에 대해서 양성을 보였으나 CK 8 LMW에서는 음성 반응을 나타내었다. 육안적인 특징, 병리조직학적 소견 및 면역조직화학염색에 의한 사이토케라틴의 반응성을 토대로 이 종괴는 개의 신우에서 발생한 이행상피암종으로 진단되었다.

초음파로 추출된 홍화색소의 특성 분석과 염색성 평가 (Physiochemical Properties and Dyeability of Safflower Colorants Extracted by Ultrasonic Treatment)

  • 김용숙;최종명
    • 한국의류산업학회지
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    • 제11권2호
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    • pp.337-343
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    • 2009
  • This study systematically investigated a method for extraction of safflower (Carthamus tinctorius Linnaeus) colorants by ultrasonic treatment. Compared to pigments productivity and cell wall structures of safflower after general and ultrasonic method, the ultrasonic method showed high extraction efficiency of safflower pigments due to destruction of safflower cell wall caused by high vibration energies. Microscopic analysis confirmed the hypothesis that the ultrasonic treatment of safflower caused its cell wall structure loosened and made efficient extraction of safflower pigments. And also, LC-MS/MS analysis revealed that productivities of the yellow and red safflower pigments by ultrasonic method were 21.9% and 14.6% higher, respectively, than those of pigments extracted by general method. The ultrasonic extracted yellow and red colorants could be used to dye not only natural fibers like cotton, silk and wool, but also synthetic fiber like nylon, and generally gave a better color tone than the general extracted colorants from safflower due to the affinities of red and yellow colorant on different fibers. As the yellow and red colorant were extracted by ultrasonic treatment in water, the K/S value on of 550/440nm of cotton and rayon was increased but in the case of silk and wool the change of this value was almost not detected. Finally, this technique might provide a solution to establish reproducibility and standardization for the extraction and dyeing methods on fabrics.